CN104233451B - 利用场与特征对比的tsv浴评估 - Google Patents

利用场与特征对比的tsv浴评估 Download PDF

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Publication number
CN104233451B
CN104233451B CN201410268283.8A CN201410268283A CN104233451B CN 104233451 B CN104233451 B CN 104233451B CN 201410268283 A CN201410268283 A CN 201410268283A CN 104233451 B CN104233451 B CN 104233451B
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electrode
experiment
current density
current
potential
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Chinese (zh)
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CN104233451A (zh
Inventor
里·布罗根
史蒂文·T·迈耶
马修·托鲁
约瑟夫·理查森
大卫·W·波特
傅海英
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Lam Research Corp
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Lam Research Corp
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    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25DPROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D21/00Processes for servicing or operating cells for electrolytic coating
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25DPROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D21/00Processes for servicing or operating cells for electrolytic coating
    • C25D21/12Process control or regulation
    • C25D21/14Controlled addition of electrolyte components
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B41PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
    • B41CPROCESSES FOR THE MANUFACTURE OR REPRODUCTION OF PRINTING SURFACES
    • B41C1/00Forme preparation
    • B41C1/18Curved printing formes or printing cylinders
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25DPROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D21/00Processes for servicing or operating cells for electrolytic coating
    • C25D21/12Process control or regulation
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/26Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating electrochemical variables; by using electrolysis or electrophoresis
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/26Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating electrochemical variables; by using electrolysis or electrophoresis
    • G01N27/403Cells and electrode assemblies
    • G01N27/413Concentration cells using liquid electrolytes measuring currents or voltages in voltaic cells
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/26Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating electrochemical variables; by using electrolysis or electrophoresis
    • G01N27/416Systems
    • HELECTRICITY
    • H05ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05KPRINTED CIRCUITS; CASINGS OR CONSTRUCTIONAL DETAILS OF ELECTRIC APPARATUS; MANUFACTURE OF ASSEMBLAGES OF ELECTRICAL COMPONENTS
    • H05K3/00Apparatus or processes for manufacturing printed circuits
    • H05K3/22Secondary treatment of printed circuits
    • H05K3/24Reinforcing of the conductive pattern
    • H05K3/241Reinforcing of the conductive pattern characterised by the electroplating method; means therefor, e.g. baths or apparatus
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25DPROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D7/00Electroplating characterised by the article coated
    • C25D7/12Semiconductors
    • C25D7/123Semiconductors first coated with a seed layer or a conductive layer

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Molecular Biology (AREA)
  • Immunology (AREA)
  • Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Pathology (AREA)
  • Automation & Control Theory (AREA)
  • Manufacturing & Machinery (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Electroplating Methods And Accessories (AREA)
  • Electrodes Of Semiconductors (AREA)
  • Testing Or Measuring Of Semiconductors Or The Like (AREA)
CN201410268283.8A 2013-06-14 2014-06-16 利用场与特征对比的tsv浴评估 Active CN104233451B (zh)

Priority Applications (1)

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CN201710979575.6A CN107858742B (zh) 2013-06-14 2014-06-16 利用场与特征对比的tsv浴评估

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US201361835418P 2013-06-14 2013-06-14
US61/835,418 2013-06-14
US14/275,750 2014-05-12
US14/275,750 US9689083B2 (en) 2013-06-14 2014-05-12 TSV bath evaluation using field versus feature contrast

Related Child Applications (1)

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CN104233451A CN104233451A (zh) 2014-12-24
CN104233451B true CN104233451B (zh) 2017-11-24

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CN201710979575.6A Active CN107858742B (zh) 2013-06-14 2014-06-16 利用场与特征对比的tsv浴评估

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US (2) US9689083B2 (cg-RX-API-DMAC7.html)
JP (1) JP6433161B2 (cg-RX-API-DMAC7.html)
KR (2) KR102297508B1 (cg-RX-API-DMAC7.html)
CN (2) CN104233451B (cg-RX-API-DMAC7.html)
SG (2) SG10201802369YA (cg-RX-API-DMAC7.html)
TW (1) TWI643980B (cg-RX-API-DMAC7.html)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6170938B2 (ja) 2011-12-12 2017-07-26 ノベラス・システムズ・インコーポレーテッドNovellus Systems Incorporated 電気めっき溶液内のレベラー濃度の監視
US9598787B2 (en) * 2013-03-14 2017-03-21 Rohm And Haas Electronic Materials Llc Method of filling through-holes
US9689083B2 (en) 2013-06-14 2017-06-27 Lam Research Corporation TSV bath evaluation using field versus feature contrast
JP6890375B2 (ja) * 2014-10-21 2021-06-18 株式会社半導体エネルギー研究所 装置
US10094038B2 (en) 2015-04-13 2018-10-09 Lam Research Corporation Monitoring electrolytes during electroplating
CN105018977B (zh) * 2015-07-17 2017-09-12 深圳市板明科技有限公司 一种填孔电镀整平剂、制备方法及应用该整平剂的电镀液
US10508357B2 (en) 2016-02-15 2019-12-17 Rohm And Haas Electronic Materials Llc Method of filling through-holes to reduce voids and other defects
US10512174B2 (en) 2016-02-15 2019-12-17 Rohm And Haas Electronic Materials Llc Method of filling through-holes to reduce voids and other defects
WO2017204019A1 (ja) * 2016-05-27 2017-11-30 公立大学法人大阪府立大学 電気銅めっき液評価システム、電気銅めっき液評価方法および電気銅めっき液評価用チップ
US20180202060A1 (en) * 2017-01-18 2018-07-19 Eci Technology, Inc. Measurement of total accelerator in an electrodeposition solution
US10094035B1 (en) * 2017-10-16 2018-10-09 Lam Research Corporation Convection optimization for mixed feature electroplating
KR102785430B1 (ko) * 2017-11-17 2025-03-21 라시크 아이엔씨. 기재로부터의 프로세스 가스의 저장 및 전달을 위한 방법, 시스템, 및 디바이스
JP6971915B2 (ja) * 2018-06-05 2021-11-24 株式会社荏原製作所 めっき方法、めっき装置、及び限界電流密度を推定する方法
US10903050B2 (en) 2018-12-10 2021-01-26 Lam Research Corporation Endpoint sensor based control including adjustment of an edge ring parameter for each substrate processed to maintain etch rate uniformity
CN114514340B (zh) * 2019-07-26 2025-03-21 朗姆研究公司 先进封装应用的差别对比镀覆
US12305307B2 (en) 2020-01-10 2025-05-20 Lam Research Corporation TSV process window and fill performance enhancement by long pulsing and ramping
CN113311032B (zh) * 2020-02-27 2024-05-31 芯恩(青岛)集成电路有限公司 Ecp填充监测设备及监测方法

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5196096A (en) * 1992-03-24 1993-03-23 International Business Machines Corporation Method for analyzing the addition agents in solutions for electroplating of PbSn alloys
JP2001152398A (ja) * 1999-08-05 2001-06-05 Fujitsu Ltd 電気めっき方法、めっき液評価方法、めっき装置、半導体装置の製造方法
JP2004217997A (ja) * 2003-01-14 2004-08-05 Fujitsu Ltd 電解めっき成長の添加剤固有特性の評価装置、電解めっき方法、及び半導体装置の製造方法
JP2005171347A (ja) * 2003-12-12 2005-06-30 Shinko Electric Ind Co Ltd 電解銅めっき液の管理方法
CN1764746A (zh) * 2003-03-25 2006-04-26 凸版印刷株式会社 电镀铜液的分析方法、其分析装置和半导体产品的制造方法
CN1957115A (zh) * 2004-05-25 2007-05-02 应用材料公司 用于电镀浴化学剂控制的方法
CN102097347A (zh) * 2009-11-13 2011-06-15 瑞萨电子株式会社 半导体集成电路器件的制造方法
CN103014823A (zh) * 2013-01-05 2013-04-03 江苏物联网研究发展中心 改进铜电沉积的添加剂效果快速判定方法
CN103035503A (zh) * 2011-09-29 2013-04-10 瑞萨电子株式会社 一种制造半导体器件的方法

Family Cites Families (53)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA988879A (en) 1972-11-06 1976-05-11 Cominco Ltd. Electrolytic lead refining
US4324621A (en) 1979-12-26 1982-04-13 Cominco Ltd. Method and apparatus for controlling the quality of electrolytes
US4479852A (en) * 1983-01-21 1984-10-30 International Business Machines Corporation Method for determination of concentration of organic additive in plating bath
US5223118A (en) 1991-03-08 1993-06-29 Shipley Company Inc. Method for analyzing organic additives in an electroplating bath
CN1059475C (zh) * 1996-12-29 2000-12-13 中南工业大学 金属电积过程中在线控制有机添加剂的方法和装置
US7531079B1 (en) 1998-10-26 2009-05-12 Novellus Systems, Inc. Method and apparatus for uniform electropolishing of damascene IC structures by selective agitation
US7449098B1 (en) 1999-10-05 2008-11-11 Novellus Systems, Inc. Method for planar electroplating
JP3897936B2 (ja) 1999-08-31 2007-03-28 株式会社荏原製作所 硫酸銅めっき液中のレベラー濃度測定方法
EP1136595A4 (en) 1999-08-30 2006-07-19 Ebara Corp METHOD FOR MEASURING THE DIRECT CONCENTRATION OF COATING SOLUTIONS AND METHOD AND DEVICE FOR CONTROLLING COATING SOLUTIONS
JP2001073200A (ja) 1999-08-30 2001-03-21 Ebara Corp めっき液管理方法及び管理装置
US6243615B1 (en) * 1999-09-09 2001-06-05 Aegis Analytical Corporation System for analyzing and improving pharmaceutical and other capital-intensive manufacturing processes
US6280602B1 (en) 1999-10-20 2001-08-28 Advanced Technology Materials, Inc. Method and apparatus for determination of additives in metal plating baths
EP1132500A3 (en) * 2000-03-08 2002-01-23 Applied Materials, Inc. Method for electrochemical deposition of metal using modulated waveforms
US6740220B1 (en) 2000-07-28 2004-05-25 The United States Of America As Represented By The Secretary Of The Navy Electrocatalytic cathode device of palladium and iridium on a high density or porous carbon support and a method for making such a cathode
US6645364B2 (en) 2000-10-20 2003-11-11 Shipley Company, L.L.C. Electroplating bath control
DE60113214T2 (de) 2000-11-02 2006-06-08 Shipley Co., L.L.C., Marlborough Plattierungsbadanalyse
US6458262B1 (en) 2001-03-09 2002-10-01 Novellus Systems, Inc. Electroplating chemistry on-line monitoring and control system
US6740221B2 (en) 2001-03-15 2004-05-25 Applied Materials Inc. Method of forming copper interconnects
US20040046121A1 (en) 2001-07-15 2004-03-11 Golden Josh H. Method and system for analyte determination in metal plating baths
US6936157B2 (en) 2001-08-09 2005-08-30 Advanced Technology Materials, Inc. Interference correction of additives concentration measurements in metal electroplating solutions
GB2379977B (en) 2001-09-25 2005-04-06 Kidde Plc High sensitivity particle detection
US6572753B2 (en) 2001-10-01 2003-06-03 Eci Technology, Inc. Method for analysis of three organic additives in an acid copper plating bath
JP2003129298A (ja) * 2001-10-17 2003-05-08 Matsushita Electric Ind Co Ltd メッキ液評価装置、メッキ液評価方法、電子デバイスの製造装置及び電子デバイスの製造方法
US6733656B2 (en) * 2002-04-03 2004-05-11 Eci Technology Inc. Voltammetric reference electrode calibration
US7144488B2 (en) 2002-06-05 2006-12-05 Shipley Company, L.L.C. Electrode, electrochemical cell, and method for analysis of electroplating baths
EP1540046A4 (en) 2002-07-19 2007-04-04 Technic PROCESS AND DEVICE AT REAL TIME MONITORING OF TECHNICAL ELECTROLYTES
US7799200B1 (en) 2002-07-29 2010-09-21 Novellus Systems, Inc. Selective electrochemical accelerator removal
US7405163B1 (en) 2003-12-17 2008-07-29 Novellus Systems, Inc. Selectively accelerated plating of metal features
US7449099B1 (en) 2004-04-13 2008-11-11 Novellus Systems, Inc. Selectively accelerated plating of metal features
US6749739B2 (en) 2002-10-07 2004-06-15 Eci Technology, Inc. Detection of suppressor breakdown contaminants in a plating bath
JP4534983B2 (ja) * 2003-03-25 2010-09-01 凸版印刷株式会社 電気銅めっき液の分析方法、その分析装置
JP2004323971A (ja) 2003-04-25 2004-11-18 Rohm & Haas Electronic Materials Llc 改良された浴分析
JP2005148011A (ja) 2003-11-19 2005-06-09 Ebara Corp 硫酸銅めっき液の有機添加剤濃度の測定方法及び測定装置
US7435320B2 (en) 2004-04-30 2008-10-14 Advanced Technology Materials, Inc. Methods and apparatuses for monitoring organic additives in electrochemical deposition solutions
US7291253B2 (en) * 2004-05-04 2007-11-06 Eci Technology, Inc. Detection of an unstable additive breakdown product in a plating bath
US7186326B2 (en) 2004-05-27 2007-03-06 Eci Technology, Inc. Efficient analysis of organic additives in an acid copper plating bath
US7232513B1 (en) 2004-06-29 2007-06-19 Novellus Systems, Inc. Electroplating bath containing wetting agent for defect reduction
KR20060074593A (ko) 2004-12-27 2006-07-03 동부일렉트로닉스 주식회사 반도체 소자의 농도적정 모니터링 장치 및 그 방법
WO2006110437A1 (en) 2005-04-08 2006-10-19 The Trustees Of Columbia University In The City Of New York Systems and methods for monitoring plating and etching baths
CN2828067Y (zh) 2005-06-09 2006-10-18 福州大学 电镀液中添加剂浓度的实时监测装置
US7662981B2 (en) 2005-07-16 2010-02-16 Rohm And Haas Electronic Materials Llc Leveler compounds
CN100529750C (zh) 2006-01-17 2009-08-19 欧恩吉亚洲股份有限公司 电镀铜加速剂浓度分析方法及其沉积电解液
CN101004402A (zh) * 2006-01-18 2007-07-25 伊希特化股份有限公司 监控铜电镀液填孔能力的方法
US20070215490A1 (en) * 2006-03-18 2007-09-20 Rockwood Electrochemicals Asia Ltd. Method of analyzing accelerator for copper electroplating
US8500985B2 (en) 2006-07-21 2013-08-06 Novellus Systems, Inc. Photoresist-free metal deposition
US7879222B2 (en) 2007-08-27 2011-02-01 Eci Technology, Inc. Detection of additive breakdown products in acid copper plating baths
US7776741B2 (en) 2008-08-18 2010-08-17 Novellus Systems, Inc. Process for through silicon via filing
KR101274363B1 (ko) 2009-05-27 2013-06-13 노벨러스 시스템즈, 인코포레이티드 얇은 시드층 상의 도금을 위한 펄스 시퀀스
US8372258B2 (en) * 2009-08-03 2013-02-12 Novellus Systems, Inc. Monitoring of electroplating additives
US8535504B2 (en) * 2010-05-03 2013-09-17 Eci Technology, Inc. Analysis of an auxiliary leveler additive in an acid copper plating bath
CN102286760B (zh) 2010-05-19 2016-10-05 诺发系统有限公司 用金属电化学填充高纵横比的大型凹入特征的方法、水溶液电镀槽溶液、电镀设备以及系统
JP6170938B2 (ja) 2011-12-12 2017-07-26 ノベラス・システムズ・インコーポレーテッドNovellus Systems Incorporated 電気めっき溶液内のレベラー濃度の監視
US9689083B2 (en) 2013-06-14 2017-06-27 Lam Research Corporation TSV bath evaluation using field versus feature contrast

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5196096A (en) * 1992-03-24 1993-03-23 International Business Machines Corporation Method for analyzing the addition agents in solutions for electroplating of PbSn alloys
JP2001152398A (ja) * 1999-08-05 2001-06-05 Fujitsu Ltd 電気めっき方法、めっき液評価方法、めっき装置、半導体装置の製造方法
JP2004217997A (ja) * 2003-01-14 2004-08-05 Fujitsu Ltd 電解めっき成長の添加剤固有特性の評価装置、電解めっき方法、及び半導体装置の製造方法
CN1764746A (zh) * 2003-03-25 2006-04-26 凸版印刷株式会社 电镀铜液的分析方法、其分析装置和半导体产品的制造方法
JP2005171347A (ja) * 2003-12-12 2005-06-30 Shinko Electric Ind Co Ltd 電解銅めっき液の管理方法
CN1957115A (zh) * 2004-05-25 2007-05-02 应用材料公司 用于电镀浴化学剂控制的方法
CN102097347A (zh) * 2009-11-13 2011-06-15 瑞萨电子株式会社 半导体集成电路器件的制造方法
CN103035503A (zh) * 2011-09-29 2013-04-10 瑞萨电子株式会社 一种制造半导体器件的方法
CN103014823A (zh) * 2013-01-05 2013-04-03 江苏物联网研究发展中心 改进铜电沉积的添加剂效果快速判定方法

Also Published As

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KR102297508B1 (ko) 2021-09-02
US9689083B2 (en) 2017-06-27
US20140367279A1 (en) 2014-12-18
KR20140146015A (ko) 2014-12-24
SG10201802369YA (en) 2018-04-27
TW201510293A (zh) 2015-03-16
CN104233451A (zh) 2014-12-24
KR20210110787A (ko) 2021-09-09
SG10201402383QA (en) 2015-01-29
US20170241041A1 (en) 2017-08-24
KR102335508B1 (ko) 2021-12-06
US10508359B2 (en) 2019-12-17
JP2015001523A (ja) 2015-01-05
TWI643980B (zh) 2018-12-11
CN107858742B (zh) 2020-06-23
JP6433161B2 (ja) 2018-12-05
CN107858742A (zh) 2018-03-30

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