CN106983681A - A kind of toothpaste containing natural rubbing agent - Google Patents
A kind of toothpaste containing natural rubbing agent Download PDFInfo
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- CN106983681A CN106983681A CN201710122608.5A CN201710122608A CN106983681A CN 106983681 A CN106983681 A CN 106983681A CN 201710122608 A CN201710122608 A CN 201710122608A CN 106983681 A CN106983681 A CN 106983681A
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- rubbing agent
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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Abstract
The present invention discloses a kind of toothpaste containing natural rubbing agent, wherein natural rubbing agent is to be crushed to broken wall Ultramicro-powder by root of Herba Houttuyniae stem is dry, forms suspension in the mixed liquor for being scattered in sucrose ester and ethanol, adds sodium bicarbonate；Cordate houttuynia rhizome powder is well mixed in deionized water with xanthans, is then added in suspension and stirs, through centrifugal treating, drying, that is, obtain natural rubbing agent.The natural toothpaste abrasives of gained of the invention are to tooth and body fanout free region, it is degradable in the environment, the natural rubbing agent and the difference of conventional friction agent that the present invention is obtained are, after being brushed teeth with the toothpaste of conventional friction agent, enamel surface occurs in that obvious artificial wedge-shaped defect, and toothpaste prepared by the natural rubbing agent of the present invention, because damage of the rubbing agent to tooth is small, the surface change on enamel essence surface is little.
Description
Technical field
The invention belongs to toothpaste abrasives technical field, and in particular to a kind of toothpaste containing natural rubbing agent.
Background technology
The composition of toothpaste mainly include rubbing agent, foaming agent, NMF, thickener, preservative, aromatic, sweetener and
Water.Wherein, rubbing agent is essential a kind of composition in formulation of tooth-paste, typically constitutes from 20~50%.Toothpaste in use,
Rubbing agent in toothpaste is the dirt and coloring matter that dental surface is attached to for removing.Raw material one as toothpaste abrasives
As require that there is appropriate hardness and friction valve, grain fineness is uniform, free from extraneous odour, comfortable taste, safety non-toxic, solubility are small and
Chemical property is stable, is not chemically reacted with the other components in toothpaste.Rubbing agent raw material conventional at present have silica,
Aluminium hydroxide, calcium carbonate etc..
At present, increasing report and investigation find there is the morbidity of people's wedge-shaped erosion of tooth of tooth-brushing habit
Rate is significantly larger than the wedge-shaped defect rate of not toothbrushing person.Research shows, rubbing agent containing excessive high hardness and containing coarse rubbing agent
Toothpaste is to the serious wear of dentine, or even dentine can be caused to expose and allergic reaction is produced.So, using silica,
The toothpaste that the rubbing agents such as aluminium hydroxide, calcium carbonate are made to have the crowd of tooth-brushing habit keeping oral cleaning health and tooth
Certain contradiction is generated between safety.And calcium carbonate, calcium phosphate, sodium metaphosphate, alumina and silica etc., all it is chemistry
Additive, is brushed teeth using the toothpaste of chemical rubbing agent, and not only because a small amount of swallow is harmful to body, it is right in waste water to be discharged into after gargling
Water body environment is polluted, and long-term use can also cause harm to the enamel of tooth, and for example enamel surface occurs substantially
It is artificial carve type defect, cause the generation of the mouth diseases such as gingivitis, carious tooth.
The content of the invention
To solve the above problems, the present invention provides a kind of toothpaste containing natural rubbing agent, the rubbing agent is neither too hard, nor too soft, and right
Human body is harmless.
The present invention is realized by following technical proposal：A kind of toothpaste containing natural rubbing agent, includes the group of following masses part
Point：1~5 part of surfactant, natural 40~50 parts of rubbing agent, 20~30 parts of glycerine, 1~5 part of sodium carboxymethylcellulose, bay
2~3 parts of alcohol sodium sulphate, 1~3 part of saccharin sodium, 0.01~0.1 part of essence；
The natural rubbing agent follows these steps to be made：
It is a, root of Herba Houttuyniae stem is dry, it is crushed to broken wall Ultramicro-powder；
B, step a broken wall Ultramicro-powder is scattered in the mixed liquor of sucrose ester and ethanol by 1~10g/mL forms suspension, will
This suspension is stirred under Ultrasonic Conditions, makes broken wall Ultramicro-powder dispersed in the solution；
C, by suspension obtained by step b under agitation, add sodium bicarbonate to suspension pH value=9~11；
D, cordate houttuynia rhizome powder is dissolved in deionized water with xanthans by 3 ︰ 0.5 mass ratio be well mixed, make the two
Concentration is 0.5~3g/L, obtains mixture；
E, by the mass ratio of suspension and mixture it is（1~3）︰ 1, mixture stirring obtained by step d is added to obtained by step c
In suspension, then persistently stir 2~10 minutes, dried through centrifugal treating, then at 60 DEG C, that is, obtain natural rubbing agent.
The sucrose ester of the step b and the mixed liquor of ethanol be by liquid-solid ratio be 0.5~1 ︰ 1, by sucrose ester in water-bath 40
Mixed liquor of the concentration for gained in 60~80v/v% ethanol is added at~70 DEG C.
The granularity of the cordate houttuynia rhizome powder of the step d is 150~200 mesh.
Advantage and effect that the present invention possesses：The natural rubbing agent of the present invention is crude fibre raw material, gained using cordate houttuynia
Natural rubbing agent hardness and relative friction forces meet the requirement of toothpaste abrasives, the clearing heat and detoxicating and detumescence work(also with cordate houttuynia
Effect；Natural rubbing agent can keep the function of cordate houttuynia for a long time, realize sustained release；The natural rubbing agent can also effectively suppress microorganism life
It is long, the quality of permanent holding toothpaste.The natural toothpaste abrasives of gained of the invention easily drop in the environment to tooth and body fanout free region
Solution, the natural rubbing agent and the difference of conventional friction agent that the present invention is obtained is, after being brushed teeth with the toothpaste of conventional friction agent, tooth enamel
Matter surface occurs in that obvious artificial wedge-shaped defect, and toothpaste prepared by the natural rubbing agent of the present invention, because rubbing agent is to tooth
The damage of tooth is small, and the surface change on enamel essence surface is little.
Embodiment
With reference to embodiment, the present invention will be further described.
Embodiment 1
Toothpaste containing natural rubbing agent, includes the component of following masses part：4 parts of surfactant, natural 45 parts of rubbing agent, glycerine
25 parts, 3 parts of sodium carboxymethylcellulose, 2.5 parts of sldium lauryl sulfate, 2 parts of saccharin sodium, 0.05 part of essence；
The natural rubbing agent follows these steps to be made：
It is a, root of Herba Houttuyniae stem is dry, it is crushed to broken wall Ultramicro-powder；
B, step a broken wall Ultramicro-powder is scattered in the mixed liquor of sucrose ester and ethanol by 8g/mL forms suspension, this is hanged
Turbid liquid is stirred under Ultrasonic Conditions, makes broken wall Ultramicro-powder dispersed in the solution；The sucrose ester of the step b and ethanol
It by liquid-solid ratio is 0.8 ︰ 1 that mixed liquor, which is, sucrose ester is added at 60 DEG C of water-bath concentration in 70v/v% ethanol gained it is mixed
Close liquid；
C, by suspension obtained by step b under agitation, add sodium bicarbonate to suspension pH value=10；
D, granularity is dissolved in deionized water by 3 ︰ 0.5 mass ratio with xanthans and mixed for the cordate houttuynia rhizome powder of 180 mesh
Uniformly, it is 2g/L to make the concentration of the two, obtains mixture；
E, by the mass ratio of suspension and mixture it is 2 ︰ 1, mixture stirring obtained by step d is added to suspended obtained by step c
In liquid, then persistently stir 8 minutes, dried through centrifugal treating, then at 60 DEG C, that is, obtain natural rubbing agent.
Embodiment 2
Toothpaste containing natural rubbing agent, includes the component of following masses part：1 part of surfactant, natural 40 parts of rubbing agent, glycerine
20 parts, 1 part of sodium carboxymethylcellulose, 2 parts of sldium lauryl sulfate, 1 part of saccharin sodium, 0.01 part of essence；
The natural rubbing agent follows these steps to be made：
It is a, root of Herba Houttuyniae stem is dry, it is crushed to broken wall Ultramicro-powder；
B, step a broken wall Ultramicro-powder is scattered in the mixed liquor of sucrose ester and ethanol by 1g/mL forms suspension, this is hanged
Turbid liquid is stirred under Ultrasonic Conditions, makes broken wall Ultramicro-powder dispersed in the solution；The sucrose ester of the step b and ethanol
It by liquid-solid ratio is 0.5 ︰ 1 that mixed liquor, which is, sucrose ester is added at 40 DEG C of water-bath concentration in 60v/v% ethanol gained it is mixed
Close liquid；
C, by suspension obtained by step b under agitation, add sodium bicarbonate to suspension pH value=9；
D, granularity is dissolved in deionized water by 3 ︰ 0.5 mass ratio with xanthans and mixed for the cordate houttuynia rhizome powder of 150 mesh
Uniformly, it is 0.5g/L to make the concentration of the two, obtains mixture；
E, by the mass ratio of suspension and mixture it is 1 ︰ 1, mixture stirring obtained by step d is added to suspended obtained by step c
In liquid, then persistently stir 2 minutes, dried through centrifugal treating, then at 60 DEG C, that is, obtain natural rubbing agent.
Embodiment 3
Toothpaste containing natural rubbing agent, includes the component of following masses part：5 parts of surfactant, natural 50 parts of rubbing agent, glycerine
30 parts, 5 parts of sodium carboxymethylcellulose, 3 parts of sldium lauryl sulfate, 3 parts of saccharin sodium, 0.1 part of essence；
The natural rubbing agent follows these steps to be made：
It is a, root of Herba Houttuyniae stem is dry, it is crushed to broken wall Ultramicro-powder；
B, step a broken wall Ultramicro-powder is scattered in the mixed liquor of sucrose ester and ethanol by 10g/mL forms suspension, by this
Suspension is stirred under Ultrasonic Conditions, makes broken wall Ultramicro-powder dispersed in the solution；The sucrose ester and ethanol of the step b
Mixed liquor be by liquid-solid ratio be 1 ︰ 1, sucrose ester is added at 70 DEG C of water-bath concentration in 80v/v% ethanol gained it is mixed
Close liquid；
C, by suspension obtained by step b under agitation, add sodium bicarbonate to suspension pH value=11；
D, granularity is dissolved in deionized water by 3 ︰ 0.5 mass ratio with xanthans and mixed for the cordate houttuynia rhizome powder of 200 mesh
Uniformly, it is 3g/L to make the concentration of the two, obtains mixture；
E, by the mass ratio of suspension and mixture it is 3 ︰ 1, mixture stirring obtained by step d is added to suspended obtained by step c
In liquid, then persistently stir 10 minutes, dried through centrifugal treating, then at 60 DEG C, that is, obtain natural rubbing agent.
Comparative example 1：Be the same as Example 1, only replaces with calcium carbonate by natural rubbing agent.
Comparative example 2：Be the same as Example 1, only replaces with calcium phosphate dihydrate by natural rubbing agent.
Comparative example 3：Be the same as Example 1, only replaces with sodium metaphosphate by natural rubbing agent.
Comparative example 4：Be the same as Example 1, only replaces with alumina by natural rubbing agent.
Comparative example 5：Be the same as Example 1, only replaces with silica by natural rubbing agent.
| To body detrimental extent | Pollution problem | Influence to enamel | |
| Comparative example 1 | Chemical substance is non-degradable | Dental surface softens | 0.003 |
| Comparative example 2 | Chemical substance is non-degradable | Tooth discoloration | 0.005 |
| Comparative example 3 | Chemical substance is non-degradable | Tooth discoloration and corrosion | 0.021 |
| Comparative example 4 | Chemical substance is non-degradable | Tooth smoothness is reduced | 0.008 |
| Comparative example 5 | Chemical substance is non-degradable | The impaired discoloration of enamel | 0.008 |
| Embodiment 1 | Natural materials are degradable harmless | Without influence | 0.0006 |
Above-mentioned detailed description is illustrating for one of them possible embodiments of the present invention, and the embodiment is simultaneously not used to
The scope of the claims of the present invention is limited, all equivalence enforcements or change without departing from carried out by the present invention are intended to be limited solely by the technology of the present invention
In the range of scheme.
Claims (3)
1. a kind of toothpaste containing natural rubbing agent, it is characterised in that include the component of following masses part：1~5 part of surfactant,
Natural 40~50 parts of rubbing agent, 20~30 parts of glycerine, 1~5 part of sodium carboxymethylcellulose, 2~3 parts of sldium lauryl sulfate, saccharin
1~3 part of sodium, 0.01~0.1 part of essence；
The natural rubbing agent follows these steps to be made：
It is a, root of Herba Houttuyniae stem is dry, it is crushed to broken wall Ultramicro-powder；
B, step a broken wall Ultramicro-powder is scattered in the mixed liquor of sucrose ester and ethanol by 1~10g/mL forms suspension, will
This suspension is stirred under Ultrasonic Conditions, makes broken wall Ultramicro-powder dispersed in the solution；
C, by suspension obtained by step b under agitation, add sodium bicarbonate to suspension pH value=9~11；
D, cordate houttuynia rhizome powder is dissolved in deionized water with xanthans by 3 ︰ 0.5 mass ratio be well mixed, make the two
Concentration is 0.5~3g/L, obtains mixture；
E, by the mass ratio of suspension and mixture it is（1~3）︰ 1, mixture stirring obtained by step d is added to obtained by step c
In suspension, then persistently stir 2~10 minutes, dried through centrifugal treating, then at 60 DEG C, that is, obtain natural rubbing agent.
2. the toothpaste according to claim 1 containing natural rubbing agent, it is characterised in that：The sucrose ester and second of the step b
It by liquid-solid ratio is 0.5~1 ︰ 1 that the mixed liquor of alcohol, which is, and it is 60~80v/v%'s that sucrose ester is added into concentration at 40~70 DEG C of water-bath
The mixed liquor of gained in ethanol.
3. the toothpaste according to claim 1 containing natural rubbing agent, it is characterised in that：The cordate houttuynia rhizome of the step d
The granularity of powder is 150~200 mesh.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710122608.5A CN106983681A (en) | 2017-03-03 | 2017-03-03 | A kind of toothpaste containing natural rubbing agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710122608.5A CN106983681A (en) | 2017-03-03 | 2017-03-03 | A kind of toothpaste containing natural rubbing agent |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106983681A true CN106983681A (en) | 2017-07-28 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710122608.5A Pending CN106983681A (en) | 2017-03-03 | 2017-03-03 | A kind of toothpaste containing natural rubbing agent |
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| Country | Link |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112891240A (en) * | 2021-02-05 | 2021-06-04 | 纳爱斯浙江科技有限公司 | Composition with cleaning power, foam experience, low tooth wear and low irritation to oral mucosa |
| US11304888B2 (en) | 2019-04-29 | 2022-04-19 | Sunstar Americas, Inc. | Oral care composition |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1686076A (en) * | 2005-04-04 | 2005-10-26 | 洪滔 | Houttuynia tooth paste |
| CN104248571A (en) * | 2014-09-19 | 2014-12-31 | 云南七丹药业股份有限公司 | Purely natural plant-containing abradant toothpaste and preparation method thereof |
| CN105640828A (en) * | 2016-01-06 | 2016-06-08 | 名臣健康用品股份有限公司 | Application of durian shell extract in oral care products |
-
2017
- 2017-03-03 CN CN201710122608.5A patent/CN106983681A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1686076A (en) * | 2005-04-04 | 2005-10-26 | 洪滔 | Houttuynia tooth paste |
| CN104248571A (en) * | 2014-09-19 | 2014-12-31 | 云南七丹药业股份有限公司 | Purely natural plant-containing abradant toothpaste and preparation method thereof |
| CN105640828A (en) * | 2016-01-06 | 2016-06-08 | 名臣健康用品股份有限公司 | Application of durian shell extract in oral care products |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US11304888B2 (en) | 2019-04-29 | 2022-04-19 | Sunstar Americas, Inc. | Oral care composition |
| CN112891240A (en) * | 2021-02-05 | 2021-06-04 | 纳爱斯浙江科技有限公司 | Composition with cleaning power, foam experience, low tooth wear and low irritation to oral mucosa |
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Application publication date: 20170728 |