CN102276796B - 镀液及镀覆方法 - Google Patents
镀液及镀覆方法 Download PDFInfo
- Publication number
- CN102276796B CN102276796B CN2011101213393A CN201110121339A CN102276796B CN 102276796 B CN102276796 B CN 102276796B CN 2011101213393 A CN2011101213393 A CN 2011101213393A CN 201110121339 A CN201110121339 A CN 201110121339A CN 102276796 B CN102276796 B CN 102276796B
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- CN
- China
- Prior art keywords
- copper
- alkyl
- present
- copper electroplating
- electroplating liquid
- Prior art date
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
- C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
- C07D295/08—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms
- C07D295/084—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms with the ring nitrogen atoms and the oxygen or sulfur atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings
- C07D295/088—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly bound oxygen or sulfur atoms with the ring nitrogen atoms and the oxygen or sulfur atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings to an acyclic saturated chain
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
- C07D233/02—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having no double bonds between ring members or between ring members and non-ring members
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
- C07D233/54—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members
- C07D233/56—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, attached to ring carbon atoms
- C07D233/60—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, attached to ring carbon atoms with hydrocarbon radicals, substituted by oxygen or sulfur atoms, attached to ring nitrogen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
- C07D295/04—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms
- C07D295/12—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms
- C07D295/125—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms with the ring nitrogen atoms and the substituent nitrogen atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings
- C07D295/13—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with substituted hydrocarbon radicals attached to ring nitrogen atoms substituted by singly or doubly bound nitrogen atoms with the ring nitrogen atoms and the substituent nitrogen atoms attached to the same carbon chain, which is not interrupted by carbocyclic rings to an acyclic saturated chain
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D333/00—Heterocyclic compounds containing five-membered rings having one sulfur atom as the only ring hetero atom
- C07D333/02—Heterocyclic compounds containing five-membered rings having one sulfur atom as the only ring hetero atom not condensed with other rings
- C07D333/04—Heterocyclic compounds containing five-membered rings having one sulfur atom as the only ring hetero atom not condensed with other rings not substituted on the ring sulphur atom
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D3/00—Electroplating: Baths therefor
- C25D3/02—Electroplating: Baths therefor from solutions
- C25D3/38—Electroplating: Baths therefor from solutions of copper
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05K—PRINTED CIRCUITS; CASINGS OR CONSTRUCTIONAL DETAILS OF ELECTRIC APPARATUS; MANUFACTURE OF ASSEMBLAGES OF ELECTRICAL COMPONENTS
- H05K3/00—Apparatus or processes for manufacturing printed circuits
- H05K3/40—Forming printed elements for providing electric connections to or between printed circuits
- H05K3/42—Plated through-holes or plated via connections
- H05K3/423—Plated through-holes or plated via connections characterised by electroplating method
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05K—PRINTED CIRCUITS; CASINGS OR CONSTRUCTIONAL DETAILS OF ELECTRIC APPARATUS; MANUFACTURE OF ASSEMBLAGES OF ELECTRICAL COMPONENTS
- H05K3/00—Apparatus or processes for manufacturing printed circuits
- H05K3/40—Forming printed elements for providing electric connections to or between printed circuits
- H05K3/42—Plated through-holes or plated via connections
- H05K3/421—Blind plated via connections
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Electroplating And Plating Baths Therefor (AREA)
- Electroplating Methods And Accessories (AREA)
- Manufacturing Of Printed Wiring (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US12/661,312 US8268157B2 (en) | 2010-03-15 | 2010-03-15 | Plating bath and method |
| US12/661,312 | 2010-03-15 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102276796A CN102276796A (zh) | 2011-12-14 |
| CN102276796B true CN102276796B (zh) | 2013-04-24 |
Family
ID=43984121
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2011101213393A Active CN102276796B (zh) | 2010-03-15 | 2011-03-15 | 镀液及镀覆方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US8268157B2 (https=) |
| EP (1) | EP2366686B1 (https=) |
| JP (3) | JP2011207878A (https=) |
| KR (1) | KR101739417B1 (https=) |
| CN (1) | CN102276796B (https=) |
| TW (1) | TWI428329B (https=) |
Families Citing this family (54)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20110220512A1 (en) * | 2010-03-15 | 2011-09-15 | Rohm And Haas Electronic Materials Llc | Plating bath and method |
| US8262895B2 (en) * | 2010-03-15 | 2012-09-11 | Rohm And Haas Electronic Materials Llc | Plating bath and method |
| WO2011135716A1 (ja) * | 2010-04-30 | 2011-11-03 | 荏原ユージライト株式会社 | 新規化合物およびその利用 |
| US8454815B2 (en) * | 2011-10-24 | 2013-06-04 | Rohm And Haas Electronics Materials Llc | Plating bath and method |
| JP5952093B2 (ja) | 2012-05-31 | 2016-07-13 | ローム・アンド・ハース電子材料株式会社 | 電解銅めっき液及び電解銅めっき方法 |
| US10405422B2 (en) | 2012-07-09 | 2019-09-03 | Shikoku Chemicals Corporation | Copper film-forming agent and method for forming copper film |
| CN103400906B (zh) * | 2012-08-28 | 2015-11-25 | 夏洋 | 一种晶硅太阳能电池栅线的仿生制备方法 |
| CN105229095A (zh) * | 2012-12-14 | 2016-01-06 | 蓝立方知识产权有限责任公司 | 高含固量环氧树脂涂料 |
| KR20140092626A (ko) | 2013-01-16 | 2014-07-24 | 삼성전자주식회사 | 구리 전해 도금액, 구리 도금 장치 및 이를 이용한 구리 범프 형성 방법 |
| US20140238868A1 (en) | 2013-02-25 | 2014-08-28 | Dow Global Technologies Llc | Electroplating bath |
| US9598787B2 (en) | 2013-03-14 | 2017-03-21 | Rohm And Haas Electronic Materials Llc | Method of filling through-holes |
| JP6211185B2 (ja) | 2013-11-06 | 2017-10-11 | ローム アンド ハース エレクトロニック マテリアルズ エルエルシーRohm and Haas Electronic Materials LLC | レベラーとしての窒素含有ポリマー |
| US9403762B2 (en) * | 2013-11-21 | 2016-08-02 | Rohm And Haas Electronic Materials Llc | Reaction products of guanidine compounds or salts thereof, polyepoxides and polyhalogens |
| US9783903B2 (en) * | 2013-12-06 | 2017-10-10 | Rohm And Haas Electronic Materials Llc | Additives for electroplating baths |
| DE102013226297B3 (de) * | 2013-12-17 | 2015-03-26 | Umicore Galvanotechnik Gmbh | Wässriger, cyanidfreier Elektrolyt für die Abscheidung von Kupfer-Zinn- und Kupfer-Zinn-Zink-Legierungen aus einem Elektrolyten und Verfahren zur elektrolytischen Abscheidung dieser Legierungen |
| US9273407B2 (en) * | 2014-03-17 | 2016-03-01 | Hong Kong Applied Science and Technology Research Institute Company Limited | Additive for electrodeposition |
| US9439294B2 (en) | 2014-04-16 | 2016-09-06 | Rohm And Haas Electronic Materials Llc | Reaction products of heterocyclic nitrogen compounds polyepoxides and polyhalogens |
| KR102301625B1 (ko) * | 2014-04-25 | 2021-09-10 | 가부시끼가이샤 제이씨유 | 동의 고속 충전 방법 |
| US9809891B2 (en) | 2014-06-30 | 2017-11-07 | Rohm And Haas Electronic Materials Llc | Plating method |
| US9783905B2 (en) | 2014-12-30 | 2017-10-10 | Rohm and Haas Electronic Mateirals LLC | Reaction products of amino acids and epoxies |
| US9611560B2 (en) * | 2014-12-30 | 2017-04-04 | Rohm And Haas Electronic Materials Llc | Sulfonamide based polymers for copper electroplating |
| US9725816B2 (en) | 2014-12-30 | 2017-08-08 | Rohm And Haas Electronic Materials Llc | Amino sulfonic acid based polymers for copper electroplating |
| KR102426521B1 (ko) | 2015-04-20 | 2022-07-27 | 아토테크 도이칠란트 게엠베하 운트 콤파니 카게 | 전해 구리 도금 배쓰 조성물 및 그 사용 방법 |
| CN105018977B (zh) * | 2015-07-17 | 2017-09-12 | 深圳市板明科技有限公司 | 一种填孔电镀整平剂、制备方法及应用该整平剂的电镀液 |
| CN105002527B (zh) * | 2015-07-31 | 2017-06-16 | 广东光华科技股份有限公司 | 整平剂溶液及其制备方法和应用 |
| TWI608132B (zh) * | 2015-08-06 | 2017-12-11 | 羅門哈斯電子材料有限公司 | 自含有吡啶基烷基胺及雙環氧化物之反應產物的銅電鍍覆浴液電鍍覆光阻劑限定之特徵的方法 |
| US9932684B2 (en) | 2015-08-06 | 2018-04-03 | Rohm And Haas Electronic Materials Llc | Method of electroplating photoresist defined features from copper electroplating baths containing reaction products of alpha amino acids and bisepoxides |
| US10006136B2 (en) | 2015-08-06 | 2018-06-26 | Dow Global Technologies Llc | Method of electroplating photoresist defined features from copper electroplating baths containing reaction products of imidazole compounds, bisepoxides and halobenzyl compounds |
| US10100421B2 (en) * | 2015-08-06 | 2018-10-16 | Dow Global Technologies Llc | Method of electroplating photoresist defined features from copper electroplating baths containing reaction products of imidazole and bisepoxide compounds |
| US10738388B2 (en) * | 2015-10-08 | 2020-08-11 | Rohm And Haas Electronic Materials Llc | Copper electroplating baths containing compounds of reaction products of amines and polyacrylamides |
| CN117845289A (zh) * | 2015-10-08 | 2024-04-09 | 罗门哈斯电子材料有限责任公司 | 含有胺、聚丙烯酰胺和双环氧化物的反应产物的铜电镀浴 |
| US10988852B2 (en) | 2015-10-27 | 2021-04-27 | Rohm And Haas Electronic Materials Llc | Method of electroplating copper into a via on a substrate from an acid copper electroplating bath |
| US10519557B2 (en) * | 2016-02-12 | 2019-12-31 | Macdermid Enthone Inc. | Leveler compositions for use in copper deposition in manufacture of microelectronics |
| US10508357B2 (en) | 2016-02-15 | 2019-12-17 | Rohm And Haas Electronic Materials Llc | Method of filling through-holes to reduce voids and other defects |
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| US10190228B2 (en) | 2016-03-29 | 2019-01-29 | Rohm And Haas Electronic Materials Llc | Copper electroplating baths and electroplating methods capable of electroplating megasized photoresist defined features |
| US11035051B2 (en) * | 2016-08-15 | 2021-06-15 | Atotech Deutschland Gmbh | Acidic aqueous composition for electrolytic copper plating |
| US10718059B2 (en) * | 2017-07-10 | 2020-07-21 | Rohm And Haas Electronic Materials Llc | Nickel electroplating compositions with cationic polymers and methods of electroplating nickel |
| CN107313082B (zh) | 2017-07-25 | 2018-08-17 | 上海新阳半导体材料股份有限公司 | 整平剂、含其的金属电镀组合物、制备方法及应用 |
| US20190136397A1 (en) * | 2017-11-08 | 2019-05-09 | Rohm And Haas Electronic Materials Llc | Electroplated copper |
| CN109989077A (zh) * | 2017-12-29 | 2019-07-09 | 广东东硕科技有限公司 | 一种铜镀液 |
| CN109989076A (zh) * | 2017-12-29 | 2019-07-09 | 广东东硕科技有限公司 | 一种整平剂 |
| AU2018399626B2 (en) | 2018-01-03 | 2023-12-07 | Ecolab Usa Inc. | Benzotriazole derivatives as corrosion inhibitors |
| JP7208913B2 (ja) * | 2018-08-28 | 2023-01-19 | 株式会社Jcu | 硫酸銅めっき液およびこれを用いた硫酸銅めっき方法 |
| CN110129841B (zh) * | 2019-06-17 | 2021-04-27 | 广东东硕科技有限公司 | 整平剂及包含其的电镀液 |
| CN111876799A (zh) * | 2020-07-07 | 2020-11-03 | 广东硕成科技有限公司 | 一种适用于背板孔金属化组合物及其孔金属化方法 |
| US20240132453A1 (en) | 2021-02-15 | 2024-04-25 | Adeka Corporation | Additive for electroplating solution, electroplating solution, electroplating method, and method of producing metal layer |
| CN113463142B (zh) * | 2021-06-03 | 2022-06-14 | 广东硕成科技股份有限公司 | 一种电镀填孔组合物及其电镀填孔方法 |
| KR102339868B1 (ko) * | 2021-07-30 | 2021-12-16 | 와이엠티 주식회사 | 레벨링제 및 이를 포함하는 비아홀 충진을 위한 전기도금 조성물 |
| KR102339866B1 (ko) * | 2021-08-04 | 2021-12-16 | 와이엠티 주식회사 | 레벨링제 및 이를 포함하는 유리비아홀 기판 도금을 위한 전기도금 조성물 |
| CN115894908B (zh) * | 2021-09-30 | 2025-06-06 | 华为技术有限公司 | 聚合物、整平剂及其制备方法、电镀液和电镀方法 |
| CN113802158B (zh) * | 2021-10-21 | 2023-06-20 | 东莞市康迈克电子材料有限公司 | 一种电镀液及其应用、镀铜工艺及镀件 |
| CN113737232B (zh) * | 2021-11-08 | 2022-01-11 | 深圳市板明科技股份有限公司 | 一种线路板通孔电镀铜整平剂及其应用、制备方法 |
| CN116265620A (zh) * | 2023-02-21 | 2023-06-20 | 广东硕成科技股份有限公司 | 一种整平剂、电镀铜药水以及盲孔镀铜方法 |
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2010
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2011
- 2011-03-14 JP JP2011055906A patent/JP2011207878A/ja not_active Withdrawn
- 2011-03-15 KR KR1020110023077A patent/KR101739417B1/ko active Active
- 2011-03-15 CN CN2011101213393A patent/CN102276796B/zh active Active
- 2011-03-15 EP EP11158232.6A patent/EP2366686B1/en not_active Not-in-force
- 2011-03-15 TW TW100108654A patent/TWI428329B/zh active
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2016
- 2016-10-27 JP JP2016210569A patent/JP2017061487A/ja active Pending
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Also Published As
| Publication number | Publication date |
|---|---|
| JP2019052374A (ja) | 2019-04-04 |
| EP2366686A2 (en) | 2011-09-21 |
| US20110220514A1 (en) | 2011-09-15 |
| CN102276796A (zh) | 2011-12-14 |
| KR101739417B1 (ko) | 2017-05-24 |
| EP2366686A3 (en) | 2011-11-02 |
| US8268157B2 (en) | 2012-09-18 |
| EP2366686B1 (en) | 2013-05-08 |
| KR20110103894A (ko) | 2011-09-21 |
| TW201139397A (en) | 2011-11-16 |
| JP6797166B2 (ja) | 2020-12-09 |
| TWI428329B (zh) | 2014-03-01 |
| JP2011207878A (ja) | 2011-10-20 |
| JP2017061487A (ja) | 2017-03-30 |
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