CN110227056A - A kind of propolis oral cleansing lotion and preparation method thereof - Google Patents
A kind of propolis oral cleansing lotion and preparation method thereof Download PDFInfo
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- CN110227056A CN110227056A CN201910684954.1A CN201910684954A CN110227056A CN 110227056 A CN110227056 A CN 110227056A CN 201910684954 A CN201910684954 A CN 201910684954A CN 110227056 A CN110227056 A CN 110227056A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/362—Polycarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/368—Carboxylic acids; Salts or anhydrides thereof with carboxyl groups directly bound to carbon atoms of aromatic rings
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
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Abstract
The invention discloses a kind of propolis oral cleansing lotions and preparation method thereof, the propolis oral cleansing lotion is prepared by propolis alcohol extract, honey, peppermint alcohol extracting thing, sweetener, acid and preservative, propolis alcohol extract is that propolis is extracted through edible ethanol, then is made into the propolis alcohol extract that propolis mass concentration is 10~20% with edible ethanol;Peppermint alcohol extracting thing is that peppermint extracts to obtain through edible ethanol, is first made into the peppermint alcohol extract that menthol extract quality concentration is 1~10% with distilled water using preceding;Honey, peppermint alcohol extracting thing, sweetener, acid and preservative quality dosage be respectively 5~15%, 1~5%, 10~15%, 5~10% and 0.5~1% of propolis quality dosage in propolis alcohol extract;The pH value of the propolis oral cleansing lotion is 3~8.The oral cleansing lotion is integrally in good taste, nonirritant, can be liked and be received by the majority of consumers.
Description
Technical field
The present invention relates to a kind of propolis oral cleansing lotions and preparation method thereof.
Background technique
Propolis is honeybee herborization resin, is mixed into its glandula secretion, beeswax and pollen etc., is process through chewing
A kind of viscous substance, wherein containing the multiple compounds such as flavones, fatty acid, aromatic acid, alcohol, aldehyde, alkene, terpene, furthermore mineral
Matter rich content.Propolis has effects that following: 1, bactericidal antiphlogistic is antiviral, eliminates pathogenic microorganism.For bacterium, virus, true
Various infection class diseases caused by bacterium, such as tuberculosis, gastritis, bronchitis, skin disease have good effect;2, calm,
Nervous system is repaired, insomnia, menopausal syndrome effect are obvious when sedation.Office Shao's anesthetic effect lining toothache, wound only
Pain effect is pretty good, while repairing nerve, activates nerve cell, can eliminate diarrhea constipation, numbness in hands and feet, skin are fullyed recover from an illness the diseases such as itch;3,
Promote tissue repair effect, Shi Yuqing ulcer, sore, wound effect are rapid.In particular for the elimination of diabetes B lower limb gangrene, even more
Compensate for the blank of modern medicine;4, soften blood vessel, improve blood circulation, reduce blood twist and platelet aggregation, bidirectional modulation
Blood stake, blood pressure, the dry indices of blood lipid;5, liver protection, protect liver, solution liver poison, can be effectively reduced the third paddy and turn atmosphere enzyme;6, enhance body
Anti-tumor capacity;7, free radical is removed, artery sclerosis is stopped by team, the plurality kinds of health care function such as increase immunity of organisms, promotion regeneration
Effect.Flavonoid substances in propolis are one of main actives of propolis, and healthcare function and clinical treatment effect are just gradually
Recognized and paid close attention to by people.
With the improvement of people ' s living standards and the movable increase of social interactions, chewing gum receive people one period
Welcome and use.But whether chewing gum can have an impact to the health of oral cavity and tooth, people produce query.In addition,
Residue after chewing-gum chewing is thrown out without care by people, affects the beauty of environment.Therefore, oral cleansing lotion has obtained people in recent years
Favor.Propolis has clinically been used widely as anti-inflammatory preparation and preparation for callouse mouth disease, propolis mouth
Chamber freshener has been subjected to domestic and international market and the welcome of consumer.But propolis smell is heavier, there is certain stimulation to oral cavity
Effect, part propolis extract is easily adhered in tooth or oral cavity, so as to cause a part of consumer groups in use by
Certain restrictions.Therefore, it is necessary to be adjusted and improve to process recipe.
Summary of the invention
It is nonirritant the technical problem to be solved by the invention is to provide a kind of in good taste, it can be liked by the majority of consumers
Love and the novel propolis oral cleansing lotion received and preparation method thereof.
In order to solve the above technical problems, the present invention discloses a kind of propolis oral cleansing lotion first, the propolis oral cavity fresh and cool
Agent is prepared by propolis alcohol extract, honey, peppermint alcohol extracting thing, sweetener, acid and preservative,
The propolis alcohol extract is that propolis is extracted through edible ethanol, then being made into propolis mass concentration with edible ethanol is 10
~20% propolis alcohol extract;The peppermint alcohol extracting thing is that peppermint extracts to obtain through edible ethanol, using preceding first with distillation
Water is made into the peppermint alcohol extract that menthol extract quality concentration is 1~10%;
The honey, peppermint alcohol extracting thing, sweetener, acid and preservative quality dosage be respectively propolis alcohol extracting
5~15%, 1~5%, 10~15%, 5~10% and the 0.5~1% of propolis quality dosage in liquid;
The pH value of the propolis oral cleansing lotion is 3~8.
Further, the sweetener is glucose, fructose, sucrose, maltose, starch sugar, lactose, stevioside, Radix Glycyrrhizae
The mixing of one or more of acid disodium, tripotassium glycyrrhetate or trisodium glycyrrhetinate.
Further, the acid is citric acid, lactic acid, tartaric acid, malic acid, acetic acid, adipic acid, fumaric acid, lemon
The mixing of one or more of lemon acid sodium or citric acid tri potassium.
Further, the preservative is benzoic acid or sorbic acid.
Further, the honey is commodity honey, i.e. commercial product.
The invention also discloses a kind of preparation method of aforementioned propolis oral cleansing lotion, this method includes
(1), it prepares propolis alcohol extract: propolis and edible ethanol, stirring, in 10~100 DEG C of temperature being added in container
Under, extract 50~100 hours, after filtered, then it is 10~20% spare for being adjusted to propolis mass concentration with edible ethanol;Not
Extracted propolis, contains impurity;
(2), it prepares mint extract: after peppermint crushes, being placed in container and stir, after being extracted 5 hours at a temperature of 30 DEG C,
Filtering, obtains mint extract, then with distilled water to be made into the peppermint extracting solution that mint extract mass concentration is 1~10% spare;
The peppermint directlys adopt natural plants;
(3), propolis alcohol extract, honey, peppermint alcohol extract, sweetener, acid and preservative is weighed in proportion to exist
It is uniformly mixed in container, then with acid tune pH value to 3~8, filters and propolis oral cleansing lotion is made.
Further, edible ethanol mass concentration used is 70% in step (1), the weight of propolis used and the edible ethanol
Amount is than being 1:5~10.
Further, propolis first progress Freezing smashing processing before extraction used in step (1).
Further, edible ethanol mass concentration used is 70% in step (2), the weight of peppermint used and the edible ethanol
Amount is than being 1:1~3.
The present invention extends the extraction time to propolis, is added to acid and sweetener, improves propolis to oral cavity
Irritation.Due to being added to acid, adjusts the pH value of mouthwass with can be convenient, has effectively acted as antisepsis,
The antibacterial effect of the preservatives such as benzoic acid, sorbic acid is increased again.It is whole in good taste, it is nonirritant, it can be by the majority of consumers
Like and receives.
Specific embodiment
Below with reference to embodiment, more specifically the elaboration contents of the present invention.Implementation of the invention is not limited to following reality
Example is applied, the accommodation in any form made to the present invention or changed all should be within the scope of the present invention.
The preparation of 1 propolis alcohol extract of embodiment
50 grams of propolis are taken, is put into after Freezing smashing in 1000 milliliters of flask, the edible second that mass concentration is 70% is added
500 grams of alcohol, 10 DEG C at a temperature of, extract 100 hours, filtering, it is spare to be adjusted to propolis mass concentration 10% with edible ethanol.
The preparation of 2 propolis alcohol extract of embodiment
50 grams of propolis are taken, is put into after Freezing smashing in 1000 milliliters of flask, the edible second that mass concentration is 70% is added
250 grams of alcohol, 30 DEG C at a temperature of, extract 50 hours, filtering, it is spare to be adjusted to propolis mass concentration 20% with edible ethanol.
The preparation of 3 propolis alcohol extract of embodiment
50 grams of propolis are taken, is put into after Freezing smashing in 1000 milliliters of flask, the edible second that mass concentration is 70% is added
300 grams of alcohol, 100 DEG C at a temperature of, extract 60 hours, filtering, it is spare to be adjusted to propolis mass concentration 15% with edible ethanol.
The preparation of 4 propolis alcohol extract of embodiment
50 grams of propolis are taken, is put into after Freezing smashing in 1000 milliliters of flask, the edible second that mass concentration is 70% is added
400 grams of alcohol, 50 DEG C at a temperature of, extract 80 hours, filtering, it is spare to be adjusted to propolis mass concentration 10% with edible ethanol.
The preparation of 5 propolis alcohol extract of embodiment
50 grams of propolis are taken, is put into after Freezing smashing in 3000 milliliters of flask, the edible second that mass concentration is 70% is added
350 grams of alcohol, 80 DEG C at a temperature of, extract 80 hours, filtering, it is spare to be adjusted to propolis mass concentration 14% with edible ethanol.
The preparation of 6 natural plants peppermint alcohol extract of embodiment
Take 50 grams of natural plants peppermint, be put into after crushing in 500 milliliters of flask, be added mass concentration be 70% it is edible
150 grams of ethyl alcohol, 30 DEG C at a temperature of, extract 5 hours, filter to obtain peppermint alcohol extracting thing, be diluted to peppermint alcohol extracting with distilled water
Taking amount of substance concentration is 5% spare.
The preparation of 7 peppermint alcohol extract of embodiment
50 grams of peppermint are taken, is put into after crushing in 500 milliliters of flask, the edible ethanol 50 that mass concentration is 70% is added
Gram, 30 DEG C at a temperature of, extract 5 hours, filter to obtain peppermint alcohol extracting thing, be diluted to menthol extract quality with distilled water
Concentration is 10% spare.
The preparation of 8 peppermint alcohol extract of embodiment
50 grams of peppermint are taken, is put into after crushing in 500 milliliters of flask, the edible ethanol 100 that mass concentration is 70% is added
Gram, 30 DEG C at a temperature of, extract 5 hours, filter to obtain peppermint alcohol extracting thing, be diluted to menthol extract quality with distilled water
Concentration is 1% spare.
The preparation of 9 propolis oral cleansing lotion of embodiment
In the mixing container, propolis alcohol extract 100 gram are added made from embodiment 1, the natural plants peppermint of embodiment 6
10 grams of alcohol extract, 0.5 gram of acid citric acid, 1 gram of sweetener glucose, 0.05 gram of preservative benzoic acid, 1.5 grams of honey,
It in the mixing container at a temperature of 30 DEG C, is stirred, after being 3 with acid tune pH value, filters finished product.
The preparation of 10 propolis oral cleansing lotion of embodiment
In the mixing container, propolis alcohol extract 100 gram are added made from embodiment 1, the natural plants peppermint of embodiment 6
10 grams of alcohol extract, 0.5 gram of acid lactic acid, 1 gram of sweetener fructose, 0.05 gram of preservative benzoic acid, 1.5 grams of honey, mixed
It in conjunction container at a temperature of 30 DEG C, is stirred, after adjusting pH value to be 3, filters finished product.
The preparation of 11 propolis oral cleansing lotion of embodiment
In the mixing container, propolis alcohol extract 100 gram are added made from embodiment 2, the natural plants peppermint of embodiment 6
20 grams of alcohol extract, 0.5 gram of acid citric acid, 1.5 grams of malic acid, 1 gram of sweetener glucose, 1 gram of sucrose, 1 gram of lactose, prevent
0.1 gram of rotten agent benzoic acid, in the mixing container at a temperature of 30 DEG C, is stirred by 1 gram of honey, is separately 5 with acid tune pH value
Afterwards, finished product is filtered.
The preparation of 12 propolis oral cleansing lotion of embodiment
In the mixing container, propolis alcohol extract 100 gram are added made from embodiment 3, the peppermint alcohol extract of embodiment 7
4.5 grams, 0.5 gram of acid tartaric acid, 0.7 gram of citric acid tri potassium, 1 gram of sweetener glucose,Starch sugar0.5 gram, preservative mountain
0.15 gram of pears acid, in the mixing container at a temperature of 30 DEG C, is stirred by 0.75 gram of honey, after being separately 8 with acid tune pH value,
Filter finished product.
The preparation of 13 propolis oral cleansing lotion of embodiment
In the mixing container, propolis alcohol extract 100 gram are added made from embodiment 4, the peppermint alcohol extract of embodiment 8
50 grams, 0.5 gram of acid adipic acid, 1 gram of sweetener stevioside, 0.05 gram of preservative benzoic acid, 1.5 grams of honey, hold in mixing
It in device at a temperature of 30 DEG C, is stirred, after being separately 7 with acid tune pH value, filters finished product.
The preparation of 14 propolis oral cleansing lotion of embodiment
In the mixing container, propolis alcohol extract 100 gram are added made from embodiment 5, the peppermint alcohol extract of embodiment 8
42 grams, 0.26 gram of acid adipic acid, 0.5 gram of citric acid, 0.5 gram of sodium citrate, 0.68 gram of sweetener stevioside, glycyrrhizic acid three
It 1 gram of sodium, 0.07 gram of preservative benzoic acid, 1.4 grams of honey, in the mixing container at a temperature of 30 DEG C, is stirred, separately uses acid
After tune pH value is 7, finished product is filtered.
The preparation of 15 propolis oral cleansing lotion of embodiment
In the mixing container, propolis alcohol extract 100 gram are added made from embodiment 5, the day peppermint alcohol extracting of embodiment 8
42 grams of liquid, 0.26 gram of acid acetic acid, 0.5 gram of citric acid, 0.5 gram of sodium citrate, 0.68 gram of sweetener tripotassium glycyrrhetate, Radix Glycyrrhizae
1 gram of sour trisodium, 1.4 grams of honey, in the mixing container at a temperature of 30 DEG C, is stirred by 0.07 gram of preservative sorbic acid, another acid
After taste agent tune pH value is 6, finished product is filtered.
Claims (9)
1. a kind of propolis oral cleansing lotion, it is characterised in that: the propolis oral cleansing lotion is by propolis alcohol extract, honey, peppermint
Alcohol extracting thing, sweetener, acid and preservative are prepared,
The propolis alcohol extract be propolis extracted through edible ethanol, then with edible ethanol be made into propolis mass concentration be 10~
20% propolis alcohol extract;The peppermint alcohol extracting thing is that peppermint extracts to obtain through edible ethanol, first uses distilled water using preceding
It is made into the peppermint alcohol extract that menthol extract quality concentration is 1~10%;
The honey, peppermint alcohol extracting thing, sweetener, acid and preservative quality dosage be respectively in propolis alcohol extract
5~15%, 1~5%, 10~15%, 5~10% and the 0.5~1% of propolis quality dosage;
The pH value of the propolis oral cleansing lotion is 3~8.
2. propolis oral cleansing lotion according to claim 1, it is characterised in that: the sweetener is glucose, fructose, sugarcane
One or both of sugar, maltose, starch sugar, lactose, stevioside, disodium glycyrrhizinate, tripotassium glycyrrhetate or trisodium glycyrrhetinate
Above mixing.
3. propolis oral cleansing lotion according to claim 1, it is characterised in that: the acid is citric acid, lactic acid, winestone
The mixing of one or more of acid, malic acid, acetic acid, adipic acid, fumaric acid, sodium citrate or citric acid tri potassium.
4. propolis oral cleansing lotion according to claim 1, it is characterised in that: the preservative is benzoic acid or sorbic acid.
5. propolis oral cleansing lotion according to claim 1, it is characterised in that: the honey is commodity honey.
6. a kind of preparation method for preparing claim 1-5 any one claim propolis oral cleansing lotion, it is characterised in that:
This method includes
(1), it prepares propolis alcohol extract: propolis and edible ethanol being added in container, stirring at a temperature of 10~100 DEG C, mentions
Take 50~100 hours, after filtered, then it is 10~20% spare for being adjusted to propolis mass concentration with edible ethanol;
(2), it prepares mint extract: after peppermint crushes, being placed in container and stir, after being extracted 5 hours at a temperature of 30 DEG C, mistake
Filter, obtains mint extract, then with distilled water to be made into the peppermint extracting solution that mint extract mass concentration is 1~10% spare;
(3), propolis alcohol extract, honey, peppermint alcohol extract, sweetener, acid and preservative are weighed in proportion in container
In be uniformly mixed, then with acid tune pH value to 3~8, filter and propolis oral cleansing lotion be made.
7. the preparation method of propolis oral cleansing lotion according to claim 6, it is characterised in that: used edible in step (1)
Ethyl alcohol mass concentration is 70%, and the weight ratio of propolis used and the edible ethanol is 1:5~10.
8. the preparation method of propolis oral cleansing lotion according to claim 6, it is characterised in that: propolis used in step (1)
Freezing smashing processing is first carried out before extraction.
9. the preparation method of propolis oral cleansing lotion according to claim 6, it is characterised in that: used edible in step (2)
Ethyl alcohol mass concentration is 70%, and the weight ratio of peppermint used and the edible ethanol is 1:1~3.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111329930A (en) * | 2020-04-30 | 2020-06-26 | 云南风联科技有限公司 | Plant tobacco-flavored oral cavity atomized liquid and preparation method thereof |
CN112370477A (en) * | 2020-11-03 | 2021-02-19 | 广东启美生物科技有限公司 | Antibacterial oral preparation for refreshing breath, strengthening teeth and protecting gingiva and equipment thereof |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN103610726A (en) * | 2013-11-21 | 2014-03-05 | 江苏江大源生态生物科技有限公司 | Compound propolis oral disinfection spray and preparation method thereof |
CN107875243A (en) * | 2017-11-24 | 2018-04-06 | 张龙兵 | Spray liquid for fresh breath |
CN108464965A (en) * | 2018-06-15 | 2018-08-31 | 沈阳药科大学 | A kind of propolis mouthwash and preparation method thereof containing active skull cap components |
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2019
- 2019-07-26 CN CN201910684954.1A patent/CN110227056A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103610726A (en) * | 2013-11-21 | 2014-03-05 | 江苏江大源生态生物科技有限公司 | Compound propolis oral disinfection spray and preparation method thereof |
CN107875243A (en) * | 2017-11-24 | 2018-04-06 | 张龙兵 | Spray liquid for fresh breath |
CN108464965A (en) * | 2018-06-15 | 2018-08-31 | 沈阳药科大学 | A kind of propolis mouthwash and preparation method thereof containing active skull cap components |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111329930A (en) * | 2020-04-30 | 2020-06-26 | 云南风联科技有限公司 | Plant tobacco-flavored oral cavity atomized liquid and preparation method thereof |
CN112370477A (en) * | 2020-11-03 | 2021-02-19 | 广东启美生物科技有限公司 | Antibacterial oral preparation for refreshing breath, strengthening teeth and protecting gingiva and equipment thereof |
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Application publication date: 20190913 |