DE1089101B - Verfahren zur Herstellung eines in Wasser leicht loeslichen sauren Wollfarbstoffes - Google Patents
Verfahren zur Herstellung eines in Wasser leicht loeslichen sauren WollfarbstoffesInfo
- Publication number
- DE1089101B DE1089101B DEF23402A DEF0023402A DE1089101B DE 1089101 B DE1089101 B DE 1089101B DE F23402 A DEF23402 A DE F23402A DE F0023402 A DEF0023402 A DE F0023402A DE 1089101 B DE1089101 B DE 1089101B
- Authority
- DE
- Germany
- Prior art keywords
- water
- readily soluble
- production
- dye
- anthraquinone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims description 10
- 210000002268 wool Anatomy 0.000 title claims description 7
- 230000002378 acidificating effect Effects 0.000 title claims description 4
- 238000000034 method Methods 0.000 title claims description 3
- 238000004519 manufacturing process Methods 0.000 title description 2
- 239000002253 acid Substances 0.000 claims description 6
- 238000004040 coloring Methods 0.000 claims description 3
- 238000006277 sulfonation reaction Methods 0.000 claims description 3
- QLBNNVIXTQHNTB-UHFFFAOYSA-N 1,4-bis(4-cyclohexylanilino)anthracene-9,10-dione Chemical compound C1=CC(NC=2C=CC(=CC=2)C2CCCCC2)=C2C(=O)C3=CC=CC=C3C(=O)C2=C1NC(C=C1)=CC=C1C1CCCCC1 QLBNNVIXTQHNTB-UHFFFAOYSA-N 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 239000002244 precipitate Substances 0.000 claims description 2
- 239000000975 dye Substances 0.000 description 9
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 238000004043 dyeing Methods 0.000 description 4
- BDHFUVZGWQCTTF-UHFFFAOYSA-N sulfonic acid Chemical compound OS(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-N 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 150000003863 ammonium salts Chemical class 0.000 description 2
- 159000000000 sodium salts Chemical class 0.000 description 2
- -1 1,4-di- (p-cyclohexylphenylamino) anthraquinone disulfonic acid Chemical compound 0.000 description 1
- 229920001353 Dextrin Polymers 0.000 description 1
- 239000004375 Dextrin Substances 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 150000001447 alkali salts Chemical class 0.000 description 1
- PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 description 1
- 150000004056 anthraquinones Chemical class 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 235000019425 dextrin Nutrition 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000010446 mirabilite Substances 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- TVRGPOFMYCMNRB-UHFFFAOYSA-N quinizarine green ss Chemical class C1=CC(C)=CC=C1NC(C=1C(=O)C2=CC=CC=C2C(=O)C=11)=CC=C1NC1=CC=C(C)C=C1 TVRGPOFMYCMNRB-UHFFFAOYSA-N 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000005185 salting out Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B1/00—Dyes with anthracene nucleus not condensed with any other ring
- C09B1/16—Amino-anthraquinones
- C09B1/20—Preparation from starting materials already containing the anthracene nucleus
- C09B1/26—Dyes with amino groups substituted by hydrocarbon radicals
- C09B1/32—Dyes with amino groups substituted by hydrocarbon radicals substituted by aryl groups
- C09B1/34—Dyes with amino groups substituted by hydrocarbon radicals substituted by aryl groups sulfonated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BE569187D BE569187A (enrdf_load_stackoverflow) | 1957-07-05 | ||
| DEF23402A DE1089101B (de) | 1957-07-05 | 1957-07-05 | Verfahren zur Herstellung eines in Wasser leicht loeslichen sauren Wollfarbstoffes |
| GB2058758A GB837935A (en) | 1957-07-05 | 1958-06-26 | Anthraquinone dyestuffs |
| FR1197569D FR1197569A (fr) | 1957-07-05 | 1958-07-04 | Colorants d'anthraquinone |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEF23402A DE1089101B (de) | 1957-07-05 | 1957-07-05 | Verfahren zur Herstellung eines in Wasser leicht loeslichen sauren Wollfarbstoffes |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1089101B true DE1089101B (de) | 1960-09-15 |
Family
ID=7090825
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEF23402A Pending DE1089101B (de) | 1957-07-05 | 1957-07-05 | Verfahren zur Herstellung eines in Wasser leicht loeslichen sauren Wollfarbstoffes |
Country Status (4)
| Country | Link |
|---|---|
| BE (1) | BE569187A (enrdf_load_stackoverflow) |
| DE (1) | DE1089101B (enrdf_load_stackoverflow) |
| FR (1) | FR1197569A (enrdf_load_stackoverflow) |
| GB (1) | GB837935A (enrdf_load_stackoverflow) |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2042757A (en) * | 1933-03-01 | 1936-06-02 | Gen Aniline Works Inc | Process of preparing acid wool dyestuffs of the anthraquinone series and the dyestuffs thus obtainable |
-
0
- BE BE569187D patent/BE569187A/xx unknown
-
1957
- 1957-07-05 DE DEF23402A patent/DE1089101B/de active Pending
-
1958
- 1958-06-26 GB GB2058758A patent/GB837935A/en not_active Expired
- 1958-07-04 FR FR1197569D patent/FR1197569A/fr not_active Expired
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2042757A (en) * | 1933-03-01 | 1936-06-02 | Gen Aniline Works Inc | Process of preparing acid wool dyestuffs of the anthraquinone series and the dyestuffs thus obtainable |
Also Published As
| Publication number | Publication date |
|---|---|
| BE569187A (enrdf_load_stackoverflow) | |
| FR1197569A (fr) | 1959-12-01 |
| GB837935A (en) | 1960-06-15 |
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