CN1183180C - 具有高伯羟基含量的长链聚醚多元醇 - Google Patents

具有高伯羟基含量的长链聚醚多元醇 Download PDF

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Publication number
CN1183180C
CN1183180C CNB008067120A CN00806712A CN1183180C CN 1183180 C CN1183180 C CN 1183180C CN B008067120 A CNB008067120 A CN B008067120A CN 00806712 A CN00806712 A CN 00806712A CN 1183180 C CN1183180 C CN 1183180C
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CN
China
Prior art keywords
dmc
weight
polyether polyol
mol
propylene oxide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CNB008067120A
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English (en)
Chinese (zh)
Other versions
CN1348476A (zh
Inventor
J
J·霍夫曼
P·古普塔
ϣ
M·迪特里希
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Covestro Deutschland AG
Original Assignee
Bayer AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
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Publication of CN1348476A publication Critical patent/CN1348476A/zh
Application granted granted Critical
Publication of CN1183180C publication Critical patent/CN1183180C/zh
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/04—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers only
    • C08G65/06—Cyclic ethers having no atoms other than carbon and hydrogen outside the ring
    • C08G65/08—Saturated oxiranes
    • C08G65/10—Saturated oxiranes characterised by the catalysts used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/2663—Metal cyanide catalysts, i.e. DMC's
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/4833—Polyethers containing oxyethylene units
    • C08G18/4837—Polyethers containing oxyethylene units and other oxyalkylene units
    • C08G18/4841—Polyethers containing oxyethylene units and other oxyalkylene units containing oxyethylene end groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/4866—Polyethers having a low unsaturation value

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Toxicology (AREA)
  • Polyethers (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Cephalosporin Compounds (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)
CNB008067120A 1999-04-24 2000-04-11 具有高伯羟基含量的长链聚醚多元醇 Expired - Lifetime CN1183180C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19918727.4 1999-04-24
DE19918727A DE19918727A1 (de) 1999-04-24 1999-04-24 Langkettige Polyetherpolyole mit hohem Anteil primärer OH-Gruppen

Publications (2)

Publication Number Publication Date
CN1348476A CN1348476A (zh) 2002-05-08
CN1183180C true CN1183180C (zh) 2005-01-05

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CNB008067120A Expired - Lifetime CN1183180C (zh) 1999-04-24 2000-04-11 具有高伯羟基含量的长链聚醚多元醇

Country Status (20)

Country Link
US (1) US6617419B1 (enExample)
EP (1) EP1173498B1 (enExample)
JP (1) JP2002543228A (enExample)
KR (1) KR100610285B1 (enExample)
CN (1) CN1183180C (enExample)
AT (1) ATE273339T1 (enExample)
AU (1) AU3819600A (enExample)
BR (1) BR0010002B1 (enExample)
CA (1) CA2367670C (enExample)
CZ (1) CZ296406B6 (enExample)
DE (2) DE19918727A1 (enExample)
ES (1) ES2226804T3 (enExample)
HK (1) HK1046147B (enExample)
HU (1) HU228388B1 (enExample)
ID (1) ID30542A (enExample)
MX (1) MXPA01010737A (enExample)
PL (1) PL199860B1 (enExample)
PT (1) PT1173498E (enExample)
RU (1) RU2242485C2 (enExample)
WO (1) WO2000064963A1 (enExample)

Families Citing this family (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19928156A1 (de) * 1999-06-19 2000-12-28 Bayer Ag Aus Polyetherpolyolen hergestellte Polyurethan-Weichschäume
CN1310998C (zh) * 2002-01-22 2007-04-18 旭硝子株式会社 聚醚类的连续制备方法
JP4273876B2 (ja) * 2003-08-25 2009-06-03 旭硝子株式会社 ポリエーテルモノオールまたはポリエーテルポリオールおよびその製造方法
ES2743249T3 (es) * 2003-10-10 2020-02-18 Shell Int Research Procedimiento para la preparación de un poliéter poliol
JP4899508B2 (ja) * 2006-02-03 2012-03-21 旭硝子株式会社 ポリエーテルポリオールの製造方法
CN100588669C (zh) * 2006-11-28 2010-02-10 王伟松 烯丙醇无规聚醚的制备方法
DE102007002555A1 (de) * 2007-01-17 2008-07-24 Bayer Materialscience Ag Doppelmetallcyanid-Katalysatoren für die Herstellung von Polyetherpolyolen
DE102007057147A1 (de) 2007-11-28 2009-06-04 Evonik Goldschmidt Gmbh Verfahren zur Alkoxylierung mit DMC-Katalysatoren im Schlaufenreaktor mit Strahlsauger
EP2241584B1 (en) * 2008-01-25 2012-03-21 Kaneka Corporation Process for producing polyalkylene oxide
TW201120076A (en) * 2009-10-05 2011-06-16 Asahi Glass Co Ltd Method for producing soft polyurethane foam and sheet
US20110230581A1 (en) 2010-03-17 2011-09-22 Bayer Materialscience Llc Process for the production of polyether polyols with a high ethylene oxide content
KR20130094688A (ko) * 2010-04-30 2013-08-26 아사히 가라스 가부시키가이샤 폴리옥시알킬렌폴리올, 폴리머 분산 폴리올, 및 연질 폴리우레탄폼, 그리고 이들의 제조 방법
JP5648797B2 (ja) * 2010-11-22 2015-01-07 旭硝子株式会社 ポリエーテルヒドロキシ化合物の製造方法
EP2530101A1 (de) * 2011-06-01 2012-12-05 Bayer MaterialScience AG Verfahren zur Herstellung von Polyetherpolyolen
CN102417594A (zh) * 2011-10-14 2012-04-18 滨州市华茂工贸有限公司 缩合醇无规聚醚的配方、生产工艺及应用
WO2013092501A1 (de) 2011-12-20 2013-06-27 Bayer Intellectual Property Gmbh Hydroxy-aminopolymere und verfahren zu deren herstellung
CN104169327A (zh) * 2012-04-18 2014-11-26 旭硝子株式会社 聚醚类的制造方法
US9051412B2 (en) * 2013-03-14 2015-06-09 Bayer Materialscience Llc Base-catalyzed, long chain, active polyethers from short chain DMC-catalyzed starters
JPWO2016072514A1 (ja) * 2014-11-07 2017-08-17 出光興産株式会社 ポリアルキレングリコールの製造方法、粘度指数向上剤、潤滑油組成物及び潤滑油組成物の製造方法
AR104981A1 (es) * 2015-06-20 2017-08-30 Dow Global Technologies Llc Proceso continuo para producir polioles de poliéter que tienen un elevado contenido de óxido de etileno polimerizado, mediante el uso de un complejo catalizador de cianuro de metal doble y un compuesto metálico de la serie de lantanida o metal del grupo 3 - grupo 15, magnesio
JP7266025B2 (ja) * 2017-09-15 2023-04-27 ダウ グローバル テクノロジーズ エルエルシー ポリエーテルポリオールを作製するための連続プロセス
US20210002423A1 (en) 2017-11-06 2021-01-07 Shell Oil Company Process for preparing a polyether polyol with a high ethylene oxide content
JP6799788B1 (ja) * 2019-01-21 2020-12-16 日油株式会社 アルキレンオキシド誘導体、消泡剤、潤滑剤、化粧料用基材およびそれを含む化粧料、毛髪用洗浄剤組成物および身体用洗浄剤組成物
JP7202524B2 (ja) * 2019-01-21 2023-01-12 日油株式会社 アルキレンオキシド誘導体、潤滑剤、消泡剤、化粧品用基材およびそれを含む化粧料
CN111303403B (zh) * 2020-04-13 2022-06-14 山东蓝星东大有限公司 端多羟基聚醚多元醇制备方法
US11753516B2 (en) 2021-10-08 2023-09-12 Covestro Llc HFO-containing compositions and methods of producing foams
EP4279534A1 (en) 2022-05-20 2023-11-22 PCC ROKITA Spolka Akcyjna A method for producing low unsaturation level oxyalkylates, an oxyalkylate, a use thereof and a polyurethane foam
PL442356A1 (pl) * 2022-09-26 2024-04-02 Pcc Rokita Spółka Akcyjna Poliol polieterowy, sposób jego wytwarzania i jego zastosowanie oraz elastyczna pianka poliuretanowa

Family Cites Families (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1063525A (en) 1963-02-14 1967-03-30 Gen Tire & Rubber Co Organic cyclic oxide polymers, their preparation and tires prepared therefrom
US3829505A (en) 1970-02-24 1974-08-13 Gen Tire & Rubber Co Polyethers and method for making the same
US3941849A (en) 1972-07-07 1976-03-02 The General Tire & Rubber Company Polyethers and method for making the same
CA1155871A (en) 1980-10-16 1983-10-25 Gencorp Inc. Method for treating polypropylene ether and poly-1,2- butylene ether polyols
US5103062A (en) * 1987-04-10 1992-04-07 Texaco Inc. Modified normally liquid, water-soluble polyoxyalkylene polyamines
US4942214A (en) * 1988-06-29 1990-07-17 W. L. Gore & Assoc. Inc. Flexible breathable polyurethane coatings and films, and the prepolymers from which they are made
JPH02191628A (ja) 1989-01-19 1990-07-27 Dai Ichi Kogyo Seiyaku Co Ltd ポリエーテルポリオール
JP2999789B2 (ja) * 1990-02-23 2000-01-17 旭硝子株式会社 ポリエーテル類の製造方法
US5158922A (en) 1992-02-04 1992-10-27 Arco Chemical Technology, L.P. Process for preparing metal cyanide complex catalyst
JP3299803B2 (ja) * 1993-02-26 2002-07-08 旭硝子株式会社 ポリエーテルポリオールの製造方法
US5482908A (en) 1994-09-08 1996-01-09 Arco Chemical Technology, L.P. Highly active double metal cyanide catalysts
US5563221A (en) 1995-06-21 1996-10-08 Arco Chemical Technology, L.P. Process for making ethylene oxide-capped polyols from double metal cyanide-catalyzed polyols
US5545601A (en) 1995-08-22 1996-08-13 Arco Chemical Technology, L.P. Polyether-containing double metal cyanide catalysts
US5700847A (en) 1995-12-04 1997-12-23 Arco Chemical Technology, L.P. Molded polyurethane foam with enhanced physical properties
US5668191A (en) * 1995-12-21 1997-09-16 Arco Chemical Technology, L.P. One-shot cold molded flexible polyurethane foam from low primary hydroxyl polyols and process for the preparation thereof
US5605939A (en) * 1996-01-26 1997-02-25 Arco Chemical Technology, L.P. Poly(oxypropylene/oxyethylene) random polyols useful in preparing flexible high resilience foam with reduced tendencies toward shrinkage and foam prepared therewith
US5627120A (en) 1996-04-19 1997-05-06 Arco Chemical Technology, L.P. Highly active double metal cyanide catalysts
US5714428A (en) 1996-10-16 1998-02-03 Arco Chemical Technology, L.P. Double metal cyanide catalysts containing functionalized polymers
RU2115667C1 (ru) * 1997-04-22 1998-07-20 Научно-исследовательский институт по нефтепромысловой химии Продукт последовательного присоединения окиси этилена и окиси пропилена к высшему жирному спирту и состав для предотвращения асфальтено-смолопарафиновых отложений
WO1999019063A1 (de) 1997-10-13 1999-04-22 Bayer Aktiengesellschaft Kristalline doppelmetallcyanid-katalysatoren für die herstellung von polyetherpolyolen
DE19810269A1 (de) 1998-03-10 2000-05-11 Bayer Ag Verbesserte Doppelmetallcyanid-Katalysatoren für die Herstellung von Polyetherpolyolen
US6008263A (en) 1998-04-03 1999-12-28 Lyondell Chemical Worldwide, Inc. Molded and slab polyurethane foam prepared from double metal cyanide complex-catalyzed polyoxyalkylene polyols and polyols suitable for the preparation thereof
US6066683A (en) 1998-04-03 2000-05-23 Lyondell Chemical Worldwide, Inc. Molded and slab polyurethane foam prepared from double metal cyanide complex-catalyzed polyoxyalkylene polyols and polyols suitable for the preparation thereof

Also Published As

Publication number Publication date
PL351384A1 (en) 2003-04-07
EP1173498B1 (de) 2004-08-11
PL199860B1 (pl) 2008-11-28
US6617419B1 (en) 2003-09-09
PT1173498E (pt) 2005-01-31
ID30542A (id) 2001-12-20
WO2000064963A1 (de) 2000-11-02
RU2242485C2 (ru) 2004-12-20
CZ20013761A3 (cs) 2002-04-17
CA2367670A1 (en) 2000-11-02
KR20010110796A (ko) 2001-12-13
DE50007388D1 (de) 2004-09-16
CZ296406B6 (cs) 2006-03-15
EP1173498A1 (de) 2002-01-23
CN1348476A (zh) 2002-05-08
ATE273339T1 (de) 2004-08-15
DE19918727A1 (de) 2000-10-26
HU228388B1 (en) 2013-03-28
ES2226804T3 (es) 2005-04-01
BR0010002A (pt) 2002-01-08
AU3819600A (en) 2000-11-10
CA2367670C (en) 2008-10-07
HK1046147A1 (en) 2002-12-27
BR0010002B1 (pt) 2010-06-15
MXPA01010737A (es) 2002-06-04
KR100610285B1 (ko) 2006-08-09
HUP0200782A3 (en) 2004-03-29
JP2002543228A (ja) 2002-12-17
HUP0200782A2 (en) 2002-06-29
HK1046147B (zh) 2005-08-19

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Effective date of registration: 20160614

Address after: Leverkusen, Germany

Patentee after: BAYER MATERIALSCIENCE AG

Address before: Germany Leverkusen

Patentee before: Bayer Aktiengesellschaft

CX01 Expiry of patent term

Granted publication date: 20050105

CX01 Expiry of patent term