A kind of toothpaste and preparation method thereof
Technical field
The present invention relates to field of toothpaste, in particular to a kind of toothpaste and preparation method thereof.
Background technology
Toothpaste is necessary dental care products in people's daily life.In recent years, some are nontoxic, there is medical treatment to protect
The Chinese herbal toothpaste of strong effect is increasingly subject to market favor, according to statistics, have the Chinese herbal toothpastes of national characters at present in occupation of
40%~50% domestic market share.
The Chinese herbal medicine usually added in Chinese herbal toothpaste is mostly the medicinal herb components with anti-inflammatory, whitening function, in addition to
The required abrasive material of addition toothpaste itself, sweetener, foaming agent and aromatic are also needed outside medicinal herb components, therefore ingredient is very multiple
Miscellaneous, various chemical addition agents are also easily so that adverse reactions such as in itself medicinal herb components are modified, go bad.
Siraitia grosvenorii is the fruit that Curcurbitaceae Siraitia grosvenorii belongs to perennial liana, is the medicine-food two-purpose of health ministry identification
Plant.Siraitia grosvenorii is rich in sweet tea glycosides, flavones, vitamin, protein, amino acid, mannitol, scavenger substances, lot of trace member
The active ingredients such as element have kobadrin, antibacterial shield tooth, anti-inflammatory and antalgic, Scavenger of ROS, peroxynitrite decomposition lipid and other effects.
Siraitia grosvenorii root tuber bitter rich in ingredients such as starch, protein, flavones, Anthraquinones, has very strong antimicrobial and anti-inflammation efficacy.
Therefore, toothpaste is prepared using Siraitia grosvenorii and its extract, is rationally set to play health-care effect using it and pass through
Count preparation process, avoid additionally adding various auxiliary materials such as abrasive material, sweetener, foaming agent, aromatic etc. be for consumers
Meaningful.
Invention content
The first object of the present invention is to provide a kind of toothpaste, and the toothpaste is with Siraitia grosvenorii fine powder and Fructus Monordicae extract
Extract powder is main component, can effectively anti-inflammatory, antibacterial, shield tooth, cleaning oral cavity.
The second object of the present invention is to provide a kind of preparation method of the toothpaste, this method simple production process, and
The health care ingredient of Siraitia grosvenorii can be retained to greatest extent.
In order to realize the above-mentioned purpose of the present invention, spy uses following technical scheme:
One aspect of the present invention is related to a kind of toothpaste, which is characterized in that the toothpaste includes following components:Siraitia grosvenorii is thin
Powder 15-25%, Fructus Monordicae extract extract powder 5-10%, coconut oil 20-30%, guar gum 10-20%, xanthans 15-25%,
Sodium benzoate 0.1-0.8%, surplus are deionized water, wherein, the sodium benzoate is the food grade sodium benzoate of national standard.
The toothpaste of the present invention is using the full fruit of new fresh fructus momordicae as raw material, is equipped with the auxiliary materials tune such as coconut oil, xanthans, guar gum
With into.Its with the substances such as lithocyte, the cellulose in Siraitia grosvenorii can replace conventional toothpaste in calcium carbonate, silica,
The industrial chemicals such as calcium monohydrogen phosphate are as abrasive material, and its scale removal works well.In addition, Siraitia grosvenorii has the sweet tea of high sugariness in itself
Glucoside, and itself has fragrance, and therefore, the addition of Siraitia grosvenorii fine powder, which can also substitute, needs sweetener to be added in general toothpaste
And aromatic.On the other hand, therefore the microstructure of Siraitia grosvenorii fine powder, easily blisters into concrete dynamic modulus shape, can play foaming
The effect of agent.It can be seen that it is of the invention by adding arhat fruit component, and eliminating in a variety of ordinary toothpastes needs to be addedization
Product component, safety greatly improve, and harm caused by toothpaste can be accidentally gulped down to avoid children, and suitable various people make
With.
Preferably, the component of the toothpaste is by mass percentage:Siraitia grosvenorii particle 18-22%, Fructus Monordicae extract
Extract powder 5-7%, coconut oil 20-25%, guar gum 13-16%, xanthans 19-22%, sodium benzoate 0.3-0.4%, surplus
For deionized water, wherein, the sodium benzoate is the food grade sodium benzoate of national standard.
Preferably, the granularity of the Siraitia grosvenorii fine powder is >=120 mesh.
Preferably, the granularity of the Fructus Monordicae extract extract powder is >=120 mesh.
It can promote disengaging for active material in Siraitia grosvenorii using the micropowders of high mesh number, play its health-care efficacy.
Another aspect of the present invention is related to the preparation method of the toothpaste, the described method comprises the following steps:
1) Siraitia grosvenorii fine powder and Fructus Monordicae extract extract powder are prepared;
2) coconut oil, guar gum, xanthans are proportionally added into emulsification pot, then add in deionized water and be sufficiently mixed
Even formation original mixture;
3) Siraitia grosvenorii fine powder, Fructus Monordicae extract extract powder and sodium benzoate are added in simultaneously in the mixture into step 2)
It is uniformly mixed, lotion is made in vacuum stirring.
Step of the present invention is relatively simple, easy to implement, and cost is relatively low, and raw material sources are extensive, also, side according to the invention
Method can farthest preserve the activity and health-care efficacy of Siraitia grosvenorii ingredient.
Preferably, the Siraitia grosvenorii fine powder in the step 1) is prepared by following steps:Use fresh sieve of sterile water wash
Chinese fruit, rear microwave drying and ultramicro grinding into >=120 mesh micropowders, wherein the Siraitia grosvenorii is arhat of no seed without insect pest
Fruit.
When selecting fruit, the Siraitia grosvenorii of low glucoside, moderate maturity is chosen, the Siraitia grosvenorii fine powder after microwave drying is ground can be
With fully discharging its bioactive substance during other components compatibility.
Preferably, microwave drying temperature≤75 DEG C, vacuum degree are -0.08~-0.098Mpa.
Preferably, the Fructus Monordicae extract extract powder in the step 1) through the following steps that prepare:
A) new fresh fructus momordicae is chosen, coarse crushing is carried out after cleaning, is carried afterwards using water;
B) water extract is concentrated, medicinal extract is formed, using being spray-dried and fine powder is made.
Preferably, in the step a), by the mesh of Siraitia grosvenorii coarse crushing to granularity >=20,2-4 times of water is added in, at 50-80 DEG C
Lower extraction 2-3 hours.
Preferably, it is stirred under vacuum in the step 3) and is carried out in vacuum emulsifying machine, mixing time is 5-10 minutes.
Compared with prior art, beneficial effects of the present invention are:
(1) toothpaste components such as abrasive material, sweetener, foaming agent, aromatic used in the present invention are the composition of Siraitia grosvenorii
Ingredient, other used auxiliary materials are also mainly derived from biology and to commonly use raw material in food medicine, and safety is good, can be to avoid
Harm caused by children accidentally gulp down toothpaste, is suitble to various people to use.
(2) Siraitia grosvenorii fine powder, the Fructus Monordicae extract extract powder selected in the present invention, production technology are protected to greatest extent
The effect of having stayed the health care ingredient of Siraitia grosvenorii, having made Siraitia grosvenorii anti-inflammatory, antibacterial, shield tooth, cleaning oral cavity is fully played.
(3) raw material sources of Siraitia grosvenorii toothpaste of the present invention are wide, simple production process, and production cost is low.
Specific embodiment
Embodiment of the present invention is described in detail below in conjunction with embodiment, but those skilled in the art will
Understand, the following example is merely to illustrate the present invention, and is not construed as limiting the scope of the invention.It is not specified in embodiment specific
Condition person, the condition suggested according to normal condition or manufacturer carry out.Reagents or instruments used without specified manufacturer is
The conventional products that can be obtained by commercially available purchase.
Embodiment 1
Siraitia grosvenorii toothpaste is prepared according to following steps
(1) preparation of the main supplementary material of Siraitia grosvenorii toothpaste
The preparation of fresh fructus momordicae fine powder:Select that low sweet tea glucoside, maturity be moderate, seedless monordica grosvenori of no disease and pests harm, through sterile
Water rinses repeatedly dries surface water, and after microwave drying, the micropowders of ultramicro grinding into 140-160 mesh preserve standby at low temperature
With.
It is prepared by Fructus Monordicae extract extract powder:Choose new fresh fructus momordicae, cleaning removes surface irregularities, and coarse crushing is into 20 purposes
Grain, adds water to be extracted 2 hours at 50 DEG C, concentrates and is spray dried to fine powder and saves backup at low temperature.
(2) formula composition of Siraitia grosvenorii toothpaste:Siraitia grosvenorii fine powder 18%, Fructus Monordicae extract extract powder 7%, coconut oil
20%, guar gum 13%, xanthans 22%, food-grade sodium benzoate 0.4%, remaining is deionized water.
(3) preparation of Siraitia grosvenorii toothpaste:First coconut oil, guar gum, xanthans are proportionally added into add in emulsification pot and be gone
Ionized water, which is sufficiently mixed, is formed uniformly original mixture, and Siraitia grosvenorii fine powder, arhat are then proportionally added into original mixture
Berry extract extract powder, food-grade sodium benzoate are simultaneously uniformly mixed, and are stirred 5 minutes in vacuum emulsifying machine and lotion is made, filling
Enter multiple tube.
Embodiment 2
Siraitia grosvenorii toothpaste is prepared according to following steps
(1) preparation of the main supplementary material of Siraitia grosvenorii toothpaste
The preparation of fresh fructus momordicae fine powder:Select that low sweet tea glucoside, maturity be moderate, seedless monordica grosvenori of no disease and pests harm, through sterile
Water rinses repeatedly dries surface water, and after microwave drying, the micropowders of ultramicro grinding into 140-160 mesh preserve standby at low temperature
With.
It is prepared by Fructus Monordicae extract extract powder:Choose new fresh fructus momordicae, cleaning removes surface irregularities, and coarse crushing is into 20 purposes
Grain, adds water to be extracted 3 hours at 80 DEG C, concentrates and is spray dried to fine powder and saves backup at low temperature.
(2) formula composition of Siraitia grosvenorii toothpaste:Siraitia grosvenorii fine powder 22%, Fructus Monordicae extract extract powder 5%, coconut oil
25%, guar gum 16%, xanthans 19%, food-grade sodium benzoate 0.3%, remaining is deionized water.
(3) preparation of Siraitia grosvenorii toothpaste:First coconut oil, guar gum, xanthans are proportionally added into add in emulsification pot and be gone
Ionized water, which is sufficiently mixed, is formed uniformly original mixture, and Siraitia grosvenorii fine powder, arhat are then proportionally added into original mixture
Berry extract extract powder, food-grade sodium benzoate are simultaneously uniformly mixed, and are stirred 10 minutes in vacuum emulsifying machine and lotion is made, filling
Enter multiple tube.
Embodiment 3
Siraitia grosvenorii toothpaste is prepared according to following steps
(1) preparation of the main supplementary material of Siraitia grosvenorii toothpaste
The preparation of fresh fructus momordicae fine powder:Select that low sweet tea glucoside, maturity be moderate, seedless monordica grosvenori of no disease and pests harm, through sterile
Water rinses repeatedly dries surface water, and after microwave drying, the micropowders of ultramicro grinding into 140-160 mesh preserve standby at low temperature
With.
It is prepared by Fructus Monordicae extract extract powder:Choose new fresh fructus momordicae, cleaning removes surface irregularities, and coarse crushing is into 20 purposes
Grain, adds water to be extracted 2 hours at 50 DEG C, concentrates and is spray dried to fine powder and saves backup at low temperature.
(2) formula composition of Siraitia grosvenorii toothpaste:Siraitia grosvenorii fine powder 15%, Fructus Monordicae extract extract powder 5%, coconut oil
20%, guar gum 10%, xanthans 15%, food-grade sodium benzoate 0.1%, remaining is deionized water.
(3) preparation of Siraitia grosvenorii toothpaste:First coconut oil, guar gum, xanthans are proportionally added into add in emulsification pot and be gone
Ionized water, which is sufficiently mixed, is formed uniformly original mixture, and Siraitia grosvenorii fine powder, arhat are then proportionally added into original mixture
Berry extract extract powder, food-grade sodium benzoate are simultaneously uniformly mixed, and are stirred 5 minutes in vacuum emulsifying machine and lotion is made, filling
Enter multiple tube.
Embodiment 4
Siraitia grosvenorii toothpaste is prepared according to following steps
(1) preparation of the main supplementary material of Siraitia grosvenorii toothpaste
The preparation of fresh fructus momordicae fine powder:Select that low sweet tea glucoside, maturity be moderate, seedless monordica grosvenori of no disease and pests harm, through sterile
Water rinses repeatedly dries surface water, and after microwave drying, the micropowders of ultramicro grinding into 140-160 mesh preserve standby at low temperature
With.
It is prepared by Fructus Monordicae extract extract powder:It chooses the cleaning of fresh fresh fructus momordicae and removes surface irregularities, coarse crushing is into 20 purposes
Particle adds water to be extracted 2 hours at 50 DEG C, concentrates and is spray dried to fine powder and saves backup at low temperature.
(2) formula composition of Siraitia grosvenorii toothpaste:Siraitia grosvenorii fine powder 25%, Fructus Monordicae extract extract powder 10%, coconut oil
30%, guar gum 20%, xanthans 25%, food-grade sodium benzoate 0.8%, remaining is deionized water.
(3) preparation of Siraitia grosvenorii toothpaste:First coconut oil, guar gum, xanthans are proportionally added into add in emulsification pot and be gone
Ionized water, which is sufficiently mixed, is formed uniformly original mixture, and Siraitia grosvenorii fine powder, arhat are then proportionally added into original mixture
Berry extract extract powder, food-grade sodium benzoate are simultaneously uniformly mixed, and are stirred 5 minutes in vacuum emulsifying machine and lotion is made, filling
Enter multiple tube.
Usage experience is evaluated
50 volunteers are chosen, it is asked to be brushed daily using the toothpaste prepared in the embodiment of the present invention 1 in morning in 15 days
Tooth carries out questionnaire survey after 5 minutes, 15 days to 50 volunteers, please its scale removal, fresh breath and use for toothpaste of the present invention
Experience and evaluated (including fragrance, sugariness etc.), conclusion is divided into satisfied and dissatisfied, and the result for being satisfied with number and satisfaction rate is as follows
Shown in table:
|
Scale removal |
Fresh breath |
Use feeling |
It is satisfied with number |
42 |
48 |
43 |
Satisfaction rate |
84% |
96% |
86% |
Siraitia grosvenorii toothpaste usage experience is evaluated
Hemostasis and anti-inflammation application case
Case 1
Zhang, 25 years old, people from hazard prevention, bleeding gums symptoms last 3 years happened occasionally, and attempts various Chinese herbal medicine teeth
Cream is brushed teeth, and is had no result.Using the Siraitia grosvenorii toothpaste of the present invention from June, 2015, bleeding gums symptom is improved after 10 days, and
Adhere to that the toothpaste using the present invention is brushed teeth gum not normal condition bleed bottom again so far.Zhang has broken away from the tired of bleeding gums from this
It disturbs.
Case 2
Slowly certain, 29 years old, during which Hefei ,Anhui people from city, bleeding gums symptoms last 7 years often occurs, attempts various Chinese and Western
Medicine toothpaste, which is brushed teeth, is showed no improvement.In August, 2015 plays the Siraitia grosvenorii toothpaste using the present invention, and bleeding gums symptom obtains after 13 days
Improve, and adhere to that the toothpaste using the present invention is brushed teeth gum not normal condition bleed bottom again so far.Slowly certain has broken away from tooth from this
The puzzlement of oulorrhagia.
Case 3
Lee, 40 years old, people from Beijing suffered from periodontitis 1 year, deep to be perplexed by swelling and aching of gum.This hair is used from April, 2015
Bright toothpaste, after a week swelling and aching of gum phenomenon be eased, adhere to using the present invention toothpaste brush teeth daily twice, swelling and aching of gum
Phenomenon is clearly better, and gradually fully recovers.Toothache puzzlement is broken away from from this.
Although illustrate and describing the present invention with specific embodiment, it will be appreciated that without departing substantially from the present invention's
Many other change and modification can be made in the case of spirit and scope.It is, therefore, intended that in the following claims
Including belonging to all such changes and modifications in the scope of the invention.