CN115315298B - 精制方法 - Google Patents

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Publication number
CN115315298B
CN115315298B CN202180023513.2A CN202180023513A CN115315298B CN 115315298 B CN115315298 B CN 115315298B CN 202180023513 A CN202180023513 A CN 202180023513A CN 115315298 B CN115315298 B CN 115315298B
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wavelength
infrared
solvent
crystal form
compound
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Chinese (zh)
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CN115315298A (zh
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藤内谦光
加藤大贵
近藤良夫
山田和成
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NGK Insulators Ltd
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NGK Insulators Ltd
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D277/00—Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings
    • C07D277/02—Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings not condensed with other rings
    • C07D277/20—Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D277/32—Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D277/56—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/005—Selection of auxiliary, e.g. for control of crystallisation nuclei, of crystal growth, of adherence to walls; Arrangements for introduction thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0063—Control or regulation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/38—Separation; Purification; Stabilisation; Use of additives
    • C07C227/40—Separation; Purification
    • C07C227/42—Crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D223/00—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom
    • C07D223/14—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom condensed with carbocyclic rings or ring systems
    • C07D223/18—Dibenzazepines; Hydrogenated dibenzazepines
    • C07D223/22—Dibenz [b, f] azepines; Hydrogenated dibenz [b, f] azepines
    • C07D223/24—Dibenz [b, f] azepines; Hydrogenated dibenz [b, f] azepines with hydrocarbon radicals, substituted by nitrogen atoms, attached to the ring nitrogen atom
    • C07D223/26—Dibenz [b, f] azepines; Hydrogenated dibenz [b, f] azepines with hydrocarbon radicals, substituted by nitrogen atoms, attached to the ring nitrogen atom having a double bond between positions 10 and 11
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/54—Organic compounds
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B7/00—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions
    • C30B7/02—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by evaporation of the solvent
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B7/00—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions
    • C30B7/02—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by evaporation of the solvent
    • C30B7/06—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by evaporation of the solvent using non-aqueous solvents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0018—Evaporation of components of the mixture to be separated
    • B01D9/0031—Evaporation of components of the mixture to be separated by heating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0077—Screening for crystallisation conditions or for crystal forms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/13—Crystalline forms, e.g. polymorphs
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/06—Systems containing only non-condensed rings with a five-membered ring
    • C07C2601/08—Systems containing only non-condensed rings with a five-membered ring the ring being saturated
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D277/00—Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings
    • C07D277/02—Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings not condensed with other rings
    • C07D277/20—Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D277/22—Heterocyclic compounds containing 1,3-thiazole or hydrogenated 1,3-thiazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to ring carbon atoms
    • C07D277/30—Radicals substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
CN202180023513.2A 2020-07-13 2021-07-06 精制方法 Active CN115315298B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JPPCT/JP2020/027266 2020-07-13
JP2020027266 2020-07-13
PCT/JP2021/025388 WO2022014395A1 (ja) 2020-07-13 2021-07-06 精製方法

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CN115315298A CN115315298A (zh) 2022-11-08
CN115315298B true CN115315298B (zh) 2023-09-15

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CN202180023519.XA Active CN115315299B (zh) 2020-07-13 2021-07-06 精制方法

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US (4) US20230167577A1 (enExample)
EP (3) EP4180106A4 (enExample)
JP (5) JP7096956B2 (enExample)
CN (3) CN115315297B (enExample)
WO (3) WO2022014397A1 (enExample)

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KR102485717B1 (ko) * 2017-09-01 2023-01-09 삼성전자주식회사 공기조화기
WO2025062998A1 (ja) * 2023-09-20 2025-03-27 日本碍子株式会社 結晶化装置および結晶化方法
WO2025182996A1 (ja) * 2024-02-28 2025-09-04 日本碍子株式会社 結晶化方法
WO2025181982A1 (ja) * 2024-02-28 2025-09-04 日本碍子株式会社 結晶化方法

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CN1884632A (zh) * 2006-05-23 2006-12-27 青岛大学 溶液法晶体快速生长装置
CN102267957A (zh) * 2011-08-24 2011-12-07 山东齐都药业有限公司 非布司他a晶型的制备方法
JP2014214299A (ja) * 2013-04-30 2014-11-17 旭硝子株式会社 近赤外線吸収粒子、その製造方法、分散液およびその物品
GB201604126D0 (en) * 2016-03-10 2016-04-27 Rotam Agrochem Int Co Ltd A novel form of amicarbazone, a process for its preparation and use of the same
JP2017061582A (ja) * 2014-02-07 2017-03-30 国立研究開発法人産業技術総合研究所 蛍光体微粒子の製造方法、蛍光体薄膜、波長変換膜、波長変換デバイス及び太陽電池
CN110799264A (zh) * 2017-07-05 2020-02-14 日本碍子株式会社 红外线处理装置

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Publication number Priority date Publication date Assignee Title
GB2122602A (en) * 1982-06-07 1984-01-18 Hisamitsu Pharmaceutical Co Novel 2,3-dihydro-indene derivatives
US6426406B1 (en) * 1999-07-06 2002-07-30 Allan S. Myerson Method for using laser light to control crystal form
JP2004267114A (ja) * 2003-03-10 2004-09-30 Ishii Iron Works Co Ltd 酒石酸塩の析出分離方法及びその方法を用いて得られた赤外線照射飲料
CN1884632A (zh) * 2006-05-23 2006-12-27 青岛大学 溶液法晶体快速生长装置
CN102267957A (zh) * 2011-08-24 2011-12-07 山东齐都药业有限公司 非布司他a晶型的制备方法
JP2014214299A (ja) * 2013-04-30 2014-11-17 旭硝子株式会社 近赤外線吸収粒子、その製造方法、分散液およびその物品
JP2017061582A (ja) * 2014-02-07 2017-03-30 国立研究開発法人産業技術総合研究所 蛍光体微粒子の製造方法、蛍光体薄膜、波長変換膜、波長変換デバイス及び太陽電池
GB201604126D0 (en) * 2016-03-10 2016-04-27 Rotam Agrochem Int Co Ltd A novel form of amicarbazone, a process for its preparation and use of the same
CN110799264A (zh) * 2017-07-05 2020-02-14 日本碍子株式会社 红外线处理装置

Also Published As

Publication number Publication date
EP4180106A4 (en) 2024-08-28
JP2025176115A (ja) 2025-12-03
CN115315299B (zh) 2024-06-04
JPWO2022014395A1 (enExample) 2022-01-20
EP4180105A4 (en) 2024-08-28
US20230150958A1 (en) 2023-05-18
CN115315297A (zh) 2022-11-08
US20230167577A1 (en) 2023-06-01
JPWO2022014396A1 (enExample) 2022-01-20
JP7096958B2 (ja) 2022-07-06
JPWO2022014397A1 (enExample) 2022-01-20
US20250179038A1 (en) 2025-06-05
EP4180105A1 (en) 2023-05-17
CN115315298A (zh) 2022-11-08
JP2022125073A (ja) 2022-08-26
JP7096956B2 (ja) 2022-07-06
EP4180104A1 (en) 2023-05-17
CN115315299A (zh) 2022-11-08
WO2022014397A1 (ja) 2022-01-20
CN115315297B (zh) 2024-06-04
WO2022014396A1 (ja) 2022-01-20
EP4180106A1 (en) 2023-05-17
WO2022014395A1 (ja) 2022-01-20
JP7096957B2 (ja) 2022-07-06
US20230150957A1 (en) 2023-05-18
EP4180104A4 (en) 2024-08-28

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