KR20240056349A - Functional soap for preventing hair loss using clove and method for manufacturing thereof - Google Patents

Abstract

A functional soap for preventing hair loss using cloves and a method for manufacturing the same are provided. The functional soap for preventing hair loss using cloves is formed by mixing clove powder, oil, purified water, caustic soda, and persimmon vinegar, and then saponifying at 25 to 35° C. for 40 to 50 hours. 800 parts by weight of the oil per 120 parts by weight of the purified water. to 1500 parts by weight, 120 to 160 parts by weight of the purified water, 130 to 170 parts by weight of the caustic soda, and 120 to 160 parts by weight of the persimmon vinegar.

Description

Functional anti-hair loss soap using cloves and manufacturing method thereof {FUNCTIONAL SOAP FOR PREVENTING HAIR LOSS USING CLOVE AND METHOD FOR MANUFACTURING THEREOF}

The present invention relates to an anti-hair loss functional soap using cloves and a manufacturing method thereof, and more specifically, to an anti-hair loss functional soap using cloves that can effectively prevent hair loss by mixing clove powder in an appropriate amount and a manufacturing method thereof. will be.

Hair loss is caused by fatigue, stress, disease, drugs, environmental factors, and genetic factors. Specifically, there is aging of the scalp due to environmental factors such as fine dust, yellow dust, soot, mites, formaldehyde, and exposure to ultraviolet rays, and hair loss due to genetic factors due to the action of androgen hormones.

Due to these factors, active oxygen is formed in the scalp tissue, which reduces antioxidants normally present in the skin, causes moisture loss in the stratum corneum, and reduces collagen content in the dermis. Therefore, in order to prevent hair loss, various methods are being used to keep the scalp moist and improve blood circulation to remove active oxygen. In addition, in the case of genetic factors, the consumption of foods or drugs with anti-androgen properties is being used.

Generally, when washing your hair, you use shampoo or soap to wash away sebum, sweat, dead skin cells, wastes and dust that accumulate on the scalp. In addition, to provide nutrition to the scalp and hair, rinses and nutritional supplements containing various essences are also widely used.

However, conventional shampoos, rinses, essences, etc. contain chemicals as their main ingredients, so they have the problem of causing various side effects, including skin problems, or hair loss depending on the body constitution. Accordingly, the demand for shampoos and soaps (shampoo bars) centered on natural ingredients with reduced chemical content is increasing day by day.

Meanwhile, clove (Syzygium aromaticum) refers to the dried flower buds of the clove tree, a tropical evergreen tree, before it blooms, and is also called clove. Cloves contain a variety of bioactive compounds, including eugenol, acetyleugenol, and eugenol salicylate. In addition, cloves have a unique strong taste and aroma, and have been used as a medicine and spice since ancient times.

In particular, the eugenol component contained in cloves is a natural antioxidant that has the effect of relieving pain, so it is effective in gum inflammation and gum pain, and is known to be effective in skin troubles and acne through its antibacterial effect. Accordingly, clove is used as a raw material for medicines such as toothpaste, cosmetics, and preservatives, as in prior art 1 (Korean Patent No. 10-1796699) and prior art 2 (Korean Patent No. 10-1511747). Recently, it has been reported that this eugenol component has anti-androgenic properties.

However, when using cloves, it can cause respiratory irritation, allergic skin reactions, or affect blood coagulation, so it is recommended to use an appropriate amount depending on the product type.

Accordingly, the present applicant wants to effectively utilize cloves as a material for preventing hair loss, and for this purpose, he studied the amount of cloves suitable for use as a functional soap for preventing hair loss.

Korean Patent No. 10-1796699 Korean Patent No. 10-1511747

In order to solve the above-mentioned problems, the purpose of the present invention is to provide an anti-hair loss functional soap using cloves that can effectively prevent hair loss by using cloves having various properties, and a method for manufacturing the same.

In addition, the purpose of the present invention is to provide a functional soap for preventing hair loss using cloves and a method for manufacturing the same, which can minimize side effects and improve product quality by using an appropriate amount of cloves.

The technical problems to be solved by the invention are not limited to the technical problems mentioned above, and other technical problems not mentioned will be clearly understood by those skilled in the art from the description below. You will be able to.

In order to achieve the above object, one aspect of the present invention is formed by mixing clove powder, oil, purified water, caustic soda, and persimmon vinegar and then saponifying them at 25 to 35° C. for 40 to 50 hours, with respect to 120 parts by weight of the purified water. Providing a functional soap for preventing hair loss using cloves, characterized in that 10 to 20 parts by weight of the clove powder, 780 to 980 parts by weight of the oil, 130 to 170 parts by weight of the caustic soda, and 120 to 160 parts by weight of the persimmon vinegar are mixed. do.

The oil includes patchouli essential oil, peppermint essential oil, coconut oil, bay oil, camellia oil, macadamia oil, castor oil, and sunflower oil.

Based on 120 parts by weight of purified water, 5 to 10 parts by weight of patchouli essential oil, 5 to 10 parts by weight of peppermint essential oil, 450 to 510 parts by weight of coconut oil, 100 to 140 parts by weight of bay oil, 70 to 90 parts by weight of camellia oil, It is characterized by mixing 50 to 60 parts by weight of macadamia oil, 50 to 60 parts by weight of castor oil, and 50 to 70 parts by weight of sunflower oil.

Another aspect of the present invention is a first step of preparing clove powder, oil, purified water, caustic soda, and persimmon vinegar, a second step of mixing the oil and the clove powder to form a first mixture, and adding the above to the purified water. A third step of dissolving caustic soda to form a second mixture, a fourth step of mixing the first mixture, the second mixture and the persimmon vinegar to form a third mixture, and the third mixture at 25 to 35°C. It includes a fifth step of forming a soap composition by saponification for 40 to 50 hours, comprising 10 to 20 parts by weight of the clove powder, 780 to 980 parts by weight of the oil, and 130 to 170 parts by weight of the caustic soda, based on 120 parts by weight of the purified water. A method for producing a functional anti-hair loss soap using cloves is provided, characterized in that the persimmon vinegar is mixed in a ratio of 120 to 160 parts by weight.

After mixing the first mixture, the second mixture, and the persimmon vinegar, the mixture is stirred for 15 to 30 minutes.

As a means of solving the above problem, the present invention can suppress the occurrence of hair loss and promote hair growth through the anti-inflammatory, antibacterial and anti-androgenic properties of clove.

Additionally, the present invention can minimize side effects caused by cloves by using cloves in an appropriate amount.

In addition, the present invention adds various oils along with cloves to harmonize with the unique scent of cloves to improve the quality of the product and further increase the anti-hair loss effect.

The technical effects of the present invention are not limited to those mentioned above, and other technical effects not mentioned will be clearly understood by those skilled in the art from the description below.

Figure 1 is a flow chart showing a method for manufacturing a functional anti-hair loss soap using cloves of the present invention.

Specific details, including the problems to be solved by the present invention, the means for solving the problems, and the effects of the invention, are included in the examples and drawings described below. The advantages and features of the present invention and methods for achieving them will become clear by referring to the embodiments described in detail below along with the accompanying drawings.

In the following, the anti-hair loss functional soap using clove of the present invention and its manufacturing method will be described in detail.

Functional anti-hair loss soap using cloves

One aspect of the present invention provides a functional anti-hair loss soap using clove.

The functional soap for preventing hair loss using cloves is formed by mixing clove powder, oil, purified water, caustic soda and persimmon vinegar and then saponifying at 25 to 35° C. for 40 to 50 hours. The clove powder is added to 120 parts by weight of the purified water. It may be mixed in a ratio of 10 to 20 parts by weight, 780 to 980 parts by weight of the oil, 130 to 170 parts by weight of the caustic soda, and 120 to 160 parts by weight of the persimmon vinegar.

In other words, the functional soap for preventing hair loss using cloves of the present invention may be formed into soap through a saponification reaction when the fatty acid component contained in the oil meets the alkaline component of caustic soda along with clove powder having a hair loss prevention function. At this time, the present invention may provide the optimal mixing ratio of clove powder, oil, and additives for forming soap so as to minimize side effects caused by cloves and implement an effective hair loss prevention function.

In the anti-hair loss functional soap of the present invention, the clove powder refers to dried flower buds of clove trees and powdered into particles of a certain size. The clove powder can be purchased commercially or can be obtained by directly collecting it. The clove powder includes eugenol, acetyl eugenol, chavicol, eugenol salcylate, beta-caryophyllene, and humulene. It is rich in antioxidant ingredients and may have antioxidant, antibacterial, anti-inflammatory and anti-androgenic properties.

In detail, by supplying eugenol to the scalp and hair through the clove powder, the androgen action on hair follicles can be suppressed. The anti-androgen properties of the clove powder may mean reducing the expression of androgen receptors. Therefore, in the case of androgenetic alopecia, the clove powder can prevent hair loss and promote hair growth.

In addition, the antioxidant effect of the clove powder can protect hair roots and hair follicles from oxidative damage, and the clove powder contains fiber, vitamin K, vitamin C, manganese (Mn), potassium (K), Ingredients such as sodium (Na), omega-3, and iodine (I) can effectively prevent hair damage.

In addition, the antibacterial and anti-inflammatory properties of the clove powder can eliminate excessive sebum production, dry scalp, and dandruff caused by fungal infections. In addition, eugenol contained in the clove powder can increase the supply of nutrients to the scalp by facilitating blood flow to the scalp, thereby strengthening hair and further promoting hair growth.

In the anti-hair loss functional soap of the present invention, the oil may include vegetable oil containing vegetable fatty acids. The oil may react with the caustic soda and solidify through a saponification process. In general, saponification refers to the formation of fatty acid salts by combining the ester functional group of a fatty acid with an alkali cation.

Specifically, the oil may include patchouli essential oil, peppermint essential oil, coconut oil, laurel oil, camellia oil, macadamia oil, castor oil, and sunflower oil.

The patchouli essential oil is a vegetable oil collected from the patchouli shrub and has adhesive properties so that it can be easily mixed with other oils. The patchouli essential oil has a rich, sweet grassy, spicy, and woody scent, and can blend well with the strong, spicy scent of clove powder. The patchouli essential oil is known to be effective in regenerating and moisturizing damaged skin, and can be included in the anti-hair loss functional soap of the present invention to regenerate damaged scalp and strengthen hair.

The peppermint essential oil is a vegetable oil collected from peppermint, one of the herbs, and its main ingredient, menthol, has an antibacterial effect. In addition, the peppermint essential oil can accelerate the growth rate of hair during the growth period by increasing blood circulation, and has been reported to increase the overall amount of hair growth by being involved in the number and depth of follicles.

The coconut oil is a vegetable oil collected from coco palm trees and remains in a liquid state above 25°C, but remains in a white solid state at temperatures below that. Accordingly, the coconut oil can maintain the shape of the soap firmly and generate abundant soap bubbles. The coconut oil can supply moisture to the scalp and stabilize the scalp.

The laurel berry oil is a vegetable oil collected from laurel fruits and has a fresh scent unique to laurel. The bay oil is rich in antioxidant components such as curcumin and terpene, and can promote blood circulation in the scalp. In addition, the bay oil contains volatile components, so it can easily remove wastes in pores.

The camellia oil is a vegetable oil collected from camellia flowers and camellia leaves, has a high oleic acid content, is not toxic, and has natural antibacterial and antioxidant properties. In particular, camellia oil has the effect of lowering dihydrotestosterone (DHT), which causes hair loss, and can further improve the functionality of the anti-hair loss functional soap of the present invention.

The macadamia oil is an oil collected from macadamia fruits, known as nuts, and contains a large amount of lipids, fatty acids, tocopherol, and squalene, as well as various nutrients. In addition, the macadamia oil contains palmitoleic acid, which can protect hair from heat damage, and can help improve hair quality and promote hair growth.

The castor oil, also called castor oil, is a vegetable oil collected from castor beans and contains a large amount of retinoic acid, which can increase the stickiness of soap and provide transparency. In addition, the castor oil can increase consumer preference for soap by making soap foam easily and giving soap a moist feel.

The sunflower oil is a vegetable oil collected from sunflower seeds, and is rich in nutrients such as minerals, vitamins, and essential fatty acids, so it can supply nutrients to the scalp and is effective in protecting and moisturizing the scalp. .

As described above, the present invention can suppress the occurrence of scalp troubles and hair loss caused by the use of conventional chemicals by using vegetable oil, a natural material, as the fatty acid constituting soap. In addition, the oil blends harmoniously with the clove powder through its unique scent and ingredients to create an excellent scent and further increase the anti-hair loss effect.

In the anti-hair loss functional soap of the present invention, the deionized water may dilute the caustic soda and function as a solvent for mixing the clove powder and the oil.

In the anti-hair loss functional soap of the present invention, the caustic soda (sodium hydroxide, NaOH) may function as a neutralizing agent for saponification reaction. The caustic soda may react with the oil to increase the viscosity of the oil. As the viscosity of the oil increases with the caustic soda, the binding force becomes stronger, making it possible to produce soap with appropriate hardness. In one embodiment, the caustic soda may be used with a purity of 98%.

In the anti-hair loss functional soap of the present invention, the persimmon vinegar is a vinegar made by fermenting persimmon, and may act as a pH adjuster to neutralize the mild alkalinity of the soap. Additionally, the persimmon vinegar can soften the scalp and add shine to hair.

In the anti-hair loss functional soap of the present invention, the ratio of 10 to 20 parts by weight of the clove powder, 780 to 980 parts by weight of the oil, 130 to 170 parts by weight of the caustic soda, and 120 to 160 parts by weight of the persimmon vinegar with respect to 120 parts by weight of the purified water. It may be a mixture of . More preferably, 12 to 14 parts by weight of the clove powder, 781 to 946 parts by weight of the oil, 135 to 161 parts by weight of the caustic soda, and 129 to 156 parts by weight of the persimmon vinegar are mixed with 120 parts by weight of the purified water. You can.

If the amount of clove powder is less than 10 parts by weight based on 120 parts by weight of purified water, the clove powder is added in such a small amount that it may be difficult to effectively prevent hair loss through the clove powder. Additionally, if the clove powder exceeds 20 parts by weight based on 120 parts by weight of the purified water, side effects or scalp problems may occur due to excessive use of the clove powder.

If the oil is included in less than 780 parts by weight based on 120 parts by weight of the purified water, the oil, which is a major component of soap, may not be sufficiently added and the soap's unique physical properties may not be formed. If the oil is included in excess of 980 parts by weight based on 120 parts by weight of the purified water, the oil content remaining after the saponification reaction increases, and the soap may become soft or easily rancid, resulting in reduced preservability.

If the amount of caustic soda is less than 130 parts by weight based on 120 parts by weight of purified water, the content of caustic soda participating in the saponification reaction with oil is small, so the saponification reaction may not proceed smoothly or the process yield may be lowered. Additionally, if the caustic soda is included in excess of 170 parts by weight based on 120 parts by weight of the purified water, the caustic soda that did not participate in the reaction may remain on the surface of the soap and damage the scalp.

If the persimmon vinegar is included in less than 120 parts by weight based on 120 parts by weight of the purified water, it may be difficult to formulate soap at an appropriate pH. In addition, if the persimmon vinegar is included in excess of 160 parts by weight based on 120 parts by weight of the purified water, the soap may be easily decomposed, and the unique scent of the persimmon vinegar may become stronger, which may affect the quality of the product.

The anti-hair loss functional soap of the present invention may be formed by mixing the clove powder, oil, purified water, caustic soda, and persimmon vinegar, and then saponifying the mixture at 25 to 35° C. for 40 to 50 hours. Specifically, the saponification temperature may be set at a temperature within 10°C higher than room temperature (typically 25°C) to ensure that the saponification reaction occurs smoothly without deterioration of the mixture. The saponification time may be comprised of the time during which the saponification reaction can sufficiently occur at the set saponification temperature. Through this, the mixture of clove powder, oil, purified water, caustic soda, and persimmon vinegar may be formed into soap, which is a fatty acid salt, through a saponification reaction.

In one embodiment, based on 120 parts by weight of purified water, 5 to 10 parts by weight of patchouli essential oil, 5 to 10 parts by weight of peppermint essential oil, 450 to 510 parts by weight of coconut oil, 100 to 140 parts by weight of bay oil, and 70 parts by weight of camellia oil. It may be a mixture of 50 to 90 parts by weight, 50 to 60 parts by weight of macadamia oil, 50 to 60 parts by weight of castor oil, and 50 to 70 parts by weight of sunflower oil.

For 120 parts by weight of purified water, 5 parts by weight of patchouli essential oil, 5 parts by weight of peppermint essential oil, 450 parts by weight of coconut oil, 100 parts by weight of laurel oil, 70 parts by weight of camellia oil, 50 parts by weight of macadamia oil, 50 parts by weight of castor oil. If the amount of oil and sunflower oil is mixed in an amount less than 50 parts by weight, the amount of each oil added is not sufficient, so the nutrients that can help prevent hair loss are reduced and the moisturizing property is lowered, which may reduce hair loss prevention efficiency.

In addition, for 120 parts by weight of purified water, 10 parts by weight of patchouli essential oil, 10 parts by weight of peppermint essential oil, 510 parts by weight of coconut oil, 140 parts by weight of laurel oil, 90 parts by weight of camellia oil, 60 parts by weight of macadamia oil, and castor oil. If the content is mixed with more than 60 parts by weight and 70 parts by weight of sunflower oil, the oil's unique scent does not blend harmoniously with the clove powder and each oil, which lowers the scent and sensory level of the soap as a whole, affecting preference for the product. can give.

As described above, the functional soap for preventing hair loss using cloves of the present invention can effectively prevent hair loss by containing an appropriate amount of clove powder with anti-androgenic, antibacterial and antioxidant properties, and minimizes side effects due to the addition of the clove powder. The reliability of the product can be increased. In addition, by including oils with various effects along with the clove powder, the unique scent of cloves and the scents and effects of the oils can be harmoniously combined, thereby improving the quality of the product.

Manufacturing method of functional anti-hair loss soap using cloves

Another aspect of the present invention provides a method for producing functional anti-hair loss soap using the above-described clove. Accordingly, the method for manufacturing the anti-hair loss functional soap using cloves may refer to the description of the previously described anti-hair loss functional soap using cloves.

Figure 1 is a flow chart showing a method for manufacturing a functional anti-hair loss soap using cloves of the present invention.

As shown in Figure 1, first, in the first step (S10), clove powder, oil, purified water, caustic soda, and persimmon vinegar may be measured and prepared. At this time, each ingredient is measured in a ratio of 10 to 20 parts by weight of the clove powder, 780 to 980 parts by weight of the oil, 130 to 170 parts by weight of the caustic soda, and 120 to 160 parts by weight of the vinegar with respect to 120 parts by weight of the purified water. This may be to prepare.

The clove powder is added to implement the hair loss prevention function, and can be used as a commercially available product or by drying and powdering flower buds directly collected from clove trees.

The oil may be a vegetable oil containing fatty acids as a main ingredient for forming soap. Specifically, the oil may include patchouli essential oil, peppermint essential oil, coconut oil, laurel oil, camellia oil, macadamia oil, castor oil, and sunflower oil.

The purified water is added as a solvent for smooth mixing of other ingredients, and ordinary purified water can be used.

The caustic soda is added to react with the oil and coagulate the oil to form soap, and a commercially available product can be used.

The persimmon vinegar is added to adjust the pH of soap, and any vinegar prepared by fermenting persimmons using a conventional method can be used.

At this time, each ingredient is measured in a ratio of 10 to 20 parts by weight of the clove powder, 780 to 980 parts by weight of the oil, 130 to 170 parts by weight of the caustic soda, and 120 to 160 parts by weight of the vinegar with respect to 120 parts by weight of the purified water. This may be to prepare.

If the amount of clove powder is less than 10 parts by weight based on 120 parts by weight of purified water, it may be difficult to effectively prevent hair loss by adding a small amount of clove powder. Additionally, if the clove powder exceeds 20 parts by weight based on 120 parts by weight of the purified water, side effects may be caused by excessive use of the clove powder.

If the oil is included in less than 780 parts by weight based on 120 parts by weight of purified water, the physical properties of regular soap may not be achieved. If the oil is included in excess of 980 parts by weight based on 120 parts by weight of the purified water, the soap may become soft or rancid due to the remaining oil, which may affect the preservability.

If the amount of caustic soda is less than 130 parts by weight based on 120 parts by weight of purified water, the saponification reaction may not proceed smoothly. Additionally, if the caustic soda is included in excess of 170 parts by weight based on 120 parts by weight of the purified water, the caustic soda remaining on the surface of the soap may damage the skin of the soap user.

If the persimmon vinegar is included in less than 120 parts by weight relative to 120 parts by weight of the purified water, the quality of the product may deteriorate or soap bubbles may not be easily generated because the pH is not adjusted to an appropriate level. Additionally, if the persimmon vinegar is included in excess of 160 parts by weight based on 120 parts by weight of purified water, the soap may be easily decomposed.

Next, in the second step (S20), the oil and the clove powder may be mixed to form a first mixture. That is, the clove powder is mixed with the patchouli essential oil, peppermint essential oil, coconut oil, bay oil, camellia oil, macadamia oil, castor oil, and sunflower oil, prepared by measuring in the first step, to form the first mixture. You can. Mixing may be performed using a typical mixing device such as a hand blender.

In one embodiment, after sufficiently mixing the first mixture, the first mixture may be used after resting for a certain period of time so that the air flowing into the first mixture can naturally escape during the mixing process.

Next, in the third step (S30), the caustic soda may be dissolved in the purified water to form a second mixture. When the caustic soda is dissolved in the purified water, an exothermic reaction may occur and the temperature of the second mixture may increase. Accordingly, the second mixture may be naturally cooled to a temperature of 30 to 40° C. and then the next step may be performed.

Next, in the fourth step (S40), the first mixture, the second mixture, and the persimmon vinegar may be mixed to form a third mixture. That is, the first mixture of the clove powder and the oil, the second mixture of an aqueous caustic soda solution, and persimmon vinegar may all be mixed.

At this time, the first mixture, the second mixture, and the persimmon vinegar may be mixed and stirred for 15 to 30 minutes. Through stirring, the first mixture, the second mixture, and the persimmon vinegar may be uniformly dispersed in the third mixture. Stirring can be performed using a normal stirring device.

Next, in the fifth step (S50), the third mixture may be saponified at 25 to 35°C for 40 to 50 hours to form a soap composition. That is, the saponification reaction between the oil and the caustic soda mixed in the third mixture may sufficiently occur.

At this time, before performing the saponification process in the fifth step, saponification may be performed by pouring the third mixture into a mold of the desired shape. Additionally, depending on the embodiment, the fifth step may be to perform saponification by sealing.

When the third mixture is saponified at a temperature below 25°C, the reaction speed may be slow due to the low saponification temperature, which may delay the process time and may not sufficiently allow the saponification reaction to occur. Additionally, when the third mixture is saponified at a temperature exceeding 35°C, side reactions may be formed due to the high temperature, and the viscosity of the oil, which must be increased due to the saponification reaction, may be affected.

If the third mixture is saponified for less than 40 hours, it may be difficult to produce soap with desired physical properties because the saponification reaction does not occur sufficiently. Additionally, when the third mixture is saponified for a time exceeding 50 hours, the process yield may be lowered due to the increased process time.

As described above, the method for producing anti-hair loss functional soap using cloves of the present invention is to saponify the materials mixed in the third mixture so that the saponification reaction occurs smoothly without deterioration, so that soap with the target physical properties can be easily manufactured. You can. In addition, the method for producing a functional anti-hair loss soap using cloves of the present invention can increase preservability through saponification of the clove powder with preservative components and under appropriate conditions without the use of artificial preservatives.

In the following, an experiment was conducted to demonstrate the anti-hair loss effect according to the amount of clove powder added to the anti-hair loss functional soap using cloves of the present invention and the saponification temperature of the mixture containing clove powder, and the experimental results are described in detail using a table. do.

go. Comparison of hair loss prevention effects of soap according to the amount of clove powder added

In the following experiment, 25 test subjects were asked to wash their hair with soap once a day for 30 days to compare the anti-hair loss effect of the soap according to the amount of clove powder added to the anti-hair loss functional soap using cloves. was to be carried out.

The test subjects were those who currently had hair loss symptoms or were in the process of hair loss and had experience using commercially available anti-hair loss soap or shampoo.

There are a total of 4 evaluation items: very good (5 points), excellent (4 points), average (3 points), not effective (2 points), and not very effective (1 point) for cleaning power, hair loss prevention, and hair growth promotion items. ), and if scalp trouble occurred at least once during the experiment period, it was marked as present (O) or absent (X) in the item whether scalp trouble occurred.

[Example 1]

Example 1 is an anti-hair loss functional soap produced without adding clove powder, based on the method for producing an anti-hair loss functional soap using cloves of the present invention.

[Example 2]

Example 1 is an anti-hair loss functional soap prepared by mixing 5 parts by weight of clove powder with 120 parts by weight of purified water, based on the method for producing an anti-hair loss functional soap using cloves of the present invention.

[Example 3]

Example 1 is an anti-hair loss functional soap prepared by mixing 10 parts by weight of clove powder with 120 parts by weight of purified water, based on the method for producing an anti-hair loss functional soap using cloves of the present invention.

[Example 4]

Example 1 is an anti-hair loss functional soap prepared by mixing 15 parts by weight of clove powder with 120 parts by weight of purified water, based on the method for producing an anti-hair loss functional soap using cloves of the present invention.

[Example 5]

Example 1 is an anti-hair loss functional soap prepared by mixing 20 parts by weight of clove powder with 120 parts by weight of purified water, based on the method for producing an anti-hair loss functional soap using cloves of the present invention.

[Example 6]

Example 1 is an anti-hair loss functional soap prepared by mixing 25 parts by weight of clove powder with 120 parts by weight of purified water, based on the method for producing an anti-hair loss functional soap using cloves of the present invention.

Table 1 below is a table showing the amount of clove powder added to 120 parts by weight of purified water in the anti-hair loss functional soap prepared in Examples 1 to 6 of the present invention.

division Amount of clove powder added Example 1 _ Example 2 5 parts by weight Example 3 10 parts by weight Example 4 15 parts by weight Example 5 20 parts by weight Example 6 25 parts by weight

Table 2 below is a table comparing the hair loss prevention effects of the anti-hair loss functional soaps prepared in Examples 1 to 6 of the present invention.

division Cleansing power Prevent hair loss Hair growth promotion Whether or not a double trouble is created? Example 1 4.31 3.98 3.91 X Example 2 4.44 4.48 4.46 X Example 3 4.75 4.76 4.78 X Example 4 4.80 4.83 4.81 X Example 5 4.81 4.85 4.82 X Example 6 4.81 4.65 4.68 O

As shown in Table 2, as a result of comparing the hair loss prevention effect of the anti-hair loss functional soaps prepared in Examples 1 to 6, the soaps prepared in Examples 3 to 5 showed that the soaps prepared in Examples 3 to 5 did not cause scalp troubles. , the average score of all items was 4.5 or higher, which was higher than that of other examples.

The soap prepared in Example 1 did not cause scalp trouble, but had the lowest evaluation score for preventing hair loss and promoting hair growth, less than 4.0. This can be seen as a result of not adding clove powder, which has a hair loss prevention function.

The soap prepared in Example 2 showed an evaluation score of 4.0 or higher for all items compared to Example 1, but showed an evaluation score for each item compared to Examples 2 to 6. It is believed that the effects of preventing hair loss and promoting hair growth were minimal because not enough clove powder was added.

The soap prepared in Example 6 was rated above 4.5 in all categories of cleaning power, hair loss prevention, and hair growth promotion. However, as the scalp became sensitive during the period of use, more than half of the test subjects developed scalp problems. This can be seen as a result of the addition of a large amount of clove powder, which affected the scalp and caused some side effects.

As described above, it can be confirmed that the anti-hair loss functional soap using clove of the present invention and its manufacturing method have the function of preventing hair loss and promoting hair growth through clove powder, and 10 to 20 parts by weight of clove powder per 120 parts by weight of purified water. It may be desirable to add

you. Comparison of the hair loss prevention effect of soap according to the saponification temperature of the mixture

In the following experiment, 25 test subjects were asked to wash their hair with soap once a day for 30 days to compare the anti-hair loss effect of the soap according to the amount of clove powder added to the anti-hair loss functional soap using cloves. was to be carried out.

The test subjects were those who currently had hair loss symptoms or were in the process of hair loss and had experience using commercially available anti-hair loss soap or shampoo.

There are a total of 4 evaluation items: very good (5 points), excellent (4 points), average (3 points), not effective (2 points), and not very effective (1 point) for cleaning power, hair loss prevention, and hair growth promotion items. ), and if scalp trouble occurred at least once during the experiment period, it was marked as present (O) or absent (X) in the item whether scalp trouble occurred.

[Example 7]

Example 1 is based on the method for producing a functional anti-hair loss soap using cloves of the present invention, adding 15 parts by weight of clove powder to 120 parts by weight of purified water, and saponification was performed at 20° C. for 48 hours in the fifth step. This is a functional soap to prevent hair loss.

[Example 8]

Example 1 is based on the manufacturing method of functional anti-hair loss soap using cloves of the present invention, adding 15 parts by weight of clove powder to 120 parts by weight of purified water, and saponification was performed at 25°C for 48 hours in the fifth step. This is a functional soap to prevent hair loss.

[Example 9]

Example 1 is based on the manufacturing method of functional anti-hair loss soap using cloves of the present invention, 15 parts by weight of clove powder was added to 120 parts by weight of purified water, and saponification was performed at 30° C. for 48 hours in the fifth step. This is a functional soap to prevent hair loss.

[Example 10]

Example 1 is based on the method for producing a functional anti-hair loss soap using cloves of the present invention, adding 15 parts by weight of clove powder to 120 parts by weight of purified water, and saponification was performed at 35°C for 48 hours in the fifth step. This is a functional soap to prevent hair loss.

[Example 11]

Example 1 is based on the method for producing a functional anti-hair loss soap using cloves of the present invention, 15 parts by weight of clove powder was added to 120 parts by weight of purified water, and saponification was performed at 40° C. for 48 hours in the fifth step. This is a functional soap to prevent hair loss.

Table 3 below is a table showing the saponification temperature of the anti-hair loss functional soap prepared in Examples 7 to 11 of the present invention.

division saponification temperature Example 7 20℃ Example 8 25℃ Example 9 30℃ Example 10 35℃ Example 11 40℃

Table 4 below is a table comparing the hair loss prevention effects of the anti-hair loss functional soaps prepared in Examples 7 to 11 of the present invention.

division Cleansing power Prevent hair loss Hair growth promotion Whether or not a double trouble is created? Example 7 4.25 4.31 4.33 X Example 8 4.71 4.73 4.70 X Example 9 4.80 4.83 4.81 X Example 10 4.74 4.76 4.73 X Example 11 4.22 4.28 4.24 X

As shown in Table 4, as a result of evaluating the hair loss prevention effect of the soaps prepared in Examples 7 to 11 of the present invention, the evaluation scores of the soaps prepared in Examples 8, 9, and 10 were The average was 4.5 or higher. This can be seen as a result of the saponification reaction of the mixture containing clove powder being carried out smoothly through saponification at an appropriate temperature, and the clove powder being uniformly distributed and combined.

The overall average score of the soap prepared in Example 7 was less than 4.5, confirming that the anti-hair loss effect was lower than that of Examples 8 to 9. This is because saponification was performed at 20℃, which is lower than room temperature (25℃), so the saponification reaction of the mixture containing clove powder did not occur properly, and the clove powder was not evenly dispersed and combined during the coagulation process, which slightly reduced the anti-hair loss effect. It is judged.

The soap manufactured in Example 11, like Example 7, had scores for each item all below 4.5, which was somewhat lower than that of Example 7. This can be seen as the fact that the physical properties of the soap became softer than those of other examples due to the slightly higher temperature, and the clove powder was not effectively contained in the soap and was lost during the saponification process, lowering the overall hair loss prevention effect.

As described above, the anti-hair loss functional soap using cloves of the present invention and its manufacturing method can further improve the anti-hair loss effect by saponifying a mixture containing clove powder at an appropriate temperature, and the saponification temperature is 25 to 35 ° C. This may be desirable.

As such, a person skilled in the art will understand that the technical configuration of the present invention described above can be implemented in other specific forms without changing the technical idea or essential features of the present invention.

Therefore, the embodiments described above should be understood in all respects as illustrative and not restrictive, and the scope of the present invention is indicated by the claims described later rather than the detailed description above, and the meaning and scope of the claims and their All changes or modified forms derived from the equivalent concept should be construed as falling within the scope of the present invention.

S10. The first step is to measure and prepare clove powder, oil, purified water, caustic soda, and persimmon vinegar.
S20. A second step of mixing the oil and the clove powder to form a first mixture.
S30. A third step of dissolving the caustic soda in the purified water to form a second mixture.
S40. A fourth step of mixing the first mixture, the second mixture, and the persimmon vinegar to form a third mixture.
S50. A fifth step of forming a soap composition by saponifying the third mixture at 25 to 35°C for 40 to 50 hours.

Claims (5)

It is formed by mixing clove powder, oil, purified water, caustic soda and persimmon vinegar and then saponifying at 25 to 35°C for 40 to 50 hours,
Cloves, characterized in that 10 to 20 parts by weight of the clove powder, 780 to 980 parts by weight of the oil, 130 to 170 parts by weight of the caustic soda, and 120 to 160 parts by weight of the persimmon vinegar are mixed with 120 parts by weight of the purified water. Functional soap for preventing hair loss. According to paragraph 1,
The oil is a functional soap for preventing hair loss using cloves, which includes patchouli essential oil, peppermint essential oil, coconut oil, bay oil, camellia oil, macadamia oil, castor oil and sunflower oil. According to paragraph 2,
The oil is,
Based on 120 parts by weight of purified water, 5 to 10 parts by weight of patchouli essential oil, 5 to 10 parts by weight of peppermint essential oil, 450 to 510 parts by weight of coconut oil, 100 to 140 parts by weight of bay oil, 70 to 90 parts by weight of camellia oil, A functional soap for preventing hair loss using cloves, characterized in that it is mixed in a ratio of 50 to 60 parts by weight of macadamia oil, 50 to 60 parts by weight of castor oil, and 50 to 70 parts by weight of sunflower oil. A first step of measuring and preparing clove powder, oil, purified water, caustic soda, and persimmon vinegar;
A second step of mixing the oil and the clove powder to form a first mixture;
A third step of dissolving the caustic soda in the purified water to form a second mixture;
A fourth step of mixing the first mixture, the second mixture, and the persimmon vinegar to form a third mixture; and
A fifth step of forming a soap composition by saponifying the third mixture at 25 to 35° C. for 40 to 50 hours,
Cloves, characterized in that 10 to 20 parts by weight of the clove powder, 780 to 980 parts by weight of the oil, 130 to 170 parts by weight of the caustic soda, and 120 to 160 parts by weight of the persimmon vinegar are mixed with 120 parts by weight of the purified water. Method for manufacturing anti-hair loss functional soap. According to clause 4,
In the fourth step,
A method for producing a functional anti-hair loss soap using cloves, characterized in that the first mixture, the second mixture and the persimmon vinegar are mixed and then stirred for 15 to 30 minutes.