KR101481371B1 - Toothpaste composition containing Curcuma longa L and production method thereof - Google Patents

Abstract

The present invention provides a highly functional toothpaste composition, wherein a natural ingredient is used to prevent tooth-decay, remove bad breath, relieve inflammation, alleviate oral diseases, treat toothaches, and whiten teeth. The highly functional toothpaste composition of the present invention comprises: tumeric; natural organic sulfur; a mint exract; a red ginseng fermented extract; and an antibacterial composite extract consisting of one or more extracted from green tea, dried orange peels, Houttuynia cordata, herb patience, licorices, and morus barks.

Description

BACKGROUND OF THE INVENTION 1. Field of the Invention [0001] The present invention relates to a dentifrice composition containing Curcuma longa L and a production method thereof,

The present invention relates to a dentifrice composition containing ugum, and more particularly, to a dentifrice composition containing ugum, and more particularly, to a dentifrice composition containing a dentifrice composition and a method for producing the dentifrice composition. And to a method of making the same.

Recently, efforts to prevent periodontal disease, bad breath, and acne have been actively pursued through functional toothpaste.

As a prior art, Korean Patent No. 10-0859967 discloses a dentifrice composition containing a gingko extract and a dentifrice composition. The dentifrice composition comprises a phytoncide, which is prepared by pre-treating (extracting, refining, concentrating, etc.) A dentifrice composition having antimicrobial and antiseptic action, and a manufacturing method thereof.

In addition, Korean Patent No. 10-0999406 discloses a dentifrice composition containing an extract of Aspergillus oryzae as an active ingredient. In order to inhibit and inhibit the germs that cause gum disease, and to sterilize and treat inflammation, Disclosed is a dentifrice composition for alleviating, treating and preventing gum disease.

However, among the conventional dentifrice compositions containing dentifrice extracts and dentifrice production methods, there are limitations in mass production because of difficulty in obtaining raw materials due to limitations of raw materials and the like, and there are technical problems due to the complexity of raw material processing techniques.

In addition, the dentifrice composition containing the extract of Aspergillus oryzae as an active ingredient in the prior art has the extract of Aspergillus oryzae and the extract of the aspergillus as the main ingredients of the toothpaste. However, these ingredients alone provide satisfactory periodontal disease, elimination of bad breath, none.

Accordingly, there is an urgent need to develop a toothpaste ingredient which can contain a natural ingredient as a main ingredient and which can be easily obtained and prevent tooth decay, remove periodontal disease, bad breath, prevent acne, and whitening effect.

Korean Patent No. 10-0859967 Korean Patent No. 10-0999406

The present invention has been conceived to solve the above-mentioned problems, and it is an object of the present invention to provide a tooth care product which can prevent not only tooth decay but also bad breath removal, inflammation removal and oral disease using natural materials, A functional dentifrice composition and a process for producing the same.

To achieve the above object, the present invention provides a dentifrice composition containing curcuma longa L powder, a natural organic sulfur, a peppermint extract, a red ginseng fermentation extract, a green tea, a dandelion, , And an extract of an antimicrobial complex comprising at least one of the extracts.

The dentifrice composition according to the present invention may comprise 1 to 5% by weight of the herbal powder, 0.5 to 1.5% by weight of the natural organic sulfur, 1 to 3% by weight of the mint extract, 0.5-2.5% by weight of the red ginseng fermentation extract, and 7-10% by weight of the antibacterial complex extract.

In addition, the dentifrice composition according to the present invention can be used as a dentifrice composition containing xylitol, vegetable glycerin, xanthan gum, Yucca recurvifolia extract, sodium cocoyl apple amino acids, sodium phytate ), Calcium carbonate or bicarbonate, kaolin clay, natural bamboo salt, propolis, aniseed natural preservative from star anise, lemon essential oil, peppermint essential oil, and spearmint essential oil.

In another embodiment of the present invention, the calcium carbonate that may be included in the dentifrice composition is nano-sized to be nano-sized calcium carbonate.

The method for producing a dentifrice-containing dentifrice composition according to the present invention is a preferred embodiment,

a) adding vegetal glycerin to the vessel A, heating the vessel, adding xylitol to the vessel, dissolving the vessel, adding xanthan gum,

b) An antimicrobial compound extract obtained by extracting at least one of a peppermint extract, a red ginseng fermentation extract, a green tea, a dandelion, a dandelion, a lily of the valley, Adding sodium cocoyl apple amino acids and sodium phytate to the mixture and then mixing with the composition obtained in step a)

c) adding calcium carbonate, kaolin clay, urea powder, natural organic sulfur and ammonium bamboo to the composition obtained in step b)

d) adding to the composition obtained in step c) propolis, an anisanic acid preservative of star anise component, lemon essential oil, peppermint essential oil, And adding spearmint essential oil.

The dentifrice composition of the present invention can be prepared by containing a natural material as an effective ingredient, and thus is easily available and has excellent human stability.

In addition, the present invention is characterized by the excellent antibacterial and anti-inflammatory properties by containing ugum powder, natural organic sulfur, and antimicrobial composite natural extract, so that it is possible not only to effectively prevent tooth decay and tooth decay (gum bleeding) The effect of whitening (tartar removal) is also excellent.

BRIEF DESCRIPTION OF THE DRAWINGS Fig. 1 is a schematic view for explaining components of a dentifrice composition of the present invention and a production process thereof. Fig.

Curcuma longa L. contained in the dentifrice composition of the present invention is a perennial herbaceous plant belonging to the genus Ginger and has a similar appearance to turmeric, but has both smooth surfaces on both sides of the leaves. It grows naturally in Southeast Asia including southern China, India, and Okinawa, and is cultivated in the southern part of Korea.

Curcumin, a major yellow pigment, is known to play a role in antioxidant and cell protection (Chatcrjrr et al., 1999). According to several studies in Korea, (Prriyadarsini, 1997). It is also known to protect against diseases. Many studies on curcumin have been actively carried out and many papers have been published. In a representative study, the antioxidant activity of Ulgum (Kang et al., 1998; Selvam et al., 1995; Jeong et al., 2004), anticancer (Ryu et al., 2005; Khar et al. (Mazumder et al., 1995) and anti-inflammatory (Ammon & Wahl, 1991; Gupta & Gahsh, 1999). In addition, Ulgum has anti-angiogenic and anti-inflammatory effects, Many studies have shown that cholesterol levels in the liver are reduced and liver and nervous system functions. In particular, Ulgum has been shown to be effective against gum disease.

Ulgum is dried ginger roots, which are ginger root, and roots are roots. Although turmeric is part of the same root, it is a different species from Ulgum in strict sense. In other words, it is a different kind of crop. It is the same root, but it is divided according to the region. Ulugum is close to gray and turmeric is yellow.

In a preferred embodiment, the dentifrice composition according to the present invention contains a powdery molten salt, which is readily available in the market.

The natural organic sulfur (MSM, Methy Sulfonyl Methane) contained in the dentifrice composition of the present invention is a non-toxic, odorless sulfur extracted from plants and is a water-soluble white powder of 99.9% of Dimethy Sulfone.

The natural organic sulfur eliminates natural antidote, natural anticancer, natural emulsifier function, various chemical poison, decontamination and heavy metal poison. It also protects the body and scalp from environmental factors (dyes, perms, strong cleansing) along with detoxification.

In addition, sulfur has excellent ability to remove wastes and toxins, cell regeneration ability, strong pain relieving action, and strong inflammatory action. In particular, vegetable sulfur is a nontoxic component that has a strong property of transporting substances, so that it permeates deeply into the skin of the human body and exerts its weakness. It has strong action to expand the blood vessels and to enhance blood flow. Sulfur changes the cross-linking process of collagen, which is the constituent of connective tissue, and quickly reduces scar tissue. In particular, it acts as a natural antibiotic when using teeth. Such natural organic sulfur can be obtained from known products.

The peppermint extract contained in the dentifrice composition of the present invention is an extract of Mentha arvensis L, and the mint is perennial perennial plant of the perennial plant with the monocotyledonous plant. The main ingredient of mint contains menthol, menton, isom menton, campin, limonene and so on.

The efficacy of peppermint improves fever, inflammation, dryness, bile secretion, increase mucous secretion of respiratory tract, capillary dilation, excitement of central nervous system, increase of uterine contraction, boil. Dyspepsia, sore throat, tonsil pruritus, abdominal pain, diarrhea, vomiting, headache, toothache, cold, swelling and eye congestion.

As one embodiment of the pepper extraction method of the present invention, 1 kg of pepper is preheated at 50 degrees for 3 hours, heated for 3 hours and 30 minutes in the range of 95 degrees to 105 degrees, rapidly cooled, and subjected to ultrasonic cold extraction at 95 degrees .

In the fermented extract of red ginseng contained in the dentifrice composition of the present invention, saponin of red ginseng promotes secretion of catecholamine in the adrenal gland and inhibits lipid peroxidation, thereby inhibiting radical formation It has a beneficial effect in vivo. In particular, it is effective in restoring skin function.

As a method for extracting fermented red ginseng extract of the present invention, the following method can be adopted as a preferred embodiment.

- Method 1 -

400 g of ginseng and 400 g of ginseng were immersed in 12 L of purified water, preheated at 50 ° C. for 4 hours, heated at 90 ° C. for 40 hours, heated again at 105 ° C. for 32 hours to obtain red ginseng extract, And fermented using lactic acid bacteria for 72 hours while maintaining the temperature. Then, it is sterilized by heating at 100 degrees and then extracted to finally obtain fermented red ginseng extract.

- Method 2 -

The shade of the red ginseng extract is kept at 37 ° C and the external temperature is shut off. 2 g of 1 g of the undiluted solution of EM is added to the solution, and 20 g of natural betaine powder is kept for 72 hours. When the solution is warmed to room temperature, There is also a way to keep work and ferment.

The antimicrobial compound extract contained in the dentifrice composition of the present invention is obtained by extracting and mixing at least one of green tea, dandruff, mulberry, mulberry, licorice, and mulberry, and if the above six kinds are all contained, the efficacy can be maximized .

The efficacy of each component of the antimicrobial compound extract of the present invention is as follows.

1) Catechin, a polyphenolic compound contained in green tea, is used for aging management, whitening, skin soothing and cleansing and cleansing of mouth odor.

2) Dermis refers to the mature peel of citrus unshiu Markovich or related plants. It has high content of vitamin A, C and carbohydrate and organic acid content. It has vasodilator, anti ulcer, excellent diuretic effect. Cycle appetite and energy well, relieve thirst. Stop coughing and nausea. It contains a lot of Hsferradine, a fluroboronide compound with vitamin P action that reduces blood vessel permeability and blood vessel resistance to prevent blood vessel rupture.

3) Houttuynia cordata THUNB. Has excellent anti-inflammatory action to remove inflammation. In particular, a component called quercitrin is excellent for removing the toxins from the skin and expanding capillaries to purify blood.

4) The tortoises lower the root fever and treat the antibacterial, alopecia and bruises. Bactericidal action is excellent, as well as skin inflammation and long-term internal inflammation treatment. It inhibits cancer cell formation and prevents metastasis. It has excellent antimicrobial effects when gingival inflammation or hemorrhage, and the gums that show swollen gums and eruptive responses calm down.

5) Licorice binds to poisonous substance in liver, detoxifies and restores hepatic function. It is effective for drug addiction, hepatitis, urticaria, dermatitis, eczema. In addition, Jinhae also has a genetic effect, antihistamine, anti-catecholin action. It has been shown to be effective in relieving pain caused by sudden tensions in muscles and tissues, increasing body weight, increasing leukocyte counts, diuretic action, and anti-inflammatory effects. In particular, components such as liquiritin and liquiritigenin inhibit the development of peptic ulcers have.

6) Mori Cortex Radicis extracts from the mulberry root and acts as a blood pressure lowering agent, which is good for high blood pressure and good for diabetes. And it has the effect of suppressing the development of Staphylococcus aureus, influenza bacteria, and dysentery germs, and it has a function of suppressing the development of Staphylococcus aureus, diuretic, sedative, analgesic, body temperature drop and swelling. Also, the whitening effect is excellent.

The antibacterial complex extract of the present invention can be obtained by the following production method of one embodiment.

1) 300 g of green tea, 300 g of dermis and 300 g of watercress were immersed in 1500 g of 35-degree alcohol for 3 hours, heated at 95 ° C for 1 hour and 30 minutes, and then 6 L of purified water was poured to adjust the temperature to 105 ° C. The extract is extracted with a low-temperature vacuum extractor.

2) Immerse 500g of corn syrup, 600g of sorghum, 400g of licorice in 1500g of 35 degrees alcohol for 3 hours, heat it at 105 ℃ for 2 hours and 30 minutes, then pour 9L of purified water and adjust it to 105 ℃ for 2 hours Extract 3 L of extract with a low temperature vacuum extractor for 1 minute.

The extraction method may be modified by those skilled in the art depending on the type and amount of the materials contained in the extract.

The dentifrice-containing dentifrice composition according to the present invention is a dentifrice composition containing xylitol, vegetable glycerin, xanthan gum, Yucca recurvifolia extract, sodium cocoyl apple amino acids, sodium phytate sodium phytate, calcium carbonate or bicarbonate, kaolin clay, bamboo salt, propolis, aniseed natural preservative from star anise, lemon essential oil, peppermint essential oil peppermint essential oil, and spearmint essential oil.

The xylitol is a sugar alcohol-based natural sweetener used for chewing gum, confectionery, medicines, and oral hygiene products. The effect of xylitol on tooth decay is due to its pentose structure. It is said that the lactic acid which eats and discharges the glucose or fructose contained in the food such as mutans bacteria such as mutans bacteria or sorbitin bacteria corrodes the surface of the teeth. It is easy to decompose the 6-carboxy but the 5-valent xylitol easily decomposes. can not do it. As a result, the acid causing the tooth decay does not occur, and the tooth decayed from the tooth surface. In addition, xylitol is used as a preventive additive for tooth decay because it is suitable for prevention of tooth decay, such as promoting saliva secretion, as well as a refreshing effect that refreshes mouth.

The vegetable glycerin It is also called glycerol and is sweet in the form of transparent syrup. Glycerin prevents water evaporation and helps hydration. In addition, glycerin is harmless to human body, excellent in moisturizing effect, and has strong moisture absorption capacity. Vegetable glycerin is a natural product made from palm oil and palm oil. It is an ingredient that is soluble in water and has an effect of suppressing dermatitis. Especially, when it is used in mouth, it can prevent dryness of mouth.

It is a food additive for increasing the tackiness and viscosity of black xanthan gum, enhancing emulsion stability, and improving the physical properties and texture of food. It is extracted from sugarcane and used to make gel type. In addition, it has the properties of thickening action, coating film, gelation, etc. It also has a moisturizing effect and stabilizes the adrenal gland. Provides good spreading texture. Therefore, it is used as a stabilizer, thickener, binder, emulsifier, high-solubility, foaming agent, etc. in foods.

The yucca is an evergreen shrub with a monocotyledonous plant lily, and is effective for rheumatism and gout. It is also effective for neuralgia, arthritis, hypertension, hyperlipidemia, and has an effect of inhibiting AIDS infection. Also, It controls asthma. It has been found that this is due to saponin (a steroid hormone precursor substance), which is a functional ingredient contained in soybean or Korean ginseng.

In particular, Yucca extract is a liquid extracted from Yucca root and has a peculiar odor. It is added for foam preservation and quality preservation. It contains saponin glycoside. When it is mixed with water, it contains bubbles and the stability of foam is high. The feeling of use can be improved. The yucca extract contained in the present invention can be obtained from commercially available products.

remind Sodium cocoyl apple amino acids are a very mild apple surfactant (APL) that does not irritate the skin at all and can be used safely for sensitive skin and baby skin. It is made by acylation reaction of essential amino acid obtained from apple juice. It does not denature skin protein and does not affect skin exfoliation system.

The sodium phytate is extracted from rice bran and used as an antioxidant.

Calcium carbonate, which may be contained in the present invention, is used as an abrasive. In one embodiment, precipitated calcium carbonate is preferably used. Such calcium carbonate or precipitated calcium carbonate removes the plaque attached to the tooth surface. As another embodiment, bicarbonate may be used instead of calcium carbonate. In another embodiment of the present invention, the calcium carbonate that may be included in the dentifrice composition is nano-sized to be nano-sized calcium carbonate. As described above, by using calcium carbonate, which is a nanoized dry material, wear of the teeth can be minimized.

Kaolin clay (kaolin Clay) of the present invention is to have a soft, tough clay used in pharmaceuticals and cosmetics and in the most fundamental efficacy of the clay to actively the physiological function of the cell by generating a large quantity of far infrared rays and anions as natural minerals generates a thermal energy It has a photoelectric effect that releases harmful substances, and is excellent in cleansing power and decomposition power. It is used as a tooth abrasive. It absorbs teeth and removes calculus.

In addition, Kaolin White Clay is well-suited for very sensitive skin and has excellent absorbency, attracting the dirt of the pores, promoting blood circulation, and has excellent sedative effect.

The bamboo salt which may be contained in the dentifrice composition of the present invention is a salt of baked 9 times in a bamboo container and acts as a natural disinfectant. The efficacy of bamboo salt is as follows.

1) Cell production function: It plays a role of restoring dead or destroyed cells at a rapid rate, 2) Anti-inflammatory action: It acts to remove inflammation, 3) Hypocentesis: It works to clear blood, 4) Improvement: It improves the immunity and resistance by changing acidic constitution to weakly alkaline constitution. 5) Detoxification: It works to wash the poison in the body at a high rate. 6) Antibacterial action: Reducing power not only excretes a large amount of wastes, but also protects against damages caused by active oxygen.

Propolis, which may be contained in the dentifrice composition of the present invention, is a natural antimicrobial substance as a mixture of resinous substances collected from plants such as buds and sap of trees. Antimicrobial, sterilization and immunity activation, immune function enhancement, cell activation and cell regeneration, antiallergic, genetic damage defense, vasoconstriction, antioxidant, and anticancer drug side effects. Propolis also acts to control symptoms.

The propolis and porphyritis salts may be obtained from known products.

A natural preservative may be included in the composition of the present invention, and as a preferred embodiment, an anise acid (liquid) natural preservative of star anise component may be included.

The dentifrice composition according to the present invention may contain the above-mentioned three kinds of essential oils. The essential oil is a major component of aromatherapy, which is recently regarded as an alternative medicine, and is a volatile organic compound extracted from a plant by distillation Point.

For lemon essential oils, Lemon (Citrus limonum) is mainly composed of aldehydes and monoterpene hydrocarbons, and is said to have effects such as preservation, sterilization and immunity strengthening. In particular, lemon was found to be highly effective against cavities caused by oral bacteria.

In spearmint essential oils, spearmint (Mentha spicata) It is similar to peppermint, but it is good for children because it is weak. It treats cold, heat, and influenza, and is effective in treating asthma, bronchitis, mucosal inflammation, and sinusitis. It can also be used as a local anesthetic, bactericide, anticonvulsant, astringent, antiseptic, tofu, bile release accelerator, expectorant, appetizer.

In peppermint essential oils, peppermint (Mentha piperita) is the main constituent of menthol and menthone, and is effective in the treatment of itching and inflammation, and is also effective in preservation, anticonvulsant and dementia .

Especially, the anticonvulsive effect of peppermint is based on the action on the nervous system, and the fresh and spicy nature of menthol improves the concentration by awakening the nerves and brain. Muscular pain, back pain, bruises, joint pain, toothache and has an effect of local anesthetic. It is also one of the most effective oils in the digestive system and is effective in indigestion, nausea, stomach pain, diarrhea and hyperlipemia. It shrinks the blood vessels and accelerates the flow of blood vessels to promote blood cell regeneration. In addition, lymphatic and fascia contracts and relaxes, enhances the function of smooth toxin release, helps to relieve headache and migraine.

The dentifrice composition according to the present invention may comprise 1 to 5% by weight of the herbal powder, 0.5 to 1.5% by weight of the natural organic sulfur, 1 to 3% by weight of the mint extract, 0.5-2.5% by weight of the red ginseng fermentation extract, and 7-10% by weight of the antibacterial complex extract.

The antimicrobial composition of the present invention may contain 1 to 2% by weight of green tea extract, 1 to 2% by weight of dandruff extract, 2 to 3% by weight of oat seed extract, 2 to 3% by weight of Sorghum extract, 1 to 2 wt% of licorice extract, and 1 to 2 wt% of extract of Mongolia bark extract.

Examples of the contents of other components that can be contained in the dentifrice composition according to the present invention are as follows.

material Capacity (wt%) material Capacity (wt%) Xylitol 25 to 30 Kaolin clay 8-12 Vegetable glycerin 16-20 Bamboo bamboo 0.5 to 1.5 Xanthan gum 0.1 to 1 Propolis 0.5 to 1.5 Yucca extract 5 ~ 7 Anisan Natural Preservative 0.5 to 1.5 Sodium cocoyl apple amino acid 4 to 6 Lemon essential oil 0.1 to 0.2 Sodium phytate 0.1 to 0.2 Spearmint Essential Oil 0.1 to 0.2 Calcium carbonate (or bicarbonate) 12-16 Peppermint Essential Oil 0.05 to 0.15

Now, an embodiment of a method for manufacturing a toothpaste composition containing acorns according to the present invention will be described below.

a) Add 18% by weight of vegetable glycerin into the container A, heat the mixture at 40 to 50 degrees Celsius, add 27% by weight of xylitol to dissolve the mixture, and add 0.5% by weight of xanthan gum to dissolve.

b) 8% by weight of an antibacterial complex extract consisting of 1% by weight of green tea extract, 1% by weight of dandruff extract, 1% by weight licorice extract, 1% by weight of manganese bark extract, 2% , 2% by weight of peppermint extract and 2% by weight of fermented red ginseng extract were mixed. Then, 6% by weight of yucca extract, 5% by weight of sodium cocoyl apple amino acids, sodium phytate, 0.1% by weight, and then mixed with the composition obtained in the step a).

c) adding 14% by weight of calcium carbonate, 10% by weight of kaolin clay, 3% by weight of urea powder, 1% by weight of natural organic sulfur and 1% by weight of natural bamboo salt to the composition obtained in step b) And mixed.

d) 1% by weight of propolis, 1% by weight of an anisanic acid natural preservative as a star anise ingredient, 0.15% by weight of lemon essential oil, 0.1% by weight of peppermint essential oil, and 0.15% by weight of spearmint essential oil, respectively.

If the final dentifrice composition obtained in the step d) is injected into a tube or the like, it can be used as a toothpaste.

- Experimental evaluation of examples and comparative examples

Table 2 below shows a preferred embodiment of the dentifrice composition containing ugly according to the present invention.

material Capacity (wt%) material Capacity (wt%) Xylitol 27 Calcium carbonate (or bicarbonate) 14 Vegetable glycerin 18 Kaolin clay 10 Dagger 0.5 Turmeric powder 3 Peppermint extract 2 Bamboo bamboo One Fermented red ginseng extract 2 Propolis One Antimicrobial complex extracts 6 species 8 Anisan Natural Preservative (liquid) One Natural organic sulfur One Lemon E.O (Essential Oil) 0.15 Yucca extract (concentrate) 6 Spearmint E.O (Essential Oil) 0.15 Apple Wash
Sodium cocoyl apple amino acid) 5 Peppermint E.O (Essential Oil) 0.1 Sodium phytate 0.1

Table 3 below shows conventionally known toothpaste ingredients.

division Name of the product manufacturer chief ingredient Comparative Example 1 Perio 46cm
White Nau Toothpaste LG Household & Health Care Colloidal silicon dioxide, aqueous hydrogen peroxide 35% Comparative Example 2 2080 Mother Mam Toothpaste Aekyung (Artificial colorant, artificial sweetener, no artificial flavor) Fluorine, vitamin E, calcium, organic extract (apple), herbal tea mixture (including natural fermented tea) Comparative Example 3 Bamboo salt toothpaste LG Household & Health Care Dentile type silica car, bamboo salt, Centella specific extract, potassium glycyrrhizinate, sodium fluoride Comparative Example 4 Perio Freshen Toothpaste LG Household & Health Care Calcium glycerophosphate, calcium carbonate, sodium monofluorophosphate

Experimental Example 1: Gingivitis inhibition experiment

In this experiment, all 20 subjects who were in the same environment were subjected to the first oral examination before the experiment. The test method was a single blind method and the same toothbrush was given to all subjects during the period of eliminating residual effect for 4 weeks before the experiment. In the experimental method, the gingival per tooth was divided into the nasal surface and the lingual surface, and the average value of the index was calculated. Each gingivitis was graded from 0 to 3 according to the criteria of roe and silence, and the gingivitis index of each tooth was calculated, and the gingival index of each individual was calculated. .

division base line After 1 month Two months later Three months later Example 0.60 0.52 0.45 0.36 Comparative Example 1 0.60 0.58 0.56 0.55 Comparative Example 2 0.60 0.60 0.57 0.57 Comparative Example 3 0.60 0.58 0.58 0.57 Comparative Example 4 0.60 0.59 0.58 0.56

As shown in Table 4, Comparative Examples 1 to 4 showed a reduction rate of about 8% or less until after 3 months, but the Example showed a reduction rate of 40%, which proved to be excellent in the treatment of inflammation.

≪ Experimental Example 2 >: Measurement experiment of whitening effect

For the measurement method, the whitening effect was measured while using the toothpaste of Examples and Comparative Examples for 3 months. Fifty subjects were selected and color tones were measured in advance with a colorimeter (Trubyte Bioform). Then, the color tone was classified into 5 groups (10 users in the embodiment and 10 users in the comparative example) Were used to distribute the dentifrice compositions of the Examples and Comparative Examples 1 to 4. To confirm the increase in lightness of the teeth, 24 kinds of standard standards of brightness were measured in a Trubyte Bioform colorimeter Ten sensory sensory items were selected and the lightness value was assigned to each of the evaluation scores from the lowest point 1 to the highest point 10. Before each toothpaste was used, , And the brightness value after brushing for 3 months was evaluated, and then the rate of increase of the average brightness value was calculated with respect to the brightness value before the test.

division Average brightness value
(Before the experiment) Average brightness value
(Three months later) Brightness Value Increase Rate (%) Example 3.5 5.5 57.1% Comparative Example 1 3.5 3.9 11.4% Comparative Example 2 3.6 4.1 13.8% Comparative Example 3 3.5 4.0 14.2% Comparative Example 4 3.7 4.0 8.1%

As shown in Table 5, the lightness value increase rate of Comparative Examples 1 to 4 was 14.2% at maximum, but the lightness increase rate of the Example was 57.1%, proving that tooth whitening and tartar removal effect were excellent.

≪ Experimental Example 3 >: Satisfaction

The toothpaste of the present invention (Examples) and the toothpaste of Comparative Examples 1 to 4 were used in 30 adult males and females, and the following items were examined, and the results of the average values were shown in the following table. The scores were classified as 0 (very poor) to 10 (very satisfied).

division Appearance color incense flavor Viscosity Cleaning power Bubble power Moisture power lubricity Refreshing Overall rating Example 8 9 9 8 9 10 8 8 9 10 88 Comparative Example 1 7 6 6 7 7 6 6 6 5 7 63 Comparative Example 2 7 7 8 8 6 8 7 7 7 7 72 Comparative Example 3 6 6 6 6 6 8 7 6 6 7 64 Comparative Example 4 7 6 6 6 7 6 7 7 6 7 65

As shown in Table 6 above, the dentifrice composition of the present invention was satisfactory in all aspects of the above items as compared with the dentifrice composition components of the conventional comparative examples 1 to 4, and the total score of satisfaction was also 25 points Respectively.

While the present invention has been particularly shown and described with reference to exemplary embodiments thereof, it is to be understood that the invention is not limited to the disclosed embodiments, but, on the contrary, is intended to cover various modifications and equivalent arrangements included within the spirit and scope of the appended claims.

Claims (3)

Curcuma longa L powder;
Natural organic sulfur;
Mint extract;
Fermented red ginseng extract;
A green tea, a dermis, a perennial herb, a sorghum, a licorice,
Wherein the dentifrice composition comprises a dentifrice composition. The method according to claim 1,
The present invention relates to a dentifrice composition comprising 1 to 5% by weight of the herbal powder, 0.5 to 1.5% by weight of the natural organic sulfur, 1 to 3% by weight of the peppermint extract, 0.5 to 2.5% By weight, and the antimicrobial compound extract is contained in an amount of 7 to 10% by weight. a) adding vegetal glycerin to the container A, heating the mixture, adding xylitol to the mixture, dissolving the mixture, adding xanthan gum;
b) An antimicrobial compound extract obtained by extracting at least one of a peppermint extract, a red ginseng fermentation extract, a green tea, a dandelion, a dandelion, a lily of the valley, Adding sodium cocoyl apple amino acids and sodium phytate to the mixture, and mixing the composition with the composition obtained in step a);
c) adding calcium carbonate, kaolin clay, urea powder, natural organic sulfur and boric acid salt to the composition obtained in step b) and mixing them; And
d) adding to the composition obtained in step c) propolis, an anisanic acid natural preservative of star anise component, lemon essential oil, peppermint essential oil, Characterized in that it comprises the step of adding spearmint essential oil to the dentifrice composition.

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