CN115404548B - 化合物含氟钛碘酸盐和含氟钛碘酸盐非线性光学晶体及制备方法和用途 - Google Patents
化合物含氟钛碘酸盐和含氟钛碘酸盐非线性光学晶体及制备方法和用途 Download PDFInfo
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- CN115404548B CN115404548B CN202110594441.9A CN202110594441A CN115404548B CN 115404548 B CN115404548 B CN 115404548B CN 202110594441 A CN202110594441 A CN 202110594441A CN 115404548 B CN115404548 B CN 115404548B
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- fluorine
- nonlinear optical
- iodate
- optical crystal
- crystal
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- 229910052731 fluorine Inorganic materials 0.000 title claims abstract description 55
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 title claims abstract description 54
- 239000011737 fluorine Substances 0.000 title claims abstract description 54
- 230000003287 optical effect Effects 0.000 title claims abstract description 54
- 239000013078 crystal Substances 0.000 title claims abstract description 53
- 150000001875 compounds Chemical class 0.000 title claims abstract description 22
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- ICIWUVCWSCSTAQ-UHFFFAOYSA-M iodate Chemical compound [O-]I(=O)=O ICIWUVCWSCSTAQ-UHFFFAOYSA-M 0.000 claims abstract description 23
- 238000001027 hydrothermal synthesis Methods 0.000 claims abstract description 17
- 239000000126 substance Substances 0.000 claims abstract description 10
- 238000000034 method Methods 0.000 claims abstract description 7
- 239000012047 saturated solution Substances 0.000 claims description 18
- 239000000203 mixture Substances 0.000 claims description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- -1 fluorine-titanium iodate Chemical compound 0.000 claims description 14
- 238000002156 mixing Methods 0.000 claims description 14
- 239000008367 deionised water Substances 0.000 claims description 12
- 229910021641 deionized water Inorganic materials 0.000 claims description 12
- 239000004570 mortar (masonry) Substances 0.000 claims description 12
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims description 12
- 239000004810 polytetrafluoroethylene Substances 0.000 claims description 12
- 238000001816 cooling Methods 0.000 claims description 8
- 239000002244 precipitate Substances 0.000 claims description 8
- 238000001914 filtration Methods 0.000 claims description 7
- 238000000227 grinding Methods 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 7
- 238000007789 sealing Methods 0.000 claims description 7
- 239000007864 aqueous solution Substances 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 229910010413 TiO 2 Inorganic materials 0.000 claims description 2
- 229910052760 oxygen Inorganic materials 0.000 claims description 2
- 150000003839 salts Chemical class 0.000 claims description 2
- 239000000243 solution Substances 0.000 claims description 2
- 101100233056 Caenorhabditis elegans ima-2 gene Proteins 0.000 claims 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims 1
- 238000004090 dissolution Methods 0.000 claims 1
- 239000001301 oxygen Substances 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 abstract description 3
- 239000000463 material Substances 0.000 description 8
- 239000011259 mixed solution Substances 0.000 description 8
- XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 description 5
- 229910016036 BaF 2 Inorganic materials 0.000 description 4
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 4
- 238000004891 communication Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 241000251468 Actinopterygii Species 0.000 description 1
- 229910013641 LiNbO 3 Inorganic materials 0.000 description 1
- 230000003321 amplification Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000002050 diffraction method Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000010365 information processing Effects 0.000 description 1
- 125000001905 inorganic group Chemical group 0.000 description 1
- ICIWUVCWSCSTAQ-UHFFFAOYSA-N iodic acid Chemical class OI(=O)=O ICIWUVCWSCSTAQ-UHFFFAOYSA-N 0.000 description 1
- 238000007648 laser printing Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000003199 nucleic acid amplification method Methods 0.000 description 1
- 239000013307 optical fiber Substances 0.000 description 1
- 230000010355 oscillation Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 229910052723 transition metal Inorganic materials 0.000 description 1
- 229910001428 transition metal ion Inorganic materials 0.000 description 1
- 150000003624 transition metals Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/10—Inorganic compounds or compositions
- C30B29/16—Oxides
- C30B29/22—Complex oxides
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B7/00—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions
- C30B7/10—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
-
- G—PHYSICS
- G02—OPTICS
- G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
- G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
- G02F1/35—Non-linear optics
- G02F1/355—Non-linear optics characterised by the materials used
- G02F1/3551—Crystals
Abstract
Description
Claims (8)
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CN115418722A (zh) * | 2022-10-13 | 2022-12-02 | 天津理工大学 | 碱土土金属含氟碘酸盐化合物及其非线性光学晶体及其制备方法及其用途 |
Citations (10)
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CN101831699A (zh) * | 2009-03-13 | 2010-09-15 | 中国科学院福建物质结构研究所 | 一种非线性光学晶体碘酸铌钡 |
CN101986191A (zh) * | 2009-07-29 | 2011-03-16 | 中国科学院福建物质结构研究所 | 一种非线性光学晶体碘酸钒钠 |
CN102995121A (zh) * | 2012-12-12 | 2013-03-27 | 中国科学院福建物质结构研究所 | 非线性光学晶体碘酸钒铊 |
CN103205811A (zh) * | 2012-01-16 | 2013-07-17 | 中国科学院新疆理化技术研究所 | 大尺寸氯氟硼酸钡非线性光学晶体及其制备方法和用途 |
CN106544727A (zh) * | 2015-09-19 | 2017-03-29 | 中国科学院新疆理化技术研究所 | 碘酸氟铋非线性光学晶体及其制备方法和用途 |
CN106757344A (zh) * | 2016-12-29 | 2017-05-31 | 武汉大学 | 两种无机氟碘酸盐晶体及其制备方法和应用 |
CN108004594A (zh) * | 2017-11-28 | 2018-05-08 | 中国科学院新疆理化技术研究所 | 碘酸铯非线性光学晶体及其制备方法和用途 |
CN108070906A (zh) * | 2017-12-15 | 2018-05-25 | 武汉大学 | 非线性光学晶体碘酸锗锂及其制备方法和应用 |
CN108456920A (zh) * | 2018-01-22 | 2018-08-28 | 中国科学院新疆理化技术研究所 | 化合物氟碘酸铯和氟碘酸铯非线性光学晶体及制备方法和用途 |
CN109023502A (zh) * | 2018-09-06 | 2018-12-18 | 中国科学院新疆理化技术研究所 | 化合物氟碘酸铈和氟碘酸铈非线性光学晶体及制备方法和用途 |
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CN101914809B (zh) * | 2010-08-11 | 2014-03-12 | 中国科学院新疆理化技术研究所 | 化合物氯硼酸钾非线性光学晶体及制备方法和用途 |
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Patent Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
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CN101831699A (zh) * | 2009-03-13 | 2010-09-15 | 中国科学院福建物质结构研究所 | 一种非线性光学晶体碘酸铌钡 |
CN101986191A (zh) * | 2009-07-29 | 2011-03-16 | 中国科学院福建物质结构研究所 | 一种非线性光学晶体碘酸钒钠 |
CN103205811A (zh) * | 2012-01-16 | 2013-07-17 | 中国科学院新疆理化技术研究所 | 大尺寸氯氟硼酸钡非线性光学晶体及其制备方法和用途 |
CN102995121A (zh) * | 2012-12-12 | 2013-03-27 | 中国科学院福建物质结构研究所 | 非线性光学晶体碘酸钒铊 |
CN106544727A (zh) * | 2015-09-19 | 2017-03-29 | 中国科学院新疆理化技术研究所 | 碘酸氟铋非线性光学晶体及其制备方法和用途 |
CN106757344A (zh) * | 2016-12-29 | 2017-05-31 | 武汉大学 | 两种无机氟碘酸盐晶体及其制备方法和应用 |
CN108004594A (zh) * | 2017-11-28 | 2018-05-08 | 中国科学院新疆理化技术研究所 | 碘酸铯非线性光学晶体及其制备方法和用途 |
CN108070906A (zh) * | 2017-12-15 | 2018-05-25 | 武汉大学 | 非线性光学晶体碘酸锗锂及其制备方法和应用 |
CN108456920A (zh) * | 2018-01-22 | 2018-08-28 | 中国科学院新疆理化技术研究所 | 化合物氟碘酸铯和氟碘酸铯非线性光学晶体及制备方法和用途 |
CN109023502A (zh) * | 2018-09-06 | 2018-12-18 | 中国科学院新疆理化技术研究所 | 化合物氟碘酸铈和氟碘酸铈非线性光学晶体及制备方法和用途 |
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Address after: 518000, 8th Floor, Building A6, Tianrui Industrial Park, No. 35 Fuyuan 1st Road, Zhancheng Community, Fuhai Street, Bao'an District, Shenzhen, Guangdong Province Patentee after: Shenzhen Qiyang Optical Technology Co.,Ltd. Country or region after: China Address before: 201-203, xushida Mingyuan, No. 263, Xin'an Fourth Road, Wenhui community, Xin'an street, Bao'an District, Shenzhen, Guangdong 518000 Patentee before: Shenzhen Qiyang Optical Technology Co.,Ltd. Country or region before: China |