CN104248571A - Purely natural plant-containing abradant toothpaste and preparation method thereof - Google Patents
Purely natural plant-containing abradant toothpaste and preparation method thereof Download PDFInfo
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- CN104248571A CN104248571A CN201410479384.XA CN201410479384A CN104248571A CN 104248571 A CN104248571 A CN 104248571A CN 201410479384 A CN201410479384 A CN 201410479384A CN 104248571 A CN104248571 A CN 104248571A
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Abstract
The invention relates to the field of oral cavity cleaning and caring products, in particular to purely natural plant-containing abradant toothpaste and a preparation method thereof. The purely natural plant-containing abradant toothpaste comprises a humectant, a sweetener, a thickener, a foaming agent, a flavoring agent and an abradant, and is characterized in that the abradant comprises one or more of pseudoginseng main root powder, pseudoginseng flower powder and pseudoginseng stem leaf powder, or pseudoginseng main root residue powder, pseudoginseng flower residue powder and pseudoginseng stem leaf residue powder which are obtained after extraction; the abradant accounts for 5-75% of the total weight of the purely natural plant-containing abradant toothpaste. The purely natural plant-containing abradant toothpaste has the effects of protect gingiva and protecting enamel and has obvious effects of eliminating inflammation, stopping bleeding and removing toothpaste spots.
Description
Technical field
The present invention relates to oral cleaning nursing article field, especially one includes pure natural plant abrasive toothpastes and preparation method thereof.
Background technology
Radix Notoginseng has another name called Radix Notoginseng, it is a jewel in Chinese crude drug that the famous pharmacy man Li Shizhen (1518-1593 A.D.) of the Ming Dynasty is called " Radix Stephaniae Sinicae (Radix Stephaniae Dielsianae) " Radix Notoginseng, record in Qing Dynasty's pharmaceutical texts supplementary Amplifications of the Compendium of Materia Medica: " ginseng qi-tonifying first; Radix Notoginseng enriches blood first; taste with and merit also etc.; therefore becoming Panax pseudoginseng, is the most precious person in Chinese medicine." Chinese patent medicine " YUNNAN BAIYAO " of China and foreign countries of becoming famous and " Pien Tze Huang ", be namely that primary raw material is made with Radix Notoginseng, Radix Notoginseng is Araliaceae, stem, leaf, flower, all can be used as medicine.Radix Notoginseng, in Chinese herbal medicine, has hemostasis, the loose effect such as blood, analgesic therapy.Arasaponin is one of Radix Notoginseng principle active component.Conventional toothpaste abrasive material is based on chemical industry abrasive materials such as calcium carbonate, silicon dioxide, calcium hydrogen phosphate, and toothpaste improper use, can cause certain damage to tooth.
summary of the invention
The invention provides a kind of pure natural plant abrasive toothpastes and preparation method thereof; mainly replace traditional calcium carbonate, silicon dioxide, calcium hydrogen phosphate in order to plant (root of Radix Notoginseng, stem and leaf, flower) abrasive material; reach protection gingiva, protect adamantine effect, there is obvious antiinflammatory, hemostasis, the effect of removal toothpaste speckle simultaneously.
For reaching goal of the invention, the invention provides following technical scheme: a kind of pure natural plant abrasive toothpastes, be made up of wetting agent, sweeting agent, thickening agent, foaming agent, flavouring agent, abrasivus, it is characterized in that, abrasivus by Radix Notoginseng main root powder, notogenseng pollen, stem and leaf of Radix Notoginseng powder or after extracting Radix Notoginseng main root residue powder, flower of Radix Notoginseng residue powder, stem and leaf of Radix Notoginseng residue powder several compositions separately or mixing form, described abrasivus weight accounts for 5% ~ 75% of total amount percentage ratio.
Further: by weight percentage: abrasivus 5% ~ 75%, wetting agent 15% ~ 65%, foaming agent 1.5% ~ 3%, sweeting agent 0.5% ~ 3%, thickening agent 0.5% ~ 2%, stabilizing agent 0.1%-1%, antiseptic 0.1%-1%, flavouring agent 0.8% ~ 2%, surplus is deionized water.
Further: described wetting agent is one or more in sorbitol, glycerol, PEG400, Polyethylene Glycol 1450, xylitol; Foaming agent is one or more in sodium lauryl sulfate, sodium cocoyl glycinate, sodium lauryl sulphate, coconut palm osmanthus acylsarcosine sodium; Thickening agent is one or more in guar gum, xanthan gum, carrageenan, hydroxyethyl-cellulose, sodium carboxymethyl cellulose; Sweeting agent is one or more in saccharin sodium, aspartame, cyclamate; Stabilizing agent is one or more in tetrasodium pyrophosphate, sodium dihydrogen phosphate, sodium silicate; Flavouring agent is the one in strawberry essence, bamboo essence, Herba Menthae Rotundifoliae essence, Ilicis Purpureae essence; Antiseptic is one or more in ethyl hydroxybenzoate, methyl hydroxybenzoate, sodium benzoate, methyl parahydroxybenzoate, propyl p-hydroxybenzoate.
A preparation method for pure natural plant abrasive toothpastes, by weight percentage by abrasivus, wetting agent, sweeting agent, stabilizing agent, antiseptic, thickening agent, foaming agent, flavouring agent mixing, obtains lotion of toothpaste by stirring, vacuum outgas.
Further: first sweeting agent stabilizing agent, antiseptic to be dissolved in water by weight percentage and stir into aqueous solution with wetting agent and mix with abrasivus, thickening agent, foaming agent, stir and vacuum outgas, then add essence mixing, to stir and vacuum outgas obtains lotion of toothpaste.
Advantageous Effects: the present invention abandons and uses conventional toothpaste abrasive material, traditional dentifrice abrasives is based on chemical industry abrasive materials such as calcium carbonate, silicon dioxide, calcium hydrogen phosphate, conventional friction toothpaste is under the effect of toothbrush, dental surface cleaning action can only be played, and dentifrice abrasives is selected improper, and dental surface also can be caused to wear and tear.The invention has the advantages that with pure natural plant abrasive material of the present invention (Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng powder or through extract after Radix Notoginseng, flower of Radix Notoginseng, stem and leaf of Radix Notoginseng residue powder) replace traditional calcium carbonate, silicon dioxide, calcium hydrogen phosphate, the softness degree of having of natural abrasive rhizosphere plant flowers, stem and leaf, root, and make the granule of natural abrasive and hardness moderate, can make moist mastic, natural abrasive self natively has hemostasis, dissipating blood stasis, analgesic therapy, enhancing immunity, the effect such as to calm the nerves.Natural abrasive toothpaste is under the effect of toothbrush, effectively can remove the thin film of dental surface, bacterial plaque, dental calculus and gum massage, and do not damage enamel and dentin, the self-contained drug effect of natural abrasive can effectively alleviate the oral problem such as gingival swelling and pain, gingival hemorrhage.So natural abrasive toothpaste not only can reach outside cleaning effect, the effect that can also have alleviates gingival swelling and pain, gingival hemorrhage and protection gingiva, protects adamantine object.
The present invention will be further described below, to facilitate the technical staff to understand.
Embodiment 1: a kind of pure natural plant abrasive toothpastes, by weight percentage: sorbitol 45%, glycerol 10%, sodium carboxymethyl cellulose 0.8%, guar gum 0.7%, tetrasodium pyrophosphate 0.2%, sodium lauryl sulphate 2%, Mint Essence 0.8%, sodium benzoate 0.1%, PEG400 4%, saccharin sodium 0.5%, Radix Notoginseng main root powder 25%, all the other are deionized water.
Embodiment 2: a kind of preparation method of pure natural plant abrasive toothpastes, first get the raw materials ready by weight percentage: sorbitol 45%, glycerol 10%, sodium carboxymethyl cellulose 0.8%, guar gum 0.7%, tetrasodium pyrophosphate 0.2%, sodium lauryl sulphate 2%, Mint Essence 0.8%, sodium benzoate 0.1%, PEG400 4%, saccharin sodium 0.5%, Radix Notoginseng main root powder 25%, all the other are deionized water; First saccharin sodium, tetrasodium pyrophosphate, sodium benzoate are dissolved in deionized water by weight percentage, suck in Manufacturing medicine extract machine by vacuum, again with the glycerol squeezed in Manufacturing medicine extract machine, sorbitol, PEG400 is mixed into aqueous solution, again Radix Notoginseng main root powder, sodium carboxymethyl cellulose, guar gum, sodium lauryl sulphate mixing, send in Manufacturing medicine extract machine, vacuum high-speed stirred is after 25 minutes, add Mint Essence, then continue stirring 10 minutes, mixing, vacuum outgas, obtain lotion of toothpaste, leave standstill after 30 minutes, by sterile filling, packaging.
Embodiment 3: a kind of pure natural plant abrasive toothpastes, by weight percentage: sorbitol 24%, PEG400 10%, sodium carboxymethyl cellulose 1.1%, sodium lauryl sulfate 1.3%, sodium dihydrogen phosphate 0.3%, bamboo essence 1%, saccharin sodium 0.8%, methyl hydroxybenzoate 0.5%, Radix Notoginseng main root powder 10%, stem and leaf of Radix Notoginseng powder 40%, all the other are deionized water.
Embodiment 4: a kind of preparation method of pure natural plant abrasive toothpastes, first get the raw materials ready by weight percentage: sorbitol 24%, PEG400 10%, sodium carboxymethyl cellulose 1.1%, sodium lauryl sulfate 1.3%, sodium dihydrogen phosphate 0.3%, bamboo essence 1%, saccharin sodium 0.8%, methyl hydroxybenzoate 0.5%, Radix Notoginseng main root powder 10%, stem and leaf of Radix Notoginseng powder 40%, all the other are deionized water; First saccharin sodium, sodium dihydrogen phosphate, methyl hydroxybenzoate are dissolved in deionized water by weight percentage, suck in Manufacturing medicine extract machine by vacuum, aqueous solution is mixed into again with the PEG400 squeezed in Manufacturing medicine extract machine, sorbitol, again Radix Notoginseng main root powder, stem and leaf of Radix Notoginseng powder, sodium carboxymethyl cellulose, sodium lauryl sulfate mixing, send in Manufacturing medicine extract machine, vacuum high-speed stirred is after 30 minutes, add bamboo essence, continuation stirring 15 minutes, mixing, vacuum outgas, obtains lotion of toothpaste, leave standstill after 30 minutes, by sterile filling, packaging.
Embodiment 5: a kind of pure natural plant abrasive toothpastes, by weight percentage: sorbitol 15%, xylitol 35%, hydroxyethyl-cellulose 1%, xanthan gum 0.6%, sodium cocoyl glycinate 1.5%, sodium silicate 0.5%, ethyl hydroxybenzoate 0.1%, through extract after flower of Radix Notoginseng residue powder 30%, aspartame 2%, Ilicis Purpureae essence 1.2%, all the other are deionized water.
Embodiment 6: a kind of preparation method of pure natural plant abrasive toothpastes, first get the raw materials ready by weight percentage: sorbitol 15%, xylitol 35%, hydroxyethyl-cellulose 1%, xanthan gum 0.6%, sodium cocoyl glycinate 1.5%, sodium silicate 0.5%, ethyl hydroxybenzoate 0.1%, colored residue powder 30%, aspartame 2%, the Ilicis Purpureae essence 1.2% of Radix Notoginseng after extracting, all the other are deionized water; First aspartame, sodium silicate, ethyl hydroxybenzoate are dissolved in deionized water by weight percentage, suck in Manufacturing medicine extract machine by vacuum, aqueous solution is mixed into again with the xylitol squeezed in Manufacturing medicine extract machine, sorbitol, again the flower of Radix Notoginseng residue powder after extracting, hydroxyethyl-cellulose, xanthan gum, sodium cocoyl glycinate mixing, send in Manufacturing medicine extract machine, vacuum high-speed stirred is after 28 minutes, add Ilicis Purpureae essence, stirring 12 minutes, mixing, vacuum outgas, obtains lotion of toothpaste, leave standstill after 30 minutes, by sterile filling, packaging.
Embodiment 7: a kind of pure natural plant abrasive toothpastes, by weight percentage: sorbitol 45%, hydroxyethyl-cellulose 1.8%, methyl hydroxybenzoate 0.1%, tetrasodium pyrophosphate 0.2%, Radix Notoginseng main root powder 10%, through extract after flower of Radix Notoginseng residue powder 20%, coconut palm osmanthus acylsarcosine sodium 2%, aspartame 1%, strawberry essence 1.1%, all the other are deionized water.
Embodiment 8: a kind of preparation method of pure natural plant abrasive toothpastes, first get the raw materials ready by weight percentage: sorbitol 45%, hydroxyethyl-cellulose 1.8%, methyl hydroxybenzoate 0.1%, tetrasodium pyrophosphate 0.2%, Radix Notoginseng main root powder 10%, flower of Radix Notoginseng residue powder 20%, coconut palm osmanthus acylsarcosine sodium 2%, aspartame 1%, strawberry essence 1.1% after extracting, all the other are deionized water; First aspartame, tetrasodium pyrophosphate, methyl hydroxybenzoate are dissolved in deionized water by weight percentage, suck in Manufacturing medicine extract machine by vacuum, aqueous solution is mixed into again with the sorbitol squeezed in Manufacturing medicine extract machine, again Radix Notoginseng main root powder, the flower of Radix Notoginseng residue powder after extracting, hydroxyethyl-cellulose, the mixing of coconut palm osmanthus acylsarcosine sodium, send in Manufacturing medicine extract machine, vacuum high-speed stirred is after 30 minutes, add strawberry essence, stirring 15 minutes, mixing, vacuum outgas, obtains lotion of toothpaste, leave standstill after 30 minutes, by sterile filling, packaging.
Embodiment 9: a kind of pure natural plant abrasive toothpastes, by weight percentage: notogenseng pollen 35%, saccharin sodium 0.6%, Herba Menthae Rotundifoliae essence 1% after xylitol 15%, PEG400 20%, SDS 1%, sodium cocoyl glycinate 1.5%, tetrasodium pyrophosphate 0.25%, sodium dihydrogen phosphate 0.1%, sodium benzoate 0.2%, xanthan gum 1%, carrageenan 0.5%, stem and leaf of Radix Notoginseng powder 15%, extraction, all the other are deionized water.
Embodiment 10: a kind of preparation method of pure natural plant abrasive toothpastes, first get the raw materials ready by weight percentage: notogenseng pollen 35%, saccharin sodium 0.6%, Herba Menthae Rotundifoliae essence 1% after xylitol 15%, PEG400 20%, SDS 1%, sodium cocoyl glycinate 1.5%, tetrasodium pyrophosphate 0.25%, sodium dihydrogen phosphate 0.1%, sodium benzoate 0.2%, xanthan gum 1%, carrageenan 0.5%, stem and leaf of Radix Notoginseng powder 15%, extraction, all the other are deionized water, by weight percentage first by saccharin sodium, tetrasodium pyrophosphate, sodium dihydrogen phosphate, sodium benzoate is dissolved in deionized water, suck in Manufacturing medicine extract machine by vacuum, again with the PEG400 squeezed in Manufacturing medicine extract machine, xylitol is mixed into aqueous solution, notogenseng pollen after again flower being extracted, stem and leaf of Radix Notoginseng powder, xanthan gum, carrageenan, sodium lauryl sulphate, sodium cocoyl glycinate mixes, send in Manufacturing medicine extract machine, vacuum high-speed stirred is after 25 minutes, add Herba Menthae Rotundifoliae essence, stirring 10 minutes, mixing, vacuum outgas, obtain lotion of toothpaste, leave standstill after 30 minutes, pass through sterile filling, packaging.
Embodiment 11: a kind of pure natural plant abrasive toothpastes, by weight percentage: glycerol 15%, Polyethylene Glycol 1,450 20%, SDS 2%, sodium carboxymethyl cellulose 1%, carrageenan 0.2%, extract after Radix Notoginseng main root powder residue 20%, carry after stem and leaf of Radix Notoginseng powder residue 30%, methyl parahydroxybenzoate 0.05%, propyl p-hydroxybenzoate 0.05%, saccharin sodium 0.8%, Herba Menthae Rotundifoliae essence 1%, all the other are deionized water.
Embodiment 12: a kind of preparation method of pure natural plant abrasive toothpastes, first get the raw materials ready by weight percentage: glycerol 15%, Polyethylene Glycol 1,450 20%, SDS 2%, sodium carboxymethyl cellulose 1%, carrageenan 0.2%, extract after Radix Notoginseng main root powder residue 20%, carry after stem and leaf of Radix Notoginseng powder residue 30%, methyl parahydroxybenzoate 0.05%, propyl p-hydroxybenzoate 0.05%, saccharin sodium 0.8%, Herba Menthae Rotundifoliae essence 1%, all the other are deionized water, by weight percentage first by saccharin sodium, methyl parahydroxybenzoate, propyl p-hydroxybenzoate is dissolved in deionized water, suck in Manufacturing medicine extract machine by vacuum, glycerol in Manufacturing medicine extract machine will be squeezed into again, Polyethylene Glycol 1450 is mixed into aqueous solution, again the main root powder after extraction, stem and leaf of Radix Notoginseng residue powder after extraction, sodium carboxymethyl cellulose, carrageenan, sodium lauryl sulphate mixes, send in Manufacturing medicine extract machine, vacuum high-speed stirred is after 28 minutes, add and stay orchid, stirring 13 minutes, mixing, vacuum outgas, obtain lotion of toothpaste, leave standstill after 30 minutes, pass through sterile filling, packaging.
Embodiment 13: a kind of pure natural plant abrasive toothpastes, by weight percentage: the Radix Notoginseng main root residue powder 45% after xylitol 55%, PEG400 4%, sodium carboxymethyl cellulose 0.5%, hydroxyethyl-cellulose 1.5%, sodium cocoyl glycinate 1.5%, sodium lauryl sulfate 1%, Mint Essence 1.5%, tetrasodium pyrophosphate 0.3%, sodium silicate 0.25%, sodium benzoate 0.1%, saccharin sodium 0.5%, extraction, all the other are deionized water.
Embodiment 14: a kind of preparation method of pure natural plant abrasive toothpastes, first get the raw materials ready by weight percentage: the Radix Notoginseng main root residue powder 45% after xylitol 55%, PEG400 4%, sodium carboxymethyl cellulose 0.5%, hydroxyethyl-cellulose 1.5%, sodium cocoyl glycinate 1.5%, sodium lauryl sulfate 1%, Mint Essence 1.5%, tetrasodium pyrophosphate 0.3%, sodium silicate 0.25%, sodium benzoate 0.1%, saccharin sodium 0.5%, extraction, all the other are deionized water, by weight percentage first by saccharin sodium, tetrasodium pyrophosphate, sodium silicate, sodium benzoate is dissolved in deionized water, suck in Manufacturing medicine extract machine by vacuum, again with the xylitol squeezed in Manufacturing medicine extract machine, PEG400 is mixed into aqueous solution, again the Radix Notoginseng main root residue powder after extraction, hydroxyethyl-cellulose, sodium carboxymethyl cellulose, sodium cocoyl glycinate, sodium lauryl sulfate, mixing, send in Manufacturing medicine extract machine, vacuum high-speed stirred is after 30 minutes, add Mint Essence, stirring 15 minutes, mixing, vacuum outgas, obtain lotion of toothpaste, leave standstill after 30 minutes, pass through sterile filling, packaging.
Embodiment 15: a kind of pure natural plant abrasive toothpastes, by weight percentage: the flower of Radix Notoginseng residue powder 25% after sorbitol 24%, glycerol 10%, xanthan gum 1%, carrageenan 1%, sodium lauryl sulphate 1.3%, coconut palm osmanthus acylsarcosine sodium 1%, bamboo essence 0.8%, sodium benzoate 0.1%, cyclamate 1%, extraction, the stem and leaf of Radix Notoginseng residue powder 25% after extraction, all the other are deionized water.
Embodiment 16: a kind of preparation method of pure natural plant abrasive toothpastes, first get the raw materials ready by weight percentage: the flower of Radix Notoginseng residue powder 25% after sorbitol 24%, glycerol 10%, xanthan gum 1%, carrageenan 1%, sodium lauryl sulphate 1.3%, coconut palm osmanthus acylsarcosine sodium 1%, bamboo essence 0.8%, sodium benzoate 0.1%, cyclamate 1%, extraction, the stem and leaf of Radix Notoginseng residue powder 25% after extraction, all the other are deionized water; First cyclamate, sodium benzoate are dissolved in deionized water by weight percentage, suck in Manufacturing medicine extract machine by vacuum, aqueous solution is mixed into again with the glycerol squeezed in Manufacturing medicine extract machine, sorbitol, again the stem and leaf of Radix Notoginseng residue powder after the flower of Radix Notoginseng residue powder after extraction, extraction, xanthan gum, carrageenan, sodium lauryl sulphate, the mixing of coconut palm osmanthus acylsarcosine sodium, send in Manufacturing medicine extract machine, vacuum high-speed stirred is after 27 minutes, add bamboo essence, stir 15 minutes again, mixing, vacuum outgas, obtains lotion of toothpaste, leave standstill after 30 minutes, by sterile filling, packaging.
Embodiment 17: a kind of pure natural plant abrasive toothpastes, by weight percentage: sorbitol 45%, glycerol 16%, sodium carboxymethyl cellulose 1.2%, guar gum 0.8%, tetrasodium pyrophosphate 0.1%, sodium lauryl sulphate 1.5%, Mint Essence 0.8%, sodium benzoate 0.1%, PEG400 4%, saccharin sodium 0.5%, Radix Notoginseng main root powder 5%, all the other are deionized water.
Embodiment 18: a kind of preparation method of pure natural plant abrasive toothpastes, first get the raw materials ready by weight percentage: sorbitol 45%, glycerol 16%, sodium carboxymethyl cellulose 1.2%, guar gum 0.8%, tetrasodium pyrophosphate 0.1%, sodium lauryl sulphate 1.5%, Mint Essence 0.8%, sodium benzoate 0.1%, PEG400 4%, saccharin sodium 0.5%, Radix Notoginseng main root powder 5%, all the other are deionized water; First saccharin sodium, tetrasodium pyrophosphate, sodium benzoate are dissolved in deionized water by weight percentage, suck in Manufacturing medicine extract machine by vacuum, again with the glycerol squeezed in Manufacturing medicine extract machine, sorbitol, PEG400 is mixed into aqueous solution, again Radix Notoginseng main root powder, sodium carboxymethyl cellulose, guar gum, sodium lauryl sulphate mixing, send in Manufacturing medicine extract machine, vacuum high-speed stirred is after 25 minutes, add Mint Essence, then continue stirring 10 minutes, mixing, vacuum outgas, obtain lotion of toothpaste, leave standstill after 30 minutes, by sterile filling, packaging.
Embodiment 19: a kind of pure natural plant abrasive toothpastes, by weight percentage: sorbitol 5%, PEG400 10%, sodium carboxymethyl cellulose 0.5%, sodium lauryl sulfate 3%, sodium dihydrogen phosphate 1%, bamboo essence 2%, saccharin sodium 3%, methyl hydroxybenzoate 1%, Radix Notoginseng main root powder 10%, stem and leaf of Radix Notoginseng powder 40%, all the other are deionized water.
Embodiment 20: a kind of preparation method of pure natural plant abrasive toothpastes, first get the raw materials ready by weight percentage: sorbitol 5%, PEG400 10%, sodium carboxymethyl cellulose 0.5%, sodium lauryl sulfate 3%, sodium dihydrogen phosphate 1%, bamboo essence 2%, saccharin sodium 3%, methyl hydroxybenzoate 1%, Radix Notoginseng main root powder 10%, stem and leaf of Radix Notoginseng powder 40%, all the other are deionized water; First saccharin sodium, sodium dihydrogen phosphate, methyl hydroxybenzoate are dissolved in deionized water by weight percentage, suck in Manufacturing medicine extract machine by vacuum, aqueous solution is mixed into again with the PEG400 squeezed in Manufacturing medicine extract machine, sorbitol, again Radix Notoginseng main root powder, stem and leaf of Radix Notoginseng powder, sodium carboxymethyl cellulose, sodium lauryl sulfate mixing, send in Manufacturing medicine extract machine, vacuum high-speed stirred is after 30 minutes, add bamboo essence, continuation stirring 15 minutes, mixing, vacuum outgas, obtains lotion of toothpaste, leave standstill after 30 minutes, by sterile filling, packaging.
Embodiment 21: a kind of pure natural plant abrasive toothpastes, by weight percentage: sorbitol 7%, xylitol 8%, hydroxyethyl-cellulose 1%, xanthan gum 0.6%, sodium cocoyl glycinate 1.5%, sodium silicate 0.5%, ethyl hydroxybenzoate 0.1%, through extract after flower of Radix Notoginseng residue powder 75%, aspartame 2%, Mint Essence 1.2%, all the other are deionized water.
Embodiment 22: a kind of preparation method of pure natural plant abrasive toothpastes, first get the raw materials ready by weight percentage: sorbitol 7%, xylitol 8%, hydroxyethyl-cellulose 1%, xanthan gum 0.6%, sodium cocoyl glycinate 1.5%, sodium silicate 0.5%, ethyl hydroxybenzoate 0.1%, flower of Radix Notoginseng residue powder 75%, aspartame 2%, Mint Essence 1.2% after extracting, all the other are deionized water; First aspartame, sodium silicate, ethyl hydroxybenzoate are dissolved in deionized water by weight percentage, suck in Manufacturing medicine extract machine by vacuum, aqueous solution is mixed into again with the xylitol squeezed in Manufacturing medicine extract machine, sorbitol, again the flower of Radix Notoginseng residue powder after extracting, hydroxyethyl-cellulose, xanthan gum, sodium cocoyl glycinate mixing, send in Manufacturing medicine extract machine, vacuum high-speed stirred is after 28 minutes, add Mint Essence, stir 12 minutes again, mixing, vacuum outgas, obtains lotion of toothpaste, leave standstill after 30 minutes, by sterile filling, packaging.
Below with pure natural plant abrasive toothpastes of the present invention and ordinary toothpaste in contrast, use after 4 weeks, 12 weeks, evaluate it to the improvement of gingivitis symptom or alleviation situation.
The normal clinic case of oral mucosa subject, through the clinical patient being defined as simple gingivitis.Recruit satisfactory experimenter 60 people, be divided into experimental group 30 people and matched group 30 people at random, there is provided Yunnan Qi Dan natural abrasive toothpaste and ordinary toothpaste to experimenter respectively, carry out common oral care, the gingival index of record baseline, 4 weeks and 12 weeks, sulcular bleeding index and plaque index.The method of group t inspection and Pair test is adopted to carry out statistical analysis.This experiment adopts randomized controlled design.Another recruitment 10 normal persons use natural abrasive toothpaste, observe the acceptance level to this product.
Effect assessment
Baseline and use product after 4 weeks and 12 weeks, the gingiva tissue health condition (gingival index, sulcular bleeding index and dental plaque index) of clinical examination person's assessment index tooth successively.The assessment of index is all completed by veteran oral cavity doctor.
Gingival index (Gingival Index, Loe and Silnness, 1967)
Sulcular bleeding index (Sulus Bleeding Index, Muhleman and Son, 1971)
Dental plaque index (Plaque Index, Lou and Siness, 1963)
Check tooth position:
Denture is divided into 6 sections:
| 17-14 | 13-23 | 24-27 |
| 47-44 | 43-33 | 34-37 |
10 are chosen for index tooth in above six sections;
| 17? 16 | 11 | 26? 27 |
| 47? 46 | 31 | 36? 37 |
As certain block index anodontia one, then check residue index tooth; As index anodontism, then check all remaining teeth of this section; If the remaining tooth of this section five, then not record.
Result
Also examination 60 people are recruited in this experiment, and wherein experimental group 30 matched group 30 people completes experiment.Two groups have 1 people to come off.
Whole experimental session, experimenter reports there are no untoward reaction.
Mean ± the standard deviation of the gingival index of experimental group and matched group baseline, 4 weeks and 12 weeks, sulcular bleeding index and plaque index is in table 1.
Table 1. experimental group and matched group gingival index and sulcular bleeding index (mean ± standard deviation)
Result shows, and two groups of gingival index, sulcular bleeding index and plaque index baseline case no difference of science of statistics (p ﹥ 0.05 table 1), illustrate that two groups of baseline case are consistent.Use natural abrasive toothpaste 4 weeks compared with baseline, gingival hemorrhage index drops to 1.61 ± 0.49 by 2.22 ± 0.71, and gingival index drops to 1.29 ± 0.34 by 1.68 ± 0.45, and plaque index drops to 1.73 ± 0.33 by 2.04 ± 0.40, all there is significant difference (p ﹤ 0.05, table 1); Use natural abrasive toothpaste 12 weeks compared with baseline, gingival hemorrhage index drops to 1.39 ± 0.39 by 2.22 ± 0.71, gingival index drops to 1.05 ± 0.34 by 1.68 ± 0.45, plaque index drops to 1.49 ± 0.35 by 2.04 ± 0.40, all there is significant difference (p ﹤ 0.05, biao 1); Within 4 weeks, all there is significant difference (p ﹤ 0.05, table 1) with within 12 weeks, respectively organizing compared with data.Use ordinary toothpaste after 4 weeks, gingival hemorrhage index drops to 1.68 ± 0.68 gingival index by 2.18 ± 0.71 and drops to 1.29 ± 0.39 by 1.59 ± 0.45, plaque index drops to 1.79 ± 0.46 by 2.05 ± 0.47, significant difference (p ﹤ 0.05 is had compared with baseline, table 1), but 4 weeks with within 12 weeks, respectively organize data no difference of science of statistics (p ﹥ 0.05, table 1), analysis may with instruct the proper use of toothpaste of patient and toothbrush method relevant.
10 routine normal persons use the natural material toothpaste that rubs after one month, all better to the reflection of comfort level, cleannes and foam situation, have 4 example reflections slightly to stimulate, totally think and can accept.
During the Clinical practice of 12 weeks by a definite date, do not have to find the untoward reaction relevant to test products or oral soft tissue damage.Use and prove, after using natural abrasive toothpaste, obvious improvement (as gingival hemorrhage dental plaque etc.) can be crossed, promote gums healthy.
Without departing from the present invention, can also carry out various conversion and equivalent replacement to the present invention, therefore, patent of the present invention is not limited to disclosed specific implementation process, and should comprise the whole embodiments fallen within the scope of the claims in the present invention.
Claims (5)
1. a pure natural plant abrasive toothpastes, be made up of wetting agent, sweeting agent, thickening agent, foaming agent, flavouring agent, abrasivus, it is characterized in that, abrasivus by Radix Notoginseng main root powder, notogenseng pollen, stem and leaf of Radix Notoginseng powder or after extracting Radix Notoginseng main root residue powder, flower of Radix Notoginseng residue powder, stem and leaf of Radix Notoginseng residue powder several compositions separately or mixing form, described abrasivus weight accounts for 5% ~ 75% of total amount percentage ratio.
2. a kind of pure natural plant abrasive toothpastes according to claim 1, it is characterized in that, by weight percentage: abrasivus 5% ~ 75%, wetting agent 15% ~ 65%, foaming agent 1.5% ~ 3%, sweeting agent 0.5% ~ 3%, thickening agent 0.5% ~ 2%, stabilizing agent 0.1%-1%, antiseptic 0.1%-1%, flavouring agent 0.8% ~ 2%, surplus is deionized water.
3. a kind of pure natural plant abrasive toothpastes according to claim 1 or 2 any one, is characterized in that, described wetting agent is one or more in sorbitol, glycerol, PEG400, Polyethylene Glycol 1450, xylitol; Foaming agent is one or more in sodium lauryl sulfate, sodium cocoyl glycinate, sodium lauryl sulphate, coconut palm osmanthus acylsarcosine sodium; Thickening agent is one or more in guar gum, xanthan gum, carrageenan, hydroxyethyl-cellulose, sodium carboxymethyl cellulose; Sweeting agent is one or more in saccharin sodium, aspartame, cyclamate; Stabilizing agent is one or more in tetrasodium pyrophosphate, sodium dihydrogen phosphate, sodium silicate; Flavouring agent is the one in strawberry essence, bamboo essence, Herba Menthae Rotundifoliae essence, Ilicis Purpureae essence, Mint Essence; Antiseptic is one or more in ethyl hydroxybenzoate, methyl hydroxybenzoate, sodium benzoate, methyl parahydroxybenzoate, propyl p-hydroxybenzoate.
4.
asthe preparation method of a kind of pure natural plant abrasive toothpastes described in claim 1-3 any one, it is characterized in that, by weight percentage by abrasivus, wetting agent, sweeting agent, stabilizing agent, antiseptic, thickening agent, foaming agent, flavouring agent mixing, obtain lotion of toothpaste by stirring, vacuum outgas.
5. the preparation method of a kind of pure natural plant abrasive toothpastes according to claim 4, it is characterized in that, first sweeting agent, stabilizing agent, antiseptic are dissolved in water and stir into aqueous solution with wetting agent more by weight percentage, then mix with abrasivus, thickening agent, foaming agent, vacuum high-speed stirred is after 25 ~ 30 minutes, adds Mint Essence, continuation stirring 10 ~ 15 minutes, mixing, vacuum outgas, obtains lotion of toothpaste, after leaving standstill 30min, by sterile filling, packaging.
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| CN201410479384.XA CN104248571A (en) | 2014-09-19 | 2014-09-19 | Purely natural plant-containing abradant toothpaste and preparation method thereof |
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| CN201410479384.XA CN104248571A (en) | 2014-09-19 | 2014-09-19 | Purely natural plant-containing abradant toothpaste and preparation method thereof |
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Inventor after: Liu Huan Inventor after: Zhou Yanmei Inventor after: Gao Mingju Inventor after: Huang Zhaozhong Inventor before: Liu Huan Inventor before: Zhou Yanmei Inventor before: Gao Mingju |
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Application publication date: 20141231 |