CN1204048C - 生产金属氧化物和有机金属氧化物组合物的方法 - Google Patents
生产金属氧化物和有机金属氧化物组合物的方法 Download PDFInfo
- Publication number
- CN1204048C CN1204048C CNB988055031A CN98805503A CN1204048C CN 1204048 C CN1204048 C CN 1204048C CN B988055031 A CNB988055031 A CN B988055031A CN 98805503 A CN98805503 A CN 98805503A CN 1204048 C CN1204048 C CN 1204048C
- Authority
- CN
- China
- Prior art keywords
- organometallic
- metal oxide
- oxide
- sample
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/16—Preparation of silica xerogels
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
- C01B13/14—Methods for preparing oxides or hydroxides in general
- C01B13/32—Methods for preparing oxides or hydroxides in general by oxidation or hydrolysis of elements or compounds in the liquid or solid state or in non-aqueous solution, e.g. sol-gel process
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/16—Preparation of silica xerogels
- C01B33/163—Preparation of silica xerogels by hydrolysis of organosilicon compounds, e.g. ethyl orthosilicate
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G1/00—Methods of preparing compounds of metals not covered by subclasses C01B, C01C, C01D, or C01F, in general
- C01G1/02—Oxides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/10—Solid density
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/11—Powder tap density
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/20—Powder free flowing behaviour
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Oxygen, Ozone, And Oxides In General (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/831,564 | 1997-04-09 | ||
| US08/831,564 US6071486A (en) | 1997-04-09 | 1997-04-09 | Process for producing metal oxide and organo-metal oxide compositions |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1258262A CN1258262A (zh) | 2000-06-28 |
| CN1204048C true CN1204048C (zh) | 2005-06-01 |
Family
ID=25259349
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB988055031A Expired - Fee Related CN1204048C (zh) | 1997-04-09 | 1998-04-09 | 生产金属氧化物和有机金属氧化物组合物的方法 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US6071486A (enExample) |
| EP (1) | EP0973691B1 (enExample) |
| JP (1) | JP2001518873A (enExample) |
| KR (1) | KR100529979B1 (enExample) |
| CN (1) | CN1204048C (enExample) |
| AU (1) | AU6894898A (enExample) |
| BR (1) | BR9808518A (enExample) |
| CA (1) | CA2286149A1 (enExample) |
| DE (1) | DE69810094T2 (enExample) |
| WO (1) | WO1998045210A1 (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101698583B (zh) * | 2009-11-13 | 2012-08-22 | 航天特种材料及工艺技术研究所 | 一种多组元气凝胶复合材料及其制备方法 |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1999036480A1 (en) * | 1998-01-15 | 1999-07-22 | Cabot Corporation | Method of preparing treated silica |
| US6159540A (en) * | 1998-01-15 | 2000-12-12 | Cabot Corporation | Polyfunctional organosilane treatment of silica |
| DE69915590T2 (de) * | 1998-01-15 | 2004-08-05 | Cabot Corp., Boston | Verfahren zur herstellung von organisch modifizierter kieselgel |
| US6174926B1 (en) | 1999-01-13 | 2001-01-16 | Cabot Corporation | Method of preparing organically modified silica |
| US6444609B1 (en) * | 2000-08-15 | 2002-09-03 | Aer Energy Resources, Inc. | Manganese-based oxygen reduction catalyst, metal-air electrode including said catalyst and methods for making the same |
| USH2121H1 (en) * | 2000-10-13 | 2005-08-02 | The United States Of America As Represented By The Secretary Of The Navy | High surface area, nanoscale, mesoporous manganese oxides with controlled solid-pore architectures and method for production thereof |
| AU2003233738A1 (en) * | 2002-06-05 | 2003-12-22 | University Technologies International Inc. | Oxygen reduction catalyst |
| US7157073B2 (en) | 2003-05-02 | 2007-01-02 | Reading Alloys, Inc. | Production of high-purity niobium monoxide and capacitor production therefrom |
| JP4773355B2 (ja) | 2003-05-19 | 2011-09-14 | キャボット コーポレイション | ニオブ酸化物及び酸素が低減したニオブ酸化物の製造方法 |
| US7771877B2 (en) | 2003-12-31 | 2010-08-10 | Lg Chem, Ltd. | Electrode active material powder with size dependent composition and method to prepare the same |
| US20060194910A1 (en) * | 2004-05-19 | 2006-08-31 | Nobuo Miyatake | Stabilization of polymers with zinc oxide nanoparticles |
| US7482382B2 (en) * | 2004-05-19 | 2009-01-27 | The Texas A&M University System | Process for preparing nano-sized metal oxide particles |
| US20070004840A1 (en) * | 2004-05-19 | 2007-01-04 | Texas A&M University | Zinc oxide polymer nanocomposites and methods of producing zinc oxide polymer nanocomposites |
| US8344054B2 (en) * | 2007-07-24 | 2013-01-01 | The Texas A & M University System | Polymer nanocomposites including dispersed nanoparticles and inorganic nanoplatelets |
| DE102008046444A1 (de) | 2008-09-09 | 2010-03-11 | Evonik Röhm Gmbh | Fassadenplatte, System und Verfahren zur Energiegewinnung |
| WO2011020671A1 (de) | 2009-08-20 | 2011-02-24 | Evonik Röhm Gmbh | Dämmplatte aus kunststoff, system und verfahren zur wärmedämmung |
| US10822807B2 (en) | 2019-02-18 | 2020-11-03 | Royal Building Products (Usa) Inc. | Assembly for improved insulation |
| WO2025071811A1 (en) | 2023-09-29 | 2025-04-03 | Dow Global Technologies Llc | Silicone – acrylic binder for thermal insulation coatings to provide resistance to corrosion under insulation |
| WO2025071812A1 (en) | 2023-09-29 | 2025-04-03 | Dow Global Technologies Llc | Silicone - acrylic binder for liquid applied thermal insulation coating compositions to resist corrosion under insulation |
Family Cites Families (42)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2269059A (en) * | 1938-05-14 | 1942-01-06 | Corning Glass Works | Method of preparing finely comminuted oxides |
| US2765242A (en) * | 1952-02-29 | 1956-10-02 | Du Pont | Process of making reinforced silica gel and esterified silica gel |
| US2739075A (en) * | 1952-03-06 | 1956-03-20 | Du Pont | Product and process |
| US2832794A (en) * | 1952-11-05 | 1958-04-29 | Allied Chem & Dye Corp | Hydrolysis of organosilanes |
| US2901460A (en) * | 1956-02-07 | 1959-08-25 | Gen Electric | Halosilane hydrolysis with tetrahydrofuran and water |
| FR1568817A (enExample) * | 1967-11-30 | 1969-05-30 | ||
| US3652214A (en) * | 1968-08-06 | 1972-03-28 | Nat Petro Chemicals Co Inc | Preparation of silica gels |
| DE2313073C2 (de) * | 1973-03-16 | 1984-11-29 | Istvan Prof. Dr. 6600 Saarbruecken Halasz | Verfahren zur chemischen Modifizierung von Oberflächen anorganischer Festkörper und deren Verwendung |
| DE2414478C3 (de) * | 1974-03-26 | 1978-07-13 | Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt | Aerogelartige strukturierte Kieselsäure und Verfahren zu ihrer Herstellung |
| JPS6144711A (ja) * | 1984-08-03 | 1986-03-04 | Agency Of Ind Science & Technol | 微粒状シリカの製法 |
| DE3429671A1 (de) * | 1984-08-11 | 1986-02-20 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von aerogelen |
| JPS6168314A (ja) * | 1984-09-07 | 1986-04-08 | Agency Of Ind Science & Technol | 多孔性シリカ、アルミナ、チタニアおよびジルコニアの製造方法 |
| US4561872A (en) * | 1984-10-22 | 1985-12-31 | Corning Glass Works | Method for making glass or ceramic article |
| FR2585973A1 (fr) * | 1985-08-06 | 1987-02-13 | Centre Nat Rech Scient | Gel monolithique et poudre d'oxydes d'elements de transition, procede de fabrication du gel et procede de preparation de couches minces de ces oxydes |
| JPS6252119A (ja) * | 1985-08-29 | 1987-03-06 | Tokuyama Soda Co Ltd | シリカ粒子の製造方法 |
| US4810415A (en) * | 1985-09-24 | 1989-03-07 | Dresser Industries, Inc. | Process for manufacturing ultra pure silica and resulting encapsulated products |
| DE3616133A1 (de) * | 1985-09-25 | 1987-11-19 | Merck Patent Gmbh | Kugelfoermige sio(pfeil abwaerts)2(pfeil abwaerts)-partikel |
| JPS62171914A (ja) * | 1986-01-25 | 1987-07-28 | Agency Of Ind Science & Technol | 微小球シリカの製造方法 |
| JPS6374911A (ja) * | 1986-09-19 | 1988-04-05 | Shin Etsu Chem Co Ltd | 微細球状シリカの製造法 |
| EP0372251B1 (de) * | 1988-11-22 | 1992-03-11 | Degussa Aktiengesellschaft | Verfahren zur Herstellung von Kieselsäuren |
| US5158758A (en) * | 1989-04-24 | 1992-10-27 | International Minerals & Chemical Corp. | Production of silica having high specific surface area |
| US5017540A (en) * | 1989-09-15 | 1991-05-21 | Sandoval Junior E | Silicon hydride surface intermediates for chemical separations apparatus |
| US4983369A (en) * | 1989-11-22 | 1991-01-08 | Allied-Signal Inc. | Process for forming highly uniform silica spheres |
| IT1240673B (it) * | 1990-04-24 | 1993-12-17 | Tenav | Microsfere di aerogels di ossidi inorganici a stretta distribuzione dei diametri dei pori e metodo per la loro preparazione |
| US5409683A (en) * | 1990-08-23 | 1995-04-25 | Regents Of The University Of California | Method for producing metal oxide aerogels |
| EP0497966B1 (en) * | 1990-08-23 | 1997-10-29 | THE REGENTS OF THE UNIVERSITY OF CALIFORNIA as represented by Lawrence Livermore National Laboratory | A METHOD FOR PRODUCING METAL OXIDE AEROGELS HAVING DENSITIES LESS THAN 0.02 g/cm?3 |
| US5106604A (en) * | 1991-03-12 | 1992-04-21 | Pradyot Agaskar | Use of metal salts in the synthesis of oligomeric hydrogensilsesquioxanes via hydrolysis/condensation reactions |
| US5206189A (en) * | 1991-10-25 | 1993-04-27 | Instituto Guido Donegani S.P.A. | Sol-gel method for the preparation of monolithic multicomponent oxide glasses |
| EP0585456B1 (en) * | 1992-02-18 | 1997-05-07 | Matsushita Electric Works Ltd | Process for producing hydrophobic aerogel |
| US5565142A (en) * | 1992-04-01 | 1996-10-15 | Deshpande; Ravindra | Preparation of high porosity xerogels by chemical surface modification. |
| CA2135875A1 (en) * | 1992-05-20 | 1993-11-25 | Kenneth G. Sharp | Process for making inorganic gels |
| US5395805A (en) * | 1993-03-25 | 1995-03-07 | Regents Of The University Of California | Method for making monolithic metal oxide aerogels |
| US5420168A (en) * | 1993-04-01 | 1995-05-30 | The Regents Of The University Of California | Method of low pressure and/or evaporative drying of aerogel |
| US5376449A (en) * | 1993-07-09 | 1994-12-27 | Martin Marietta Energy Systems, Inc. | Silica powders for powder evacuated thermal insulating panel and method |
| WO1995017347A1 (en) * | 1993-12-23 | 1995-06-29 | Ppg Industries, Inc. | Silica aerogel produced under subcritical conditions |
| US5470802A (en) * | 1994-05-20 | 1995-11-28 | Texas Instruments Incorporated | Method of making a semiconductor device using a low dielectric constant material |
| DE4422912A1 (de) * | 1994-06-30 | 1996-01-11 | Hoechst Ag | Xerogele, Verfahren zu ihrer Herstellung, sowie ihre Verwendung |
| US5473826A (en) * | 1994-08-19 | 1995-12-12 | Yazaki Corporation | Process for drying sol-gel derived porous bodies at elevated subcritical temperatures and pressures |
| DE4437424A1 (de) * | 1994-10-20 | 1996-04-25 | Hoechst Ag | Aerogelhaltige Zusammensetzung, Verfahren zu ihrer Herstellung sowie ihre Verwendung |
| US5807494A (en) * | 1994-12-15 | 1998-09-15 | Boes; Ralph Ulrich | Gel compositions comprising silica and functionalized carbon products |
| US5876686A (en) * | 1995-06-28 | 1999-03-02 | E. I. Du Pont De Nemours And Company | Process for making inorganic oxide gels in fluorocarbon solvents |
| WO1997022652A1 (en) * | 1995-12-20 | 1997-06-26 | E.I. Du Pont De Nemours And Company | Rapid process for making silica gel and silicate polymer and low density gels made thereby |
-
1997
- 1997-04-09 US US08/831,564 patent/US6071486A/en not_active Expired - Fee Related
-
1998
- 1998-04-09 AU AU68948/98A patent/AU6894898A/en not_active Abandoned
- 1998-04-09 DE DE69810094T patent/DE69810094T2/de not_active Expired - Lifetime
- 1998-04-09 CA CA002286149A patent/CA2286149A1/en not_active Abandoned
- 1998-04-09 JP JP54312398A patent/JP2001518873A/ja not_active Ceased
- 1998-04-09 WO PCT/US1998/007109 patent/WO1998045210A1/en not_active Ceased
- 1998-04-09 EP EP98914643A patent/EP0973691B1/en not_active Expired - Lifetime
- 1998-04-09 KR KR10-1999-7009294A patent/KR100529979B1/ko not_active Expired - Fee Related
- 1998-04-09 CN CNB988055031A patent/CN1204048C/zh not_active Expired - Fee Related
- 1998-04-09 BR BR9808518-2A patent/BR9808518A/pt active Search and Examination
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101698583B (zh) * | 2009-11-13 | 2012-08-22 | 航天特种材料及工艺技术研究所 | 一种多组元气凝胶复合材料及其制备方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| WO1998045210A1 (en) | 1998-10-15 |
| CN1258262A (zh) | 2000-06-28 |
| US6071486A (en) | 2000-06-06 |
| AU6894898A (en) | 1998-10-30 |
| KR20010006214A (ko) | 2001-01-26 |
| DE69810094D1 (de) | 2003-01-23 |
| CA2286149A1 (en) | 1998-10-15 |
| BR9808518A (pt) | 2000-10-31 |
| JP2001518873A (ja) | 2001-10-16 |
| EP0973691B1 (en) | 2002-12-11 |
| DE69810094T2 (de) | 2003-09-25 |
| KR100529979B1 (ko) | 2005-11-22 |
| EP0973691A1 (en) | 2000-01-26 |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20050601 Termination date: 20110409 |