CN108670904A - A kind of coconut oil VC toothpaste and preparation method thereof - Google Patents
A kind of coconut oil VC toothpaste and preparation method thereof Download PDFInfo
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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Abstract
The present invention relates to a kind of coconut oil VC toothpaste and preparation method thereof, the coconut oil VC toothpaste is active ingredient by using calcium bicarbonate, coconut oil, vitamin C, nano silicon dioxide, plant extracts etc. and carries out suitable weight proportion, under the synergistic effect of each raw material component, the coconut oil VC toothpaste being prepared, the oral cavities class disease such as it can reach oral cleaning when cleaning oral cavity but also mitigate and cure gingivitis, periodontitis, it is with obvious effects.In addition, the method for the present invention production cost is low, wide market.
Description
Technical field
The invention belongs to technical field of toothpaste, and in particular to a kind of coconut oil VC toothpaste and preparation method thereof.
Background technology
Hainan coconut is typical tropical agricultural product, and Hainan coconut accounts for 99% or more of national total output, and coconut whole body is
It is precious, it is estimated that a kind more than 300 can be processed at present, and the coconut processing enterprise in Hainan can only process a kind more than 130 at present, perhaps
More byproducts cannot abundant processing and utilization, resource loses in vain.Coconut oil is in our conventional foods uniquely by Medium chain fatty
The grease of acid composition, the long-chain fat molecule of other foods of Medium chain fatty molecular proportion is small, easily digested, dietotherapy coconut
Without employing human body pancreas digestive ferment system, enzyme and hormonal system to body apply the pressure of very little for the digestion of oil.And
Liver is more likely to the fuel source for using medium chain fatty acid as production capacity, and then improves the efficiency of metabolism.
Toothpaste is common cleaning supplies in daily life, there is very long history.Toothpaste can remove dental surface
Film and bacterial plaque, it is non-stimulated to oral mucosa, it is non-toxic, it is particularly significant to cleaning oral cavity, oral health.Currently, with mouth
The kind of the continuous development of chamber cleaning supplies, toothpaste is varied, via the toothpaste of single cleaning action, develops into
The various health-care toothpastes with different function.Occurs the work(of many addition active ingredient of Chinese herbs in toothpaste market at present
Energy property toothpaste, such as pseudo-ginseng toothpaste, shiny pricklyash toothpaste, mica filled polypropylene, but its effect is only rested on to general mouth disease
Prevention on, and the drug resistance that bacterium generates gradually produces inhibiting effect to the pharmacological property of toothpaste, to gingivitis, the teeth such as periodontitis
Disease prevention and cure effect in terms of tooth is very little.
Invention content
In order to solve the above problem of the existing technology, the present invention provides one kind can reaching mouth when cleaning oral cavity
Chamber cleaning can mitigate and cure again the coconut oil VC toothpaste and preparation method thereof of the oral cavities such as gingivitis, periodontitis class disease.
The technical solution adopted in the present invention is：
A kind of coconut oil VC toothpaste, raw material components include：
20~50 parts by weight of calcium bicarbonate, 15~25 parts by weight of coconut oil, 1.5~3 parts by weight of vitamin C, sorbierite 5~
15 parts by weight, 0.5~1 parts by weight of cellulose gum, 0.5~1.5 parts by weight of xanthans, 0.05~0.1 parts by weight of sodium benzoate, coke
0.1~0.2 parts by weight of sodium phosphate, 15~20 parts by weight of nano silicon dioxide, 10~15 parts by weight of plant extracts, deionized water
15-45 parts by weight.
The raw material components of the further preferred coconut oil VC toothpaste include：
The parts by weight of 30~40 parts by weight of calcium bicarbonate, 18~22 parts by weight of coconut oil, Catergen~2.5, sorbierite 8~
12 parts by weight, 0.6~0.8 parts by weight of cellulose gum, 0.8~1.2 parts by weight of xanthans, 0.06~0.08 weight of sodium benzoate
Part, 0.12~0.18 parts by weight of sodium pyrophosphate, 16~18 parts by weight of nano silicon dioxide, 11~13 parts by weight of plant extracts,
Deionized water 20-40 parts by weight.
The raw material components of the further preferred coconut oil VC toothpaste include：
35 parts by weight of calcium bicarbonate, 20 parts by weight of coconut oil, Catergen .2 parts by weight, 10 parts by weight of sorbierite, fiber
0.7 parts by weight of plain glue, 1 parts by weight of xanthans, 0.07 parts by weight of sodium benzoate, 0.15 parts by weight of sodium pyrophosphate, nanometer titanium dioxide
17 parts by weight of silicon, 12 parts by weight of plant extracts, 30 parts by weight of deionized water.
The raw material components of the further preferred coconut oil VC toothpaste further include：0.1~5 parts by weight of glycerine, Mint Essence
0.1~1.5 parts by weight.
The plant extracts includes one or more in houttuynia extract, dried orange peel extracts, Merremia boisiana extract
Mixture.
The preparation method of the houttuynia extract is：By feed liquid 1:20~30 by 60~80% ethyl alcohol of Herba Houttuyniae
In 50~60 DEG C of extracting at constant temperature 18~for 24 hours, filtering is concentrated under reduced pressure into paste in 30~45 DEG C, is dried under vacuum condition, powder
It is broken to get；
The preparation method of the dried orange peel extracts is：Dried orange peel is crushed, the water of 10~15 times of amounts is added, 2~4h is impregnated, adds
Heat boils 2~3h, repeats to decoct 3~5 times, filtering, and merging filtrate is concentrated under reduced pressure, is drying to obtain；
The preparation method of the Merremia boisiana extract is：Golden clock rattan is crushed, the water of 10~15 times of amounts of addition, immersion 2~
2~3h is boiled in 4h, heating, repeats to decoct 3~5 times, filtering, and merging filtrate is concentrated under reduced pressure, is drying to obtain.
The coconut oil is prepared with the following method：
(1) drying and crushing：Coconut meat is smashed, squeezer squeezes out coconut milk, obtains shredded coconut stuffing；By shredded coconut stuffing temperature be -40~-
20~48h is dried in vacuo under the conditions of 60 DEG C, treated that shredded coconut stuffing crushes by vacuum freeze drying；
(2) it digests：The shredded coconut stuffing and water that are handled by step (1) are mixed to prepare the first mixture, in first mixing
Complex enzyme is added in object, 12~48h of enzymolysis is carried out under the conditions of 37~42 DEG C, and the second mixture is made after enzyme deactivation；
The mass ratio of the complex enzyme and first mixture is 1:3~5；
The complex enzyme is cellulase and papain according to mass ratio 1:3~1:6 are mixed to prepare；
(3) centrifugation carries oil：Carrying out centrifugal treating after second mixture is cooled to room temperature, centrifugal speed is 2000~
2500r/min, centrifugation time are 2~8min, and upper layer is made grease, is filtered to remove impurity to get coconut oil.
A method of the coconut oil VC toothpaste is prepared, is included the following steps：
(S1) other components in addition to nano silicon dioxide, plant extracts are added in emulsification pot, are sufficiently mixed
Uniformly, original mixture is formed；
(S2) nano silicon dioxide and plant extracts are added into step (1) described original mixture, in stirring condition
Under be sufficiently mixed uniformly to get coconut oil VC toothpaste.
In step (S2), the stirring is vacuum stirring.
In step (S2), the rate for carrying out the stirring is 1000~2000rpm.
Beneficial effects of the present invention are：
Coconut oil VC toothpaste of the present invention, by using calcium bicarbonate, coconut oil, vitamin C, nanometer titanium dioxide
Silicon, plant extracts etc. are active ingredient and carry out suitable weight proportion and be prepared under the synergistic effect of each raw material component
The coconut oil VC toothpaste arrived can reach oral cleaning when cleaning oral cavity but also mitigate and cure the mouths such as gingivitis, periodontitis
Chamber class disease, it is with obvious effects.In addition, the method for the present invention production cost is low, wide market.
Specific implementation mode
With reference to embodiment, the invention will be further described.
In following example 1g is represented with 1 parts by weight.
Embodiment 1
The present embodiment provides a kind of coconut oil VC toothpaste, raw material components include：
20 parts by weight of calcium bicarbonate, 25 parts by weight of coconut oil, 1.5 parts by weight of vitamin C, 15 parts by weight of sorbierite, fiber
0.5 parts by weight of plain glue, 1.5 parts by weight of xanthans, 0.05 parts by weight of sodium benzoate, 0.2 parts by weight of sodium pyrophosphate, nanometer titanium dioxide
15 parts by weight of silicon, 15 parts by weight of plant extracts, 15 parts by weight of deionized water；
The plant extracts is houttuynia extract, dried orange peel extracts, Merremia boisiana extract according to mass ratio 1:1:1 group
At mixture.
The preparation method of the houttuynia extract is：By feed liquid 1:20 by Herba Houttuyniae with 60% ethyl alcohol in 50 DEG C of perseverances
Temperature extraction for 24 hours, filtering, be concentrated under reduced pressure into paste in 30 DEG C, dried under vacuum condition, crush to get；The dried orange peel extracts
Preparation method be：Dried orange peel is crushed, the water of 10 times of amounts is added, is impregnated for 24 hours, 2h is boiled in heating, repeats to decoct 3 times, filter, closes
And filtrate, it is concentrated under reduced pressure, is drying to obtain；The preparation method of the Merremia boisiana extract is：Golden clock rattan is crushed, 10 times of amounts are added
Water, impregnate 2h, 2h is boiled in heating, repeats to decoct 3 times, filtering, and merging filtrate is concentrated under reduced pressure, is drying to obtain.
Further, the present invention provides a kind of preparation method of the coconut oil, includes the following steps：
(1) drying and crushing：Coconut meat is smashed, squeezer squeezes out coconut milk, obtains shredded coconut stuffing；By shredded coconut stuffing temperature be -40 DEG C
Under the conditions of be dried in vacuo 20h, by vacuum freeze drying, treated that shredded coconut stuffing crushes；
(2) it digests：The shredded coconut stuffing and water that are handled by step (1) are mixed to prepare the first mixture, in first mixing
Complex enzyme is added in object, enzymolysis 48h is carried out under the conditions of 37 DEG C, and the second mixture is made after enzyme deactivation；
The mass ratio of the complex enzyme and first mixture is 1:3；
The complex enzyme is cellulase and papain according to mass ratio 1:3 are mixed to prepare；
(3) centrifugation carries oil：Centrifugal treating, centrifugal speed 2000r/ are carried out after second mixture is cooled to room temperature
Grease is made in min, centrifugation time 2min, upper layer, is filtered to remove impurity to get coconut oil.
Further, the present invention provides a kind of preparation method of the coconut oil, includes the following steps：
(S1) other components in addition to nano silicon dioxide, plant extracts are added in emulsification pot, are sufficiently mixed
Uniformly, original mixture is formed；
(S2) nano silicon dioxide and plant extracts are added into step (1) described original mixture, in vacuum condition
Under, be sufficiently mixed uniformly to get coconut oil VC toothpaste under the mixing speed of 1000rpm.
Embodiment 2
The present embodiment provides a kind of coconut oil VC toothpaste, raw material components include：
50 parts by weight of calcium bicarbonate, 15 parts by weight of coconut oil, 3 parts by weight of vitamin C, 5 parts by weight of sorbierite, cellulose gum
1 parts by weight, 0.5 parts by weight of xanthans, 0.1 parts by weight of sodium benzoate, 0.1 parts by weight of sodium pyrophosphate, 20 weight of nano silicon dioxide
Measure part, 10 parts by weight of plant extracts, 45 parts by weight of deionized water；
The plant extracts is houttuynia extract, dried orange peel extracts, Merremia boisiana extract according to mass ratio 1:1:1 group
At mixture.
The preparation method of the houttuynia extract is：By feed liquid 1:30 by Herba Houttuyniae with 80% ethyl alcohol in 60 DEG C of perseverances
Temperature extraction 18h, filtering, be concentrated under reduced pressure into paste in 45 DEG C, dried under vacuum condition, crush to get；The dried orange peel extracts
Preparation method be：Dried orange peel is crushed, the water of 15 times of amounts is added, impregnates 4h, 3h is boiled in heating, repeats to decoct 5 times, filter, closes
And filtrate, it is concentrated under reduced pressure, is drying to obtain；The preparation method of the Merremia boisiana extract is：Golden clock rattan is crushed, 15 times of amounts are added
Water, impregnate 4h, 3h is boiled in heating, repeats to decoct 5 times, filtering, and merging filtrate is concentrated under reduced pressure, is drying to obtain.
Further, the present invention provides a kind of preparation method of the coconut oil, includes the following steps：
(1) drying and crushing：Coconut meat is smashed, squeezer squeezes out coconut milk, obtains shredded coconut stuffing；By shredded coconut stuffing temperature be -60 DEG C
Under the conditions of be dried in vacuo 48h, by vacuum freeze drying, treated that shredded coconut stuffing crushes；
(2) it digests：The shredded coconut stuffing and water that are handled by step (1) are mixed to prepare the first mixture, in first mixing
Complex enzyme is added in object, enzymolysis 12h is carried out under the conditions of 42 DEG C, and the second mixture is made after enzyme deactivation；
The mass ratio of the complex enzyme and first mixture is 1:5；
The complex enzyme is cellulase and papain according to mass ratio 1:6 are mixed to prepare；
(3) centrifugation carries oil：Centrifugal treating, centrifugal speed 2500r/ are carried out after second mixture is cooled to room temperature
Grease is made in min, centrifugation time 8min, upper layer, is filtered to remove impurity to get coconut oil.
Further, the present invention provides a kind of preparation method of the coconut oil, includes the following steps：
(S1) other components in addition to nano silicon dioxide, plant extracts are added in emulsification pot, are sufficiently mixed
Uniformly, original mixture is formed；
(S2) nano silicon dioxide and plant extracts are added into step (1) described original mixture, in vacuum condition
Under, be sufficiently mixed uniformly to get coconut oil VC toothpaste under the mixing speed of 2000rpm.
Embodiment 3
The present embodiment provides a kind of coconut oil VC toothpaste, raw material components include：
30 parts by weight of calcium bicarbonate, 22 parts by weight of coconut oil, Catergen parts by weight, 12 parts by weight of sorbierite, cellulose
0.6 parts by weight of glue, 1.2 parts by weight of xanthans, 0.06 parts by weight of sodium benzoate, 0.18 parts by weight of sodium pyrophosphate, nanometer titanium dioxide
16 parts by weight of silicon, 13 parts by weight of plant extracts, 0.1 parts by weight of glycerine, 1.5 parts by weight of Mint Essence, 20 weight of deionized water
Part.
The plant extracts is houttuynia extract, dried orange peel extracts, Merremia boisiana extract according to mass ratio 1:1:1 group
At mixture.
The preparation method of the houttuynia extract is：By feed liquid 1:25 by Herba Houttuyniae with 70% ethyl alcohol in 55 DEG C of perseverances
Temperature extraction 21h, filtering, be concentrated under reduced pressure into paste in 36.5 DEG C, dried under vacuum condition, crush to get；The dried orange peel extraction
The preparation method of object is：Dried orange peel is crushed, the water of 12.5 times of amounts is added, impregnates 3h, 2.5h is boiled in heating, repeats to decoct 4 times, mistake
Filter, merging filtrate are concentrated under reduced pressure, are drying to obtain；The preparation method of the Merremia boisiana extract is：Golden clock rattan is crushed, is added
The water of 12.5 times of amounts impregnates 3h, and 2.5h is boiled in heating, repeats to decoct 4 times, filtering, and merging filtrate is concentrated under reduced pressure, is drying to obtain.
Further, the present invention provides a kind of preparation method of the coconut oil, includes the following steps：
(1) drying and crushing：Coconut meat is smashed, squeezer squeezes out coconut milk, obtains shredded coconut stuffing；By shredded coconut stuffing temperature be -50 DEG C
Under the conditions of be dried in vacuo 34h, by vacuum freeze drying, treated that shredded coconut stuffing crushes；
(2) it digests：The shredded coconut stuffing and water that are handled by step (1) are mixed to prepare the first mixture, in first mixing
Complex enzyme is added in object, enzymolysis 30h is carried out under the conditions of 39.5 DEG C, and the second mixture is made after enzyme deactivation；
The mass ratio of the complex enzyme and first mixture is 1:4；
The complex enzyme is cellulase and papain according to mass ratio 1:4.5 being mixed to prepare；
(3) centrifugation carries oil：Centrifugal treating, centrifugal speed 2200r/ are carried out after second mixture is cooled to room temperature
Grease is made in min, centrifugation time 5min, upper layer, is filtered to remove impurity to get coconut oil.
Further, the present invention provides a kind of preparation method of the coconut oil, includes the following steps：
(S1) other components in addition to nano silicon dioxide, plant extracts are added in emulsification pot, are sufficiently mixed
Uniformly, original mixture is formed；
(S2) nano silicon dioxide and plant extracts are added into step (1) described original mixture, in vacuum condition
Under, be sufficiently mixed uniformly to get coconut oil VC toothpaste under the mixing speed of 1500rpm.
Embodiment 4
The present embodiment provides a kind of coconut oil VC toothpaste, raw material components include：
40 parts by weight of calcium bicarbonate, 18 parts by weight of coconut oil, Catergen .5 parts by weight, 8 parts by weight of sorbierite, cellulose
0.8 parts by weight of glue, 0.8 parts by weight of xanthans, 0.08 parts by weight of sodium benzoate, 0.12 parts by weight of sodium pyrophosphate, nanometer titanium dioxide
18 parts by weight of silicon, 11 parts by weight of plant extracts, 5 parts by weight of glycerine, 0.1 parts by weight of Mint Essence, 40 parts by weight of deionized water.
The plant extracts is houttuynia extract, dried orange peel extracts, Merremia boisiana extract according to mass ratio 1:2:1 group
At mixture.
The preparation method of the houttuynia extract is：By feed liquid 1:25 by Herba Houttuyniae with 70% ethyl alcohol in 55 DEG C of perseverances
Temperature extraction 20h, filtering, be concentrated under reduced pressure into paste in 38 DEG C, dried under vacuum condition, crush to get；The dried orange peel extracts
Preparation method be：Dried orange peel is crushed, the water of 12 times of amounts is added, impregnates 3h, 2.5h is boiled in heating, repeats to decoct 4 times, filtering,
Merging filtrate is concentrated under reduced pressure, is drying to obtain；The preparation method of the Merremia boisiana extract is：Golden clock rattan is crushed, is added 12 times
The water of amount impregnates 3h, and 2.5h is boiled in heating, repeats to decoct 4 times, filtering, and merging filtrate is concentrated under reduced pressure, is drying to obtain.
Further, the present invention provides a kind of preparation method of the coconut oil, includes the following steps：
(1) drying and crushing：Coconut meat is smashed, squeezer squeezes out coconut milk, obtains shredded coconut stuffing；By shredded coconut stuffing temperature be -50 DEG C
Under the conditions of be dried in vacuo 36h, by vacuum freeze drying, treated that shredded coconut stuffing crushes；
(2) it digests：The shredded coconut stuffing and water that are handled by step (1) are mixed to prepare the first mixture, in first mixing
Complex enzyme is added in object, enzymolysis 30h is carried out under the conditions of 40 DEG C, and the second mixture is made after enzyme deactivation；
The mass ratio of the complex enzyme and first mixture is 1:4；
The complex enzyme is cellulase and papain according to mass ratio 1:4.5 being mixed to prepare；
(3) centrifugation carries oil：Centrifugal treating, centrifugal speed 2100r/ are carried out after second mixture is cooled to room temperature
Grease is made in min, centrifugation time 5min, upper layer, is filtered to remove impurity to get coconut oil.
Further, the present invention provides a kind of preparation method of the coconut oil, includes the following steps：
(S1) other components in addition to nano silicon dioxide, plant extracts are added in emulsification pot, are sufficiently mixed
Uniformly, original mixture is formed；
(S2) nano silicon dioxide and plant extracts are added into step (1) described original mixture, in vacuum condition
Under, be sufficiently mixed uniformly to get coconut oil VC toothpaste under the mixing speed of 1800rpm.
Embodiment 5
The present embodiment provides a kind of coconut oil VC toothpaste, raw material components include：
35 parts by weight of calcium bicarbonate, 20 parts by weight of coconut oil, Catergen .2 parts by weight, 10 parts by weight of sorbierite, fiber
0.7 parts by weight of plain glue, 1 parts by weight of xanthans, 0.07 parts by weight of sodium benzoate, 0.15 parts by weight of sodium pyrophosphate, nanometer titanium dioxide
17 parts by weight of silicon, 12 parts by weight of plant extracts, 2.5 parts by weight of glycerine, 0.8 parts by weight of Mint Essence, 30 weight of deionized water
Part.
The plant extracts is houttuynia extract, dried orange peel extracts, Merremia boisiana extract according to mass ratio 1:2:2 groups
At mixture.
The preparation method of the houttuynia extract is：By feed liquid 1:25 by Herba Houttuyniae with 70% ethyl alcohol in 55 DEG C of perseverances
Temperature extraction 21h, filtering, be concentrated under reduced pressure into paste in 38 DEG C, dried under vacuum condition, crush to get；The dried orange peel extracts
Preparation method be：Dried orange peel is crushed, the water of 12 times of amounts is added, impregnates 3h, 2.5h is boiled in heating, repeats to decoct 4 times, filtering,
Merging filtrate is concentrated under reduced pressure, is drying to obtain；The preparation method of the Merremia boisiana extract is：Golden clock rattan is crushed, is added 12 times
The water of amount impregnates 2~4h, and 2.5h is boiled in heating, repeats to decoct 4 times, filtering, and merging filtrate is concentrated under reduced pressure, is drying to obtain.
Further, the present invention provides a kind of preparation method of the coconut oil, includes the following steps：
(1) drying and crushing：Coconut meat is smashed, squeezer squeezes out coconut milk, obtains shredded coconut stuffing；By shredded coconut stuffing temperature be -45 DEG C
Under the conditions of be dried in vacuo 36h, by vacuum freeze drying, treated that shredded coconut stuffing crushes；
(2) it digests：The shredded coconut stuffing and water that are handled by step (1) are mixed to prepare the first mixture, in first mixing
Complex enzyme is added in object, enzymolysis 36h is carried out under the conditions of 40 DEG C, and the second mixture is made after enzyme deactivation；
The mass ratio of the complex enzyme and first mixture is 1:4；
The complex enzyme is cellulase and papain according to mass ratio 1:4.5 being mixed to prepare；
(3) centrifugation carries oil：Centrifugal treating, centrifugal speed 2200r/ are carried out after second mixture is cooled to room temperature
Grease is made in min, centrifugation time 5min, upper layer, is filtered to remove impurity to get coconut oil.
Further, the present invention provides a kind of preparation method of the coconut oil, includes the following steps：
(S1) other components in addition to nano silicon dioxide, plant extracts are added in emulsification pot, are sufficiently mixed
Uniformly, original mixture is formed；
(S2) nano silicon dioxide and plant extracts are added into step (1) described original mixture, in vacuum condition
Under, be sufficiently mixed uniformly to get coconut oil VC toothpaste under the mixing speed of 1500rpm.
Experimental example
50 volunteers are chosen, ask it that the toothpaste prepared in the embodiment of the present invention 3 is used to be brushed in morning daily in 15 days
Tooth carries out questionnaire survey after 5 minutes, 15 days to 50 volunteers, asks scale removal, fresh breath and use that it is toothpaste of the present invention
Experience (including fragrance, sugariness etc.) to be evaluated, conclusion is divided into satisfied and dissatisfied, is satisfied with the result such as table of number and satisfaction rate
Shown in 1.
Table 1- coconut oil VC toothpaste usage experiences are evaluated
| Sample | Scale removal | Fresh breath | Use feeling |
| It is satisfied with number | 45 | 48 | 44 |
| Satisfaction rate | 90% | 96% | 88% |
As it can be seen from table 1 the usage experience of coconut oil VC toothpaste of the present invention is preferable, after user experience evaluation compared with
It is high.
Specific case is as follows：
Lee, 33 years old, bleeding gums symptoms last 3 years happened occasionally, and attempts various Chinese herbal toothpastes and brushes teeth, has no result.Make
Improved with bleeding gums symptom after coconut oil VC toothpaste of the present invention 10 days, and adhere to that the toothpaste using the present invention is brushed teeth so far,
Gum not normal condition bleed bottom again.
Zhao, 28 years old, bleeding gums disease continued 7 years, during which frequent occurrence, attempted various traditional Chinese and western medicine toothpaste and brush teeth to be showed no
Improve.After coconut oil VC toothpaste of the present invention 15 days, bleeding gums symptom is improved, and adheres to the tooth using the present invention
Cream is brushed teeth so far, gum not normal condition bleed bottom again.
The present invention is not limited to above-mentioned preferred forms, anyone can show that other are various under the inspiration of the present invention
The product of form, however, make any variation in its shape or structure, it is every that there is skill identical or similar to the present application
Art scheme, is within the scope of the present invention.
Claims (10)
1. a kind of coconut oil VC toothpaste, which is characterized in that raw material components include：
20~50 parts by weight of calcium bicarbonate, 15~25 parts by weight of coconut oil, 1.5~3 parts by weight of vitamin C, 5~15 weight of sorbierite
Measure part, 0.5~1 parts by weight of cellulose gum, 0.5~1.5 parts by weight of xanthans, 0.05~0.1 parts by weight of sodium benzoate, pyrophosphoric acid
0.1~0.2 parts by weight of sodium, 15~20 parts by weight of nano silicon dioxide, 10~15 parts by weight of plant extracts, deionized water 15-
45 parts by weight.
2. coconut oil VC toothpaste according to claim 1, which is characterized in that raw material components include：
The parts by weight of 30~40 parts by weight of calcium bicarbonate, 18~22 parts by weight of coconut oil, Catergen~2.5,8~12 weight of sorbierite
Measure part, 0.6~0.8 parts by weight of cellulose gum, 0.8~1.2 parts by weight of xanthans, 0.06~0.08 parts by weight of sodium benzoate, coke
0.12~0.18 parts by weight of sodium phosphate, 16~18 parts by weight of nano silicon dioxide, 11~13 parts by weight of plant extracts, deionization
Water 20-40 parts by weight.
3. coconut oil VC toothpaste according to claim 1, which is characterized in that raw material components include：
35 parts by weight of calcium bicarbonate, 20 parts by weight of coconut oil, Catergen .2 parts by weight, 10 parts by weight of sorbierite, cellulose gum
0.7 parts by weight, 1 parts by weight of xanthans, 0.07 parts by weight of sodium benzoate, 0.15 parts by weight of sodium pyrophosphate, nano silicon dioxide 17
Parts by weight, 12 parts by weight of plant extracts, 30 parts by weight of deionized water.
4. according to claim 1-3 any one of them coconut oil VC toothpaste, which is characterized in that raw material components further include：Glycerine
0.1~5 parts by weight, 0.1~1.5 parts by weight of Mint Essence.
5. coconut oil VC toothpaste according to claim 1, which is characterized in that the plant extracts includes cordate houttuynia extraction
One or more mixtures in object, dried orange peel extracts, Merremia boisiana extract.
6. coconut oil VC toothpaste according to claim 5, which is characterized in that the preparation method of the houttuynia extract
For：By feed liquid 1:20~30 by Herba Houttuyniae with 60~80% ethyl alcohol in 50~60 DEG C of extracting at constant temperature 18~for 24 hours, filtering, in
30~45 DEG C are concentrated under reduced pressure into paste, are dried under vacuum condition, crush to get；
The preparation method of the dried orange peel extracts is：Dried orange peel is crushed, the water of 10~15 times of amounts is added, impregnates 2~4h, heating is boiled
2~3h is boiled, repeats to decoct 3~5 times, filtering, merging filtrate is concentrated under reduced pressure, is drying to obtain；
The preparation method of the Merremia boisiana extract is：Golden clock rattan is crushed, the water of 10~15 times of amounts is added, 2~4h is impregnated, adds
Heat boils 2~3h, repeats to decoct 3~5 times, filtering, and merging filtrate is concentrated under reduced pressure, is drying to obtain.
7. coconut oil VC toothpaste according to claim 1, which is characterized in that the coconut oil is prepared into the following method
It arrives：
(1) drying and crushing：Coconut meat is smashed, squeezer squeezes out coconut milk, obtains shredded coconut stuffing；By shredded coconut stuffing temperature be -40~-60 DEG C
Under the conditions of be dried in vacuo 20~48h, by vacuum freeze drying, treated that shredded coconut stuffing crushes；
(2) it digests：The shredded coconut stuffing and water that are handled by step (1) are mixed to prepare the first mixture, in first mixture
Complex enzyme is added, 12~48h of enzymolysis is carried out under the conditions of 37~42 DEG C, the second mixture is made after enzyme deactivation；
The mass ratio of the complex enzyme and first mixture is 1:3~5；
The complex enzyme is cellulase and papain according to mass ratio 1:3~1:6 are mixed to prepare；
(3) centrifugation carries oil：Carrying out centrifugal treating after second mixture is cooled to room temperature, centrifugal speed is 2000~
2500r/min, centrifugation time are 2~8min, and upper layer is made grease, is filtered to remove impurity to get coconut oil.
8. a kind of method preparing any one of claim 1-7 coconut oil VC toothpaste, which is characterized in that including walking as follows
Suddenly：
(S1) other components in addition to nano silicon dioxide, plant extracts are added in emulsification pot, are sufficiently mixed uniformly,
Form original mixture；
(S2) nano silicon dioxide and plant extracts are added into step (1) described original mixture, under agitation into
Row is sufficiently mixed uniformly to get coconut oil VC toothpaste.
9. the preparation method of coconut oil VC toothpaste according to claim 8, which is characterized in that described to stir in step (S2)
It mixes to be stirred under vacuum.
10. the preparation method of coconut oil VC toothpaste according to claim 8, which is characterized in that in step (S2), carry out institute
The rate for stating stirring is 1000~2000rpm.
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| CN201810720138.7A CN108670904A (en) | 2018-07-03 | 2018-07-03 | A kind of coconut oil VC toothpaste and preparation method thereof |
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| CN201810720138.7A CN108670904A (en) | 2018-07-03 | 2018-07-03 | A kind of coconut oil VC toothpaste and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110368327A (en) * | 2019-08-14 | 2019-10-25 | 广州益凡医疗器械有限公司 | A kind of plaque removes gel and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105238543A (en) * | 2015-10-30 | 2016-01-13 | 海南大学 | Extraction method for coconut oil |
| CN105853318A (en) * | 2016-06-23 | 2016-08-17 | 桂林亦元生现代生物技术有限公司 | Toothpaste and preparation method thereof |
| CN105997719A (en) * | 2016-07-09 | 2016-10-12 | 青岛大学 | Natural antibacterial toothpaste |
| KR101733916B1 (en) * | 2016-03-30 | 2017-05-08 | 김유수 | Toothpaste comprising natural surface-active agent and the fabrication method the same |
-
2018
- 2018-07-03 CN CN201810720138.7A patent/CN108670904A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105238543A (en) * | 2015-10-30 | 2016-01-13 | 海南大学 | Extraction method for coconut oil |
| KR101733916B1 (en) * | 2016-03-30 | 2017-05-08 | 김유수 | Toothpaste comprising natural surface-active agent and the fabrication method the same |
| CN105853318A (en) * | 2016-06-23 | 2016-08-17 | 桂林亦元生现代生物技术有限公司 | Toothpaste and preparation method thereof |
| CN105997719A (en) * | 2016-07-09 | 2016-10-12 | 青岛大学 | Natural antibacterial toothpaste |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110368327A (en) * | 2019-08-14 | 2019-10-25 | 广州益凡医疗器械有限公司 | A kind of plaque removes gel and preparation method thereof |
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