CN107007502A - The oral care composition of noresidue sense - Google Patents
The oral care composition of noresidue sense Download PDFInfo
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- CN107007502A CN107007502A CN201710251681.2A CN201710251681A CN107007502A CN 107007502 A CN107007502 A CN 107007502A CN 201710251681 A CN201710251681 A CN 201710251681A CN 107007502 A CN107007502 A CN 107007502A
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- extract
- bitter taste
- toothpaste
- oral care
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
Abstract
The present invention relates to a kind of oral care composition containing bitter taste material extract, the characteristics of it has noresidue sense.Oral care composition of the present invention is at least containing one kind in shrubby sophora extract, Andrographis Paniculata, Caulis Akebiae extract, Radix Gentianae extract, Herba Swertiae bimaculatae extract, Bitter Melon P.E.The present invention is bitter taste/non-bitter taste.
Description
Technical field
It is especially a kind of to include bitter taste material extract to reach without residual the present invention relates to oral care composition technical field
Stay the oral care composition of sense.
Background technology
Known, oral care composition is made up of many compositions.By taking toothpaste as an example, toothpaste is by rubbing agent, NMF, anti-
The raw material such as rotten agent, foaming agent, stabilizer are constituted, these raw material each own respective smell, taste.When used toothpaste with
Afterwards, these smells, taste can not be removed immediately, can still be stayed for some time.Have such phenomenon, morning after brushing after,
Although having spent 25 ~ 30 minutes, have a hunch that toothpaste is gargled totally also in the oral cavity, not, feeling to have a meal at that time is rather amiss.This is just
It is the phenomenon that the residual sense of lotion is caused.The residual sense of lotion how is removed, makes toothpaste salubriouser, " having brushed as not brushing ",
The residual sense for how removing oral care composition is extended to, this just turns into a problem.
The content of the invention
The present invention solves the technical problem for removing the residual sense using rear oral care composition.
The technical scheme is that by adding what bitter substance was realized in oral care composition.
More specifically technical scheme is that addition is less than 1.0% in oral care composition（Weight）Bitter taste material extract
Thing, preferably adds 0.01% ~ 1.0%（Weight）Bitter taste material extract, more preferably add 0.01% ~ 0.5%（Weight）Bitter taste material
Extract, more preferably adds 0.01% ~ 0.3%（Weight）Bitter taste material extract.
Further：The bitter taste material extract at least containing shrubby sophora extract, Andrographis Paniculata, Caulis Akebiae extract,
One kind in Radix Gentianae extract, Herba Swertiae bimaculatae extract, Bitter Melon P.E.
In the oral care composition of present invention addition bitter taste material extract, other additives can be further added, for example
Rubbing agent, NMF, foaming agent, thickener, sweetener, aromatic, colouring agent, preservative, stabilizer, emulsifying agent, effect system
The various preparations such as agent, manufacture agent.
Further：The composition can add essence and saccharin sodium, can also without essence and saccharin sodium, wherein
It is preferred that without essence and saccharin sodium.
Further：The present invention is bitter taste/non-bitter taste.
Further：The oral care composition is selected from toothpaste, tooth powder, gargle, chewing gum, tooth gel, tooth
Tooth joint strip, intraoral spray and intraoral cleaning agent etc..
The effect of invention
The oral care composition noresidue sense of the present invention, " having used as useless ".
Embodiment
Toothpaste or similar oral care composition, are generally made up of many raw material, such as rubbing agent, guarantor
Humectant, foaming agent, thickener, sweetener, aromatic, colouring agent, preservative, stabilizer, emulsifying agent, effect preparation, manufacture are used
The various preparations such as agent, these preparations are usually constructed with respective smell, taste.When toothpaste being made or similar oral care group
After compound, this smell, taste are still present, and will be through that could disappear after a while after use.It is worth noting that, fragrant
Essence and/or saccharin sodium generally itself can also remain unpleasant smell, taste while fragrance sense and sweet feel is provided.
The residual sense, refers to leaving unpleasant smell, mouth in oral care composition component after use
Taste, such as greasy, pungent, sour, numb, peppery, salty, raw meat, it is sweet, pained, not smooth, not including salubrious sense, fragrance sense.
By conscientious research, experiment, find by adding bitter substance in oral care composition, can weaken residual
Sense intensity is stayed, shortens the residual sense duration, reduction composition residual sense is reached, until making its purpose disappeared, so as to complete
The present invention.
Specific research finds that the bitter substance of bitter taste is perceived by being added in oral care composition to disappear
Subtract composition residual sense.The bitter substance can be artificial synthesized or natural or be extracted from natural materials
's.The bitter substance that can be enumerated has bitter, bitter-S, bitter taste plant, bitter taste plant extracts etc..
More specifically research is found, bitter substance can be selected from bitter taste material extract in the present invention.Also, when bitter taste material is carried
The addition of thing is taken to be more than 1.0%, then the taste of bitter taste material extract is excessively strong, the mouthfeel of oral care composition becomes order
People is uncomfortable.Wherein, 0.01% ~ 1.0% is preferably added（Weight）Bitter taste material extract, more preferably add 0.01% ~ 0.5%（Weight）
Bitter taste material extract, more preferably add 0.01% ~ 0.3%（Weight）Bitter taste material extract.Further, sent out by studying
It is existing, it as bitter taste material extract, can individually add, addition can also be combined.Bitter taste material extract can be selected from deer horn wormwood artemisia, snow
Upper alpine yallow herb, coffee, kuh-seng, fritillaria, semen armeniacae amarae, peach kernel, balsam pear, Chinese violet, golden cypress, coptis root, Herba Andrographitis, Sculellaria barbata, Chinese lobelia,
Ginseng, dandelion, rough gentian, akebi, Swertia patens etc.；Wherein preferred kuh-seng, Herba Andrographitis, akebi, rough gentian, Swertia patens, balsam pear.To sum up
Described, the bitter taste material extract preferably used in the present invention is at least selected from kuh-seng, Herba Andrographitis, akebi, rough gentian, Swertia patens, balsam pear
In one kind, the preferred addition of the bitter taste material extract is less than 1.0%（Weight）, more preferably addition be 0.01% ~
1.0%（Weight）, more preferably addition is 0.01% ~ 0.5%（Weight）, more preferably addition is 0.01% ~ 0.3%（Weight）.
The extracting method of bitter taste material extract of the present invention, can enumerate ethanol extraction method, water extraction method, ultrasonic extraction
Method, supercritical extraction etc..
Heretofore described bitter taste material extract is added in the form of extract, but is not limited to extract
The other forms such as form or medicinal extract or extract solution；When otherwise as extract solution is applied to mouth of the present invention
When chamber care composition, the addition in formula should be converted to disclosed in this invention form of extract addition
Amount.
In the oral care composition of present invention addition bitter taste material extract, other additives can be further added, for example
Rubbing agent, NMF, foaming agent, thickener, sweetener, aromatic, colouring agent, preservative, stabilizer, emulsifying agent, effect system
The various preparations such as agent, manufacture agent.
It is fragrant that the oral care composition of addition bitter taste material extract of the present invention can enumerate toothpaste, tooth powder, gargle, mouth
Sugar, tooth gel, tooth joint strip, intraoral spray and intraoral cleaning agent etc..
Embodiment
The present invention is further described below by specific embodiment, following examples are descriptive, is not limit
Qualitatively, it is impossible to which protection scope of the present invention is limited with this.Based on the embodiment in the present invention, those of ordinary skill in the art exist
The every other embodiment obtained under the premise of creative work is not made, the scope of protection of the invention is belonged to.
Prepare bitter taste material extract
Shrubby sophora extract is made from ethanol extraction method, choosing is with the following method：
Kuh-seng is cut into 1 ~ 2cm segments；At 80 DEG C, with the ethanol heating and refluxing extraction 4 hours of 15 times of weight, extract 3 times；Will
Obtained extract solution is dried under reduced pressure powdering under conditions of≤50 DEG C.
Same method produces Herba Andrographitis, akebi, rough gentian, Herba Swertiae bimaculatae extract.
Example 1 ~ 8 is application of the bitter taste material extract in toothpaste, specifically.
Example 1 ~ 2 is application of the single bitter taste material extract in calcium hydrogen phosphate type toothpaste, while with usual calcium monohydrogen phosphate
Type toothpaste prescription makes experiment contrast example（i）.Toothpaste constitutive material therein is weight percent content, specifically.
Reference examples（i）：Calcium monohydrogen phosphate 50, sorbierite 10, glycerine 10, propane diols 5, silica 3, sldium lauryl sulfate
2.8, menthol 1, sodium pyrophosphate 0.7, essence 1, xanthans 0.3, hydroxyethyl cellulose 0.15, ethylparaben 0.05, Ni Bo
Tortoise beetle ester 0.03, saccharin sodium 0.1, surplus is deionized water.It is de- by vacuum after above-mentioned raw material of toothpaste is mixed evenly
Gas, after the assay was approved, filling, toothpaste is made in sealing.
Example 1：By usual calcium hydrogen phosphate type toothpaste preparation method, the kuh-seng that 0.2 is individually added into reference examples toothpaste is carried
Take thing that the toothpaste of example 1 is made, specifically,
Calcium monohydrogen phosphate 50, sorbierite 10, glycerine 10, propane diols 5, silica 3, sldium lauryl sulfate 2.8, menthol 1, burnt phosphorus
Sour sodium 0.7, essence 1, xanthans 0.3, shrubby sophora extract 0.2, hydroxyethyl cellulose 0.15, ethylparaben 0.05, nipalgin
Methyl esters 0.03, saccharin sodium 0.1, surplus is deionized water.After shrubby sophora extract and above-mentioned raw material of toothpaste are mixed evenly,
After the assay was approved, filling by vacuum outgas, toothpaste is made in sealing.
Example 2：By usual calcium hydrogen phosphate type toothpaste preparation method, added in reference examples toothpaste 0.5 essence and
The toothpaste of example 2 is made in the shrubby sophora extract for being individually added into 0.3, specifically,
Calcium monohydrogen phosphate 50, sorbierite 10, glycerine 10, propane diols 5, silica 3, sldium lauryl sulfate 2.8, menthol 1, burnt phosphorus
Sour sodium 0.7, essence 1.5, shrubby sophora extract 0.3, xanthans 0.3, hydroxyethyl cellulose 0.15, ethylparaben 0.05, Ni Bo
Tortoise beetle ester 0.03, saccharin sodium 0.1, surplus is deionized water.Shrubby sophora extract is mixed evenly with above-mentioned raw material of toothpaste
Afterwards, after the assay was approved, filling by vacuum outgas, toothpaste is made in sealing.
Example 3 ~ 4 is application of the single bitter taste material extract in calcium carbonate type toothpaste, while with usual calcium carbonate type tooth
Cream prescription makes experimental control example（ii）.Toothpaste constitutive material therein is weight percent content, specifically.
Reference examples（ii）：Calcium carbonate 50, glycerine 8, sorbierite 10, sldium lauryl sulfate 2, hydroxyethyl cellulose 0.5, peppermint
Oil 0.5, essence 1, sodium pyrophosphate 0.5, saccharin sodium 0.1, ethylparaben 0.05, surplus is deionized water.By above-mentioned toothpaste
After the assay was approved, filling by vacuum outgas after raw material is mixed evenly, toothpaste is made in sealing.
Example 3：By usual calcium carbonate type toothpaste preparation method, the akebi that 0.2 is individually added into reference examples toothpaste is extracted
The toothpaste of example 3 is made in thing, specifically,
Calcium carbonate 50, glycerine 8, sorbierite 10, sldium lauryl sulfate 2.8, hydroxyethyl cellulose 0.5, peppermint oil 0.5, essence 1,
Sodium pyrophosphate 0.5, Caulis Akebiae extract 0.2, saccharin sodium 0.1, ethylparaben 0.05, surplus is deionized water.Akebi is extracted
After the assay was approved, filling by vacuum outgas after thing is mixed evenly with above-mentioned raw material of toothpaste, toothpaste is made in sealing.
Example 4：By usual calcium carbonate type toothpaste preparation method, added in reference examples toothpaste 0.1 saccharin sodium and
The toothpaste of example 4 is made in the Caulis Akebiae extract for being individually added into 0.3, specifically,
Calcium carbonate 50, glycerine 20, sldium lauryl sulfate 2.8, hydroxyethyl cellulose 0.5, peppermint oil 0.5, essence 1, sodium pyrophosphate
0.5, Caulis Akebiae extract 0.3, saccharin sodium 0.2, ethylparaben 0.05, surplus is deionized water.By Caulis Akebiae extract with it is above-mentioned
Raw material of toothpaste be mixed evenly after, it is after the assay was approved, filling by vacuum outgas, sealing toothpaste is made.
Example 5 ~ 6 is application of the single bitter taste material extract in silicon dioxide type toothpaste, while with usual silica
Type toothpaste prescription makes experimental control example（iii）.Toothpaste constitutive material therein is weight percent content, specifically.
Reference examples（iii）：Sorbierite 60, silica 20, glycerine 10, sldium lauryl sulfate 2, sodium carboxymethylcellulose
0.8, menthol 1, sodium pyrophosphate 0.7, essence 0.8, saccharin sodium 0.1, ethylparaben 0.06, surplus is deionized water.Will be upper
After the assay was approved, filling by vacuum outgas after the raw material of toothpaste stated is mixed evenly, toothpaste is made in sealing.
Example 5：By usual silicon dioxide type toothpaste preparation method, the rough gentian that 0.5 is individually added into reference examples toothpaste is carried
Take thing that the toothpaste of example 5 is made, specifically,
Sorbierite 60, silica 20, glycerine 10, sldium lauryl sulfate 2, sodium carboxymethylcellulose 0.8, menthol 1, pyrophosphoric acid
Sodium 0.7, essence 0.8, Radix Gentianae extract 0.5, saccharin sodium 0.1, ethylparaben 0.06, surplus is deionized water.Rough gentian is carried
Take after thing and above-mentioned raw material of toothpaste be mixed evenly, after the assay was approved, filling by vacuum outgas, toothpaste is made in sealing.
Example 6：By usual silicon dioxide type toothpaste preparation method, the rough gentian that 1.0 are individually added into reference examples toothpaste is carried
Take thing that the toothpaste of example 6 is made, specifically,
Sorbierite 60, silica 20, glycerine 10, sldium lauryl sulfate 2, sodium carboxymethylcellulose 0.8, menthol 1, pyrophosphoric acid
Sodium 0.7, essence 0.8, Radix Gentianae extract 1, saccharin sodium 0.1, ethylparaben 0.06, surplus is deionized water.Rough gentian is extracted
After the assay was approved, filling by vacuum outgas after thing is mixed evenly with above-mentioned raw material of toothpaste, toothpaste is made in sealing.
Example 7 is compound application of the bitter taste material extract in silicon dioxide type toothpaste, by usual silicon dioxide type toothpaste
Preparation method, adds Radix Gentianae extract and shrubby sophora extract in reference examples toothpaste, specifically,
Example 7：Sorbierite 60, silica 20, glycerine 10, sldium lauryl sulfate 2, sodium carboxymethylcellulose 0.8, menthol
1, sodium pyrophosphate 0.7, essence 0.8, Radix Gentianae extract 0.25, shrubby sophora extract 0.25, saccharin sodium 0.1, ethylparaben 0.06,
Surplus is deionized water.After Radix Gentianae extract, shrubby sophora extract are mixed evenly with above-mentioned raw material of toothpaste, by vacuum
Degassing, after the assay was approved, filling, toothpaste is made in sealing.
Example 8 is application of the single bitter taste material extract in the silicon dioxide type toothpaste without essence and saccharin sodium, together
When with without essence and saccharin sodium silicon dioxide type toothpaste prescription make experimental control example（iv）.Toothpaste constitutive material therein
It is weight percent content, specifically.
Reference examples（iv）：Sorbierite 60, silica 20, glycerine 10, sldium lauryl sulfate 2, sodium carboxymethylcellulose
0.8, menthol 1, sodium pyrophosphate 0.7, ethylparaben 0.06, surplus is deionized water.Above-mentioned raw material of toothpaste is mixed and stirred
After the assay was approved, filling by vacuum outgas after mixing uniformly, toothpaste is made in sealing.
Example 8：By usual silicon dioxide type toothpaste preparation method, the rough gentian that 0.3 is individually added into reference examples toothpaste is carried
Take thing that the toothpaste of example 8 is made, specifically,
Sorbierite 60, silica 20, glycerine 10, sldium lauryl sulfate 2, sodium carboxymethylcellulose 0.8, menthol 1, pyrophosphoric acid
Sodium 0.7, Radix Gentianae extract 0.3, ethylparaben 0.06, surplus is deionized water.Radix Gentianae extract is former with above-mentioned toothpaste
After the assay was approved, filling by vacuum outgas after material is mixed evenly, toothpaste is made in sealing.
There are 4 evaluation personnels Jing Guo professional training（Valuation officer A, B, C, D）In the residual sense of oral care composition
Aspect is respectively to the toothpaste of example 1 ~ 8 and reference examples（i）~（iv）Compare and evaluate, specifically.
To reference examples（i）~（iv）Evaluation：After use, residual sense all continue for 30 minutes or so.
Evaluation to example 1 ~ 8：
Valuation officer A：After use, the residual sense of component is almost not felt by, the mouthfeel of example 6 is bitter only, but mouthfeel is also fine；
Valuation officer B：Salubrious just as not swiped through tooth, example 6 is bitter taste only, and mouthfeel is very special；
Valuation officer C：The residual sense duration, only example 6 can get one's bitters, comfortable taste less than one minute；
Valuation officer D：The clean mouthfeel having no precedent, seems to forget to use toothpaste, only example 6 is bitter taste after being finished,
Mouthfeel is also fine.
It is not difficult to find out from the evaluation result of valuation officer：Reach noresidue sense, the bitter taste material extract of different lotion toothpaste
Addition it is different；Essence and saccharin sodium addition are bigger, and the bitter taste material extract required for eliminating residual sense is more；It is single to add
Plus the effect that bitter taste material extract and compound addition bitter taste material extract remain sense to eliminating is essentially identical.
Test result indicates that：Containing at least one bitter taste material extract, the residual sense to toothpaste is significantly improved effect,
When bitter taste material extract is added to a certain amount of and/or certain limit, toothpaste can be made to show noresidue sense；Bitter taste material is extracted
The addition and lotion of thing, saccharin sodium content, other components such as essence content have relation；The addition of bitter taste material extract with
The increase of the addition of saccharin sodium and/or the addition of essence and increase.When the present invention is bitter taste, it can still keep without residual
The characteristics of staying sense.
Conclusion：The toothpaste that the toothpaste of the extract of material containing bitter taste is relatively not added with bitter taste material extract in terms of sense is remained has substantially
Improvement；When bitter taste material extract is added to a certain amount of and/or certain limit, lotion noresidue sense；When bitter taste is presented in toothpaste
When, it is constant to the improvement result of residual sense.
Then, tooth powder, gargle and the mouth perfume of the bitter taste material extract containing the present invention are manufactured using usual way
Sugar.Also, the scope of the present invention is not limited thereto.
Example 9 is application of the bitter taste material extract in tooth powder, and tooth powder constitutive material therein, which is weight percentage, to be contained
Amount, specifically.
Calcium carbonate 75, lauryl sodium sulfate 2, Herba Swertiae bimaculatae extract 0.3, essence 0.5, menthol 1, saccharin sodium 0.1, Buddhist nun
Tortoise beetle ester 0.03 is moored, surplus is glycerine.By calcium carbonate, lauryl sodium sulfate, Herba Swertiae bimaculatae extract, methyl hydroxybenzoate, saccharin
Sodium is mixed evenly, and adds glycerine, essence and menthol, is mixed evenly again, through tooth powder is made after the assay was approved.
Example 10 is application of the bitter taste material extract in gargle, and gargle constitutive material therein is weight percent
Than content, specifically.
Edible ethanol 15, glycerine 10, Crodaret 1, Caulis Akebiae extract 0.3, essence 0.5, menthol
0.5, saccharin sodium 0.1, methyl hydroxybenzoate 0.05, surplus is deionized water.Glycerine, Crodaret are added to
Dissolved in ionized water, add edible ethanol and Caulis Akebiae extract, after being mixed evenly again, add essence, saccharin sodium
And methyl hydroxybenzoate, fully filtered after dissolving, through gargle is made after the assay was approved.
Example 11 is application of the bitter taste material extract in chewing gum, and chewing gum constitutive material therein is weight percent
Than content, specifically.
Glucose 20, Icing Sugar 20, xylitol 20, maltose 15, calcium carbonate 2, Radix Gentianae extract 0.5, menthol 1, surplus is
Matrix.The matrix that glucose, Icing Sugar, xylitol, maltose, calcium carbonate have been dissolved by heating, adds again after being well mixed
Enter Radix Gentianae extract and menthol, be sufficiently mixed uniform, cooling stripping and slicing, packaging, through chewing gum is made after the assay was approved.
Present invention thus provides oral care composition, it is with noresidue sense feature, oral care combination
Thing is also very unique, because it may have bitter mouthfeel.
Finally it should be noted that：The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations；Although
The present invention is described in detail with reference to the foregoing embodiments, it will be understood by those within the art that：It still may be used
To be modified to the technical scheme described in foregoing embodiments, or equivalent substitution is carried out to which part technical characteristic；
And these modification or replace, do not make appropriate technical solution essence depart from various embodiments of the present invention technical scheme spirit and
Scope.
Claims (5)
1. a kind of oral care composition of noresidue sense, the composition, which is included, is less than 1.0%（Weight）Bitter taste material extract
Thing, more preferably comprising 0.01% ~ 1.0%（Weight）Bitter taste material extract, more preferably comprising 0.01% ~ 0.5%（Weight）Bitter taste
Extract is expected, more preferably comprising 0.01% ~ 0.3%（Weight）Bitter taste material extract.
2. oral care composition according to claim 1, it is characterised in that the bitter taste material extract is at least containing hardship
One kind in conopsea extraction, Andrographis Paniculata, Caulis Akebiae extract, Radix Gentianae extract, Herba Swertiae bimaculatae extract, Bitter Melon P.E.
3. oral care composition according to claim 1, it is characterised in that the composition can add essence and sugar
Smart sodium, can also be without essence and saccharin sodium, wherein it is preferred that without essence and saccharin sodium.
4. oral care composition according to any one of claim 1 to 3, it is characterised in that the composition is choosing
From toothpaste, tooth powder, gargle, chewing gum, tooth gel, tooth joint strip, intraoral spray and intraoral cleaning agent.
5. oral care composition according to any one of claim 1 to 4, it is characterised in that the composition is hardship
Taste/non-bitter taste.
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| CN108159165A (en) * | 2018-03-20 | 2018-06-15 | 扬州工业职业技术学院 | A kind of compound Chinese medicine extract and its application in oral care product is prepared |
| CN108158913A (en) * | 2018-03-20 | 2018-06-15 | 扬州工业职业技术学院 | A kind of deodorization and sterilization Chinese medicinal toothpaste and preparation method thereof |
| CN108158913B (en) * | 2018-03-20 | 2020-10-27 | 扬州工业职业技术学院 | Sterilizing and deodorizing traditional Chinese medicine toothpaste and preparation method thereof |
| CN108159165B (en) * | 2018-03-20 | 2021-05-28 | 扬州工业职业技术学院 | Compound traditional Chinese medicine extract and application thereof in preparation of oral care products |
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Application publication date: 20170804 |