DD147103A5 - Verfahren zur herstellung von 2-alkoxy-4,6-dichlor-s-triazinen - Google Patents
Verfahren zur herstellung von 2-alkoxy-4,6-dichlor-s-triazinen Download PDFInfo
- Publication number
- DD147103A5 DD147103A5 DD79216460A DD21646079A DD147103A5 DD 147103 A5 DD147103 A5 DD 147103A5 DD 79216460 A DD79216460 A DD 79216460A DD 21646079 A DD21646079 A DD 21646079A DD 147103 A5 DD147103 A5 DD 147103A5
- Authority
- DD
- German Democratic Republic
- Prior art keywords
- cyanuric chloride
- nozzle
- tubular container
- container
- alkoxy
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 17
- 238000002360 preparation method Methods 0.000 title claims abstract description 5
- 239000007788 liquid Substances 0.000 claims abstract description 29
- MGNCLNQXLYJVJD-UHFFFAOYSA-N cyanuric chloride Chemical compound ClC1=NC(Cl)=NC(Cl)=N1 MGNCLNQXLYJVJD-UHFFFAOYSA-N 0.000 claims abstract description 25
- 238000006243 chemical reaction Methods 0.000 claims abstract description 19
- 238000002156 mixing Methods 0.000 claims abstract description 15
- 239000002253 acid Substances 0.000 claims abstract description 9
- 150000001298 alcohols Chemical class 0.000 claims abstract description 8
- 239000011230 binding agent Substances 0.000 claims abstract description 6
- 239000007921 spray Substances 0.000 claims description 14
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 4
- 229910052801 chlorine Inorganic materials 0.000 claims description 4
- 239000000460 chlorine Substances 0.000 claims description 4
- QPJDMGCKMHUXFD-UHFFFAOYSA-N cyanogen chloride Chemical compound ClC#N QPJDMGCKMHUXFD-UHFFFAOYSA-N 0.000 claims description 4
- 239000003513 alkali Substances 0.000 claims description 2
- 210000000481 breast Anatomy 0.000 claims description 2
- 239000011261 inert gas Substances 0.000 claims description 2
- 238000002844 melting Methods 0.000 claims description 2
- 230000008018 melting Effects 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims 2
- 125000003342 alkenyl group Chemical group 0.000 claims 1
- 125000004429 atom Chemical group 0.000 claims 1
- 125000004432 carbon atom Chemical group C* 0.000 claims 1
- 210000004907 gland Anatomy 0.000 claims 1
- 239000000376 reactant Substances 0.000 abstract description 3
- 230000000630 rising effect Effects 0.000 abstract 1
- 239000012530 fluid Substances 0.000 description 8
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- 239000002904 solvent Substances 0.000 description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 4
- ZSIAUFGUXNUGDI-UHFFFAOYSA-N hexan-1-ol Chemical compound CCCCCCO ZSIAUFGUXNUGDI-UHFFFAOYSA-N 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- BWZVCCNYKMEVEX-UHFFFAOYSA-N 2,4,6-Trimethylpyridine Chemical compound CC1=CC(C)=NC(C)=C1 BWZVCCNYKMEVEX-UHFFFAOYSA-N 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000000370 acceptor Substances 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- SBASXUCJHJRPEV-UHFFFAOYSA-N 2-(2-methoxyethoxy)ethanol Chemical compound COCCOCCO SBASXUCJHJRPEV-UHFFFAOYSA-N 0.000 description 2
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 2
- AMQJEAYHLZJPGS-UHFFFAOYSA-N N-Pentanol Chemical compound CCCCCO AMQJEAYHLZJPGS-UHFFFAOYSA-N 0.000 description 2
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 2
- XXROGKLTLUQVRX-UHFFFAOYSA-N allyl alcohol Chemical compound OCC=C XXROGKLTLUQVRX-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- XLJMAIOERFSOGZ-UHFFFAOYSA-N cyanic acid Chemical compound OC#N XLJMAIOERFSOGZ-UHFFFAOYSA-N 0.000 description 2
- 238000004049 embossing Methods 0.000 description 2
- ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 description 2
- 150000007530 organic bases Chemical class 0.000 description 2
- XQALCMPPZHQMLW-UHFFFAOYSA-N 1,3-diethoxypropan-1-ol Chemical compound CCOCCC(O)OCC XQALCMPPZHQMLW-UHFFFAOYSA-N 0.000 description 1
- QTOMCRXZFDHJOL-UHFFFAOYSA-N 2,2-dimethylpentan-1-ol Chemical compound CCCC(C)(C)CO QTOMCRXZFDHJOL-UHFFFAOYSA-N 0.000 description 1
- JKAPWXKZLYJQJJ-UHFFFAOYSA-N 2,4-dichloro-6-methoxy-1,3,5-triazine Chemical compound COC1=NC(Cl)=NC(Cl)=N1 JKAPWXKZLYJQJJ-UHFFFAOYSA-N 0.000 description 1
- WCASXYBKJHWFMY-NSCUHMNNSA-N 2-Buten-1-ol Chemical compound C\C=C\CO WCASXYBKJHWFMY-NSCUHMNNSA-N 0.000 description 1
- XNWFRZJHXBZDAG-UHFFFAOYSA-N 2-METHOXYETHANOL Chemical compound COCCO XNWFRZJHXBZDAG-UHFFFAOYSA-N 0.000 description 1
- POAOYUHQDCAZBD-UHFFFAOYSA-N 2-butoxyethanol Chemical compound CCCCOCCO POAOYUHQDCAZBD-UHFFFAOYSA-N 0.000 description 1
- SZIFAVKTNFCBPC-UHFFFAOYSA-N 2-chloroethanol Chemical compound OCCCl SZIFAVKTNFCBPC-UHFFFAOYSA-N 0.000 description 1
- ZNQVEEAIQZEUHB-UHFFFAOYSA-N 2-ethoxyethanol Chemical compound CCOCCO ZNQVEEAIQZEUHB-UHFFFAOYSA-N 0.000 description 1
- 229940093475 2-ethoxyethanol Drugs 0.000 description 1
- LNRIEBFNWGMXKP-UHFFFAOYSA-N 2-ethylsulfanylethanol Chemical compound CCSCCO LNRIEBFNWGMXKP-UHFFFAOYSA-N 0.000 description 1
- QPRQEDXDYOZYLA-UHFFFAOYSA-N 2-methylbutan-1-ol Chemical compound CCC(C)CO QPRQEDXDYOZYLA-UHFFFAOYSA-N 0.000 description 1
- NDVWOBYBJYUSMF-UHFFFAOYSA-N 2-methylcyclohexan-1-ol Chemical compound CC1CCCCC1O NDVWOBYBJYUSMF-UHFFFAOYSA-N 0.000 description 1
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 description 1
- YEYKMVJDLWJFOA-UHFFFAOYSA-N 2-propoxyethanol Chemical compound CCCOCCO YEYKMVJDLWJFOA-UHFFFAOYSA-N 0.000 description 1
- LAMUXTNQCICZQX-UHFFFAOYSA-N 3-chloropropan-1-ol Chemical compound OCCCCl LAMUXTNQCICZQX-UHFFFAOYSA-N 0.000 description 1
- XHMWPVBQGARKQM-UHFFFAOYSA-N 3-ethoxy-1-propanol Chemical compound CCOCCCO XHMWPVBQGARKQM-UHFFFAOYSA-N 0.000 description 1
- JSGVZVOGOQILFM-UHFFFAOYSA-N 3-methoxy-1-butanol Chemical compound COC(C)CCO JSGVZVOGOQILFM-UHFFFAOYSA-N 0.000 description 1
- MSHFRERJPWKJFX-UHFFFAOYSA-N 4-Methoxybenzyl alcohol Chemical compound COC1=CC=C(CO)C=C1 MSHFRERJPWKJFX-UHFFFAOYSA-N 0.000 description 1
- 240000006829 Ficus sundaica Species 0.000 description 1
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 description 1
- 229910000318 alkali metal phosphate Inorganic materials 0.000 description 1
- HOPRXXXSABQWAV-UHFFFAOYSA-N anhydrous collidine Natural products CC1=CC=NC(C)=C1C HOPRXXXSABQWAV-UHFFFAOYSA-N 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- UTBIMNXEDGNJFE-UHFFFAOYSA-N collidine Natural products CC1=CC=C(C)C(C)=N1 UTBIMNXEDGNJFE-UHFFFAOYSA-N 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- HPXRVTGHNJAIIH-UHFFFAOYSA-N cyclohexanol Chemical compound OC1CCCCC1 HPXRVTGHNJAIIH-UHFFFAOYSA-N 0.000 description 1
- VSSAZBXXNIABDN-UHFFFAOYSA-N cyclohexylmethanol Chemical compound OCC1CCCCC1 VSSAZBXXNIABDN-UHFFFAOYSA-N 0.000 description 1
- XCIXKGXIYUWCLL-UHFFFAOYSA-N cyclopentanol Chemical compound OC1CCCC1 XCIXKGXIYUWCLL-UHFFFAOYSA-N 0.000 description 1
- XXJWXESWEXIICW-UHFFFAOYSA-N diethylene glycol monoethyl ether Chemical compound CCOCCOCCO XXJWXESWEXIICW-UHFFFAOYSA-N 0.000 description 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 1
- -1 ether radical Chemical class 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 125000005843 halogen group Chemical group 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- PHTQWCKDNZKARW-UHFFFAOYSA-N isoamylol Chemical compound CC(C)CCO PHTQWCKDNZKARW-UHFFFAOYSA-N 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 239000012074 organic phase Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- AQIXEPGDORPWBJ-UHFFFAOYSA-N pentan-3-ol Chemical compound CCC(O)CC AQIXEPGDORPWBJ-UHFFFAOYSA-N 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 229960005323 phenoxyethanol Drugs 0.000 description 1
- WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 description 1
- TVDSBUOJIPERQY-UHFFFAOYSA-N prop-2-yn-1-ol Chemical compound OCC#C TVDSBUOJIPERQY-UHFFFAOYSA-N 0.000 description 1
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 235000020095 red wine Nutrition 0.000 description 1
- 230000003716 rejuvenation Effects 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- GFYHSKONPJXCDE-UHFFFAOYSA-N sym-collidine Natural products CC1=CN=C(C)C(C)=C1 GFYHSKONPJXCDE-UHFFFAOYSA-N 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/26—Nozzle-type reactors, i.e. the distribution of the initial reactants within the reactor is effected by their introduction or injection through nozzles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
- B01J10/02—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor of the thin-film type
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2850339A DE2850339C2 (de) | 1978-11-20 | 1978-11-20 | Verfahren zur Herstellung von 2-Alkoxy-4,6-dichlor-s-triazinen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DD147103A5 true DD147103A5 (de) | 1981-03-18 |
Family
ID=6055173
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DD79216460A DD147103A5 (de) | 1978-11-20 | 1979-10-25 | Verfahren zur herstellung von 2-alkoxy-4,6-dichlor-s-triazinen |
Country Status (22)
| Country | Link |
|---|---|
| US (1) | US4271299A (cs) |
| JP (1) | JPS5573665A (cs) |
| AT (1) | AT368139B (cs) |
| BE (1) | BE880142A (cs) |
| BR (1) | BR7907284A (cs) |
| CA (1) | CA1101861A (cs) |
| CH (1) | CH642640A5 (cs) |
| CS (1) | CS253554B2 (cs) |
| DD (1) | DD147103A5 (cs) |
| DE (1) | DE2850339C2 (cs) |
| ES (1) | ES483876A1 (cs) |
| FR (1) | FR2441619A1 (cs) |
| GB (1) | GB2036736B (cs) |
| HU (1) | HU184070B (cs) |
| IL (1) | IL58606A (cs) |
| IN (1) | IN153839B (cs) |
| IT (1) | IT1119156B (cs) |
| NL (1) | NL7908438A (cs) |
| RO (1) | RO79414A (cs) |
| SE (1) | SE447252B (cs) |
| YU (1) | YU172279A (cs) |
| ZA (1) | ZA796282B (cs) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5229513A (en) * | 1992-09-17 | 1993-07-20 | General Electric Company | Method for preparing substituted dichlorotriazines |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL208063A (cs) * | 1956-06-15 | |||
| US3198797A (en) * | 1960-04-12 | 1965-08-03 | Geigy Chem Corp | 2, 4-dichloro-6-dialkylhydroxy-anilino-1, 3, 5-triazines |
| FR1534235A (fr) * | 1966-08-11 | 1968-07-26 | Bayer Ag | Procédé de préparation d'une suspension aqueuse neutre de chlorure de cyanuryle exempte de solvants |
| DD111378A5 (cs) * | 1973-06-27 | 1975-02-12 | ||
| RO70804A (ro) * | 1974-11-20 | 1980-08-15 | Deutsche Gold-Und Silber-Scheideanstalt Vormals Roessler,De | Procedeu si dispozitiv pentru prepararea unor solutii sau suspensii de clorura de cianuril |
-
1978
- 1978-11-20 DE DE2850339A patent/DE2850339C2/de not_active Expired
-
1979
- 1979-07-16 YU YU01722/79A patent/YU172279A/xx unknown
- 1979-08-14 IT IT68672/79A patent/IT1119156B/it active
- 1979-08-29 IN IN90/CAL/79A patent/IN153839B/en unknown
- 1979-09-04 ES ES483876A patent/ES483876A1/es not_active Expired
- 1979-10-25 DD DD79216460A patent/DD147103A5/de unknown
- 1979-11-01 IL IL58606A patent/IL58606A/xx unknown
- 1979-11-06 CS CS797566A patent/CS253554B2/cs unknown
- 1979-11-09 BR BR7907284A patent/BR7907284A/pt unknown
- 1979-11-13 GB GB7939170A patent/GB2036736B/en not_active Expired
- 1979-11-15 US US06/094,479 patent/US4271299A/en not_active Expired - Lifetime
- 1979-11-19 SE SE7909570A patent/SE447252B/sv not_active IP Right Cessation
- 1979-11-19 BE BE6/47016A patent/BE880142A/fr not_active IP Right Cessation
- 1979-11-19 CH CH1030579A patent/CH642640A5/de not_active IP Right Cessation
- 1979-11-19 CA CA340,148A patent/CA1101861A/en not_active Expired
- 1979-11-19 AT AT0735379A patent/AT368139B/de not_active IP Right Cessation
- 1979-11-19 NL NL7908438A patent/NL7908438A/nl not_active Application Discontinuation
- 1979-11-19 HU HU79DE1025A patent/HU184070B/hu unknown
- 1979-11-20 FR FR7928610A patent/FR2441619A1/fr active Granted
- 1979-11-20 ZA ZA00796282A patent/ZA796282B/xx unknown
- 1979-11-20 RO RO7999287A patent/RO79414A/ro unknown
- 1979-11-20 JP JP14963279A patent/JPS5573665A/ja active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| SE7909570L (sv) | 1980-05-21 |
| ATA735379A (de) | 1982-01-15 |
| IN153839B (cs) | 1984-08-18 |
| ES483876A1 (es) | 1980-04-16 |
| GB2036736A (en) | 1980-07-02 |
| YU172279A (en) | 1983-12-31 |
| CA1101861A (en) | 1981-05-26 |
| IT7968672A0 (it) | 1979-08-14 |
| HU184070B (en) | 1984-06-28 |
| SE447252B (sv) | 1986-11-03 |
| ZA796282B (en) | 1980-11-26 |
| US4271299A (en) | 1981-06-02 |
| RO79414A (ro) | 1982-06-25 |
| CS253554B2 (en) | 1987-11-12 |
| NL7908438A (nl) | 1980-05-22 |
| IT1119156B (it) | 1986-03-03 |
| DE2850339C2 (de) | 1981-02-26 |
| FR2441619A1 (fr) | 1980-06-13 |
| BE880142A (fr) | 1980-05-19 |
| FR2441619B1 (cs) | 1983-06-24 |
| GB2036736B (en) | 1983-03-09 |
| JPS5573665A (en) | 1980-06-03 |
| DE2850339B1 (de) | 1980-06-12 |
| IL58606A0 (en) | 1980-02-29 |
| CH642640A5 (de) | 1984-04-30 |
| BR7907284A (pt) | 1980-07-15 |
| IL58606A (en) | 1984-02-29 |
| AT368139B (de) | 1982-09-10 |
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