CN101903336B - 酰基甘氨酸盐的制备方法 - Google Patents
酰基甘氨酸盐的制备方法 Download PDFInfo
- Publication number
- CN101903336B CN101903336B CN200880121606.3A CN200880121606A CN101903336B CN 101903336 B CN101903336 B CN 101903336B CN 200880121606 A CN200880121606 A CN 200880121606A CN 101903336 B CN101903336 B CN 101903336B
- Authority
- CN
- China
- Prior art keywords
- weight
- composition
- formula
- meter
- acyl group
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 0 *NCC(O)=O Chemical compound *NCC(O)=O 0.000 description 1
- OKJIRPAQVSHGFK-UHFFFAOYSA-M CC(NCC([O-])=O)=O Chemical compound CC(NCC([O-])=O)=O OKJIRPAQVSHGFK-UHFFFAOYSA-M 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
Landscapes
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Veterinary Medicine (AREA)
- Dermatology (AREA)
- Epidemiology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Birds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Cosmetics (AREA)
- Detergent Compositions (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102007055265.5 | 2007-11-20 | ||
| DE102007055265A DE102007055265A1 (de) | 2007-11-20 | 2007-11-20 | Verfahren zur Herstellung von Acylglycinaten |
| PCT/EP2008/009646 WO2009065530A2 (de) | 2007-11-20 | 2008-11-14 | Verfahren zur herstellung von acylglycinaten |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101903336A CN101903336A (zh) | 2010-12-01 |
| CN101903336B true CN101903336B (zh) | 2014-06-25 |
Family
ID=40394359
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN200880121606.3A Active CN101903336B (zh) | 2007-11-20 | 2008-11-14 | 酰基甘氨酸盐的制备方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US8338483B2 (enExample) |
| EP (2) | EP2248512A3 (enExample) |
| JP (1) | JP5496905B2 (enExample) |
| CN (1) | CN101903336B (enExample) |
| BR (1) | BRPI0819337A2 (enExample) |
| DE (1) | DE102007055265A1 (enExample) |
| ES (1) | ES2530217T3 (enExample) |
| WO (1) | WO2009065530A2 (enExample) |
Families Citing this family (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102006038853A1 (de) * | 2006-08-18 | 2008-02-21 | Clariant International Limited | Verfahren zur Herstellung von Acylglycinaten mittels Direktoxidation |
| DE102008003825A1 (de) * | 2008-01-10 | 2009-07-16 | Clariant International Ltd. | Verfahren zur Herstellung von Acylglycinaten mittels Direktoxidation |
| DE102011107503A1 (de) * | 2011-07-15 | 2012-03-01 | Clariant International Ltd. | Verfahren zur Herstellung von Acylglycinaten und Zusammensetzungen enthaltend derartige Verbindungen |
| US8822711B2 (en) * | 2011-07-28 | 2014-09-02 | Conopco, Inc. | Method for preparing fatty acyl amido carboxylic acid based surfactants |
| US8658589B2 (en) | 2011-07-28 | 2014-02-25 | Conopco, Inc. | Fatty acyl amido based surfactant concentrates |
| EP2870136B1 (en) | 2012-07-03 | 2018-10-24 | Stepan Company | Process for preparing n-acyl amino acid salts |
| RU2624026C2 (ru) * | 2012-08-23 | 2017-06-30 | Гэлакси Сёфэктентс Лтд. | Способ получения основанных на n-ациламинокислоте поверхностно-активных веществ с применением основанных на n-ациламинокислоте поверхностно-активных веществ или соответствующих ангидридов в качестве катализаторов |
| CN102863352A (zh) * | 2012-09-05 | 2013-01-09 | 长沙普济生物科技有限公司 | 一种椰油酰基氨基酸钠的合成方法 |
| WO2015000931A2 (en) | 2013-07-05 | 2015-01-08 | Akzo Nobel Chemicals International B.V. | The synthesis of new anionic surfactants and their use as collectors in froth flotation of non-sulphidic ores |
| JP6595472B2 (ja) | 2013-08-19 | 2019-10-23 | ステパン カンパニー | N−アシルアミノ酸塩を調製するためのプロセス |
| CN105683151B (zh) | 2013-10-31 | 2020-11-03 | 味之素株式会社 | 包含n-长链酰基酸性氨基酸和/或其盐的水溶液及其制造方法 |
| CN104649927B (zh) * | 2013-11-25 | 2017-10-31 | 江苏四新界面剂科技有限公司 | 一种正十一烷二酰基二谷氨酸三乙醇胺盐及其制备方法 |
| EP3080086B1 (en) | 2013-12-09 | 2017-07-05 | Unilever PLC, a company registered in England and Wales under company no. 41424 of | Process of making adamantanamides |
| CN103965072B (zh) * | 2014-04-02 | 2016-08-17 | 烟台恒迪克能源科技有限公司 | 一种癸二酰基谷氨酸的合成方法 |
| CN103951581B (zh) * | 2014-04-05 | 2016-04-27 | 烟台恒迪克能源科技有限公司 | 一种正十一碳二酰基二天门冬氨酸-双-二甘醇胺盐的合成 |
| DE102015014929A1 (de) * | 2015-11-13 | 2017-05-18 | Bernd Kunze | Verfahren zur Herstellung von N-Acylderivaten, die Fettsäure-Reste enthalten |
| EP3708643A4 (en) | 2017-11-06 | 2021-08-18 | Ajinomoto Co., Inc. | DETERGENT COMPOSITION |
| US12123004B2 (en) | 2018-07-18 | 2024-10-22 | Modular Genetics, Inc. | Generation of acyl amino acids |
| EP3647303B1 (en) * | 2018-10-31 | 2022-08-31 | Clariant International Ltd | Process for preparing fatty acid chlorides and n-acyl amino acid salts |
| CN111187174A (zh) * | 2020-01-16 | 2020-05-22 | 广东丽臣奥威实业有限公司 | 一种脂肪酰甘氨酸盐或脂肪衍生物酰甘氨酸盐的生产及纯化方法 |
| CN114369036B (zh) * | 2021-12-30 | 2024-04-19 | 广州花语精细化工有限公司 | 一种降低甘氨酸类表面活性剂中胺类副产物的方法 |
| CN115160169B (zh) * | 2022-07-25 | 2024-04-16 | 湖州欧利生物科技有限公司 | 椰油酰甘氨酸盐表面活性剂的生产工艺 |
| CN117003661A (zh) * | 2023-07-07 | 2023-11-07 | 广东聚石科技研究院有限公司 | 一种n-酰基氨基酸的制备方法 |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4828824A (en) * | 1986-09-15 | 1989-05-09 | L'oreal | Dentifrice containing a poly(hydroxypropyl ether) non-ionic surfactant and a salt of a specific derivative of a protein degradation product |
| US5458881A (en) * | 1991-06-03 | 1995-10-17 | Givaudan-Lavirotte | N-acylated derivatives of mixtures of amino acids derived from hydrolysates of cereal proteins and their applications |
| CN1120533A (zh) * | 1994-05-02 | 1996-04-17 | 赫彻斯特股份公司 | N-酰基-α-氨基酸衍生物的制备方法 |
| CN1332721A (zh) * | 1998-12-28 | 2002-01-23 | 旭化成株式会社 | 生产酸性n-长链酰氨基酸的方法 |
Family Cites Families (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IT490450A (enExample) | 1951-07-19 | |||
| JP2969397B2 (ja) * | 1991-09-10 | 1999-11-02 | 花王株式会社 | N−長鎖アシル−β−アラニンの製造方法 |
| DE69422366T2 (de) * | 1993-03-30 | 2000-08-24 | Ajinomoto Co., Inc. | Waschmittelzusammensetzung |
| JP3362468B2 (ja) | 1993-08-25 | 2003-01-07 | 味の素株式会社 | N−混合飽和脂肪酸アシル中性アミノ酸の製造法 |
| JP3304646B2 (ja) | 1994-06-07 | 2002-07-22 | 味の素株式会社 | 洗浄剤組成物 |
| US5710295A (en) | 1995-06-06 | 1998-01-20 | Hampshire Chemical Corp. | Preparation of alkali metal acyl amino acids |
| JPH1081656A (ja) * | 1996-09-06 | 1998-03-31 | Ajinomoto Co Inc | N−長鎖アシル酸性アミノ酸またはその塩の製造法 |
| FR2765109B1 (fr) * | 1997-06-25 | 2001-02-09 | Seppic Sa | Composition comprenant un lipoaminoacide et les constituants d'un extrait de plantes riches en tanins et utilisation en cosmetique |
| JP4407846B2 (ja) | 1998-02-27 | 2010-02-03 | 花王株式会社 | 1級アルコールの酸化方法 |
| JP2001278778A (ja) * | 2000-03-31 | 2001-10-10 | Shiseido Co Ltd | 皮膚洗浄料 |
| US6828452B2 (en) * | 2001-01-18 | 2004-12-07 | Cognis Deutschland Gmbh & Co. Kg | Method for producing acyl amino acids |
| US6703517B2 (en) | 2001-11-26 | 2004-03-09 | Ajinomoto Co., Inc. | Method for preparing N-long chain acyl neutral amino acid |
| EP1672055B1 (en) | 2003-10-03 | 2008-10-01 | Ajinomoto Co., Inc. | Detergent compositions and processes for the production thereof |
| DE102004048324A1 (de) | 2003-10-08 | 2005-05-12 | Ajinomoto Kk | Kristalle von N-langkettigen Acyglycin-Salzen, Verfahren zu ihrer Herstellung und diese Kristalle enthaltende Reinigungsmittel-Zusammensetzungen |
| JP2007269662A (ja) * | 2006-03-30 | 2007-10-18 | Ajinomoto Co Inc | クリーム状皮膚洗浄剤組成物 |
| US20070299269A1 (en) | 2006-06-27 | 2007-12-27 | Conopco, Inc., D/B/A Unilever | Process for converting primary amidoalcohols to amidocarboxylic acids in high yield |
| US7307187B1 (en) | 2006-06-27 | 2007-12-11 | Conopco, Inc. | Process for converting primary amidoalcohols to amidocarboxylic acids in high yield |
| DE102006038853A1 (de) | 2006-08-18 | 2008-02-21 | Clariant International Limited | Verfahren zur Herstellung von Acylglycinaten mittels Direktoxidation |
| DE102008003825A1 (de) | 2008-01-10 | 2009-07-16 | Clariant International Ltd. | Verfahren zur Herstellung von Acylglycinaten mittels Direktoxidation |
-
2007
- 2007-11-20 DE DE102007055265A patent/DE102007055265A1/de not_active Withdrawn
-
2008
- 2008-11-14 WO PCT/EP2008/009646 patent/WO2009065530A2/de not_active Ceased
- 2008-11-14 CN CN200880121606.3A patent/CN101903336B/zh active Active
- 2008-11-14 JP JP2010534399A patent/JP5496905B2/ja active Active
- 2008-11-14 EP EP20100008258 patent/EP2248512A3/de not_active Ceased
- 2008-11-14 US US12/743,458 patent/US8338483B2/en not_active Expired - Fee Related
- 2008-11-14 ES ES08852108.3T patent/ES2530217T3/es active Active
- 2008-11-14 BR BRPI0819337 patent/BRPI0819337A2/pt not_active IP Right Cessation
- 2008-11-14 EP EP08852108.3A patent/EP2212278B1/de active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4828824A (en) * | 1986-09-15 | 1989-05-09 | L'oreal | Dentifrice containing a poly(hydroxypropyl ether) non-ionic surfactant and a salt of a specific derivative of a protein degradation product |
| US5458881A (en) * | 1991-06-03 | 1995-10-17 | Givaudan-Lavirotte | N-acylated derivatives of mixtures of amino acids derived from hydrolysates of cereal proteins and their applications |
| CN1120533A (zh) * | 1994-05-02 | 1996-04-17 | 赫彻斯特股份公司 | N-酰基-α-氨基酸衍生物的制备方法 |
| CN1332721A (zh) * | 1998-12-28 | 2002-01-23 | 旭化成株式会社 | 生产酸性n-长链酰氨基酸的方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| US20100273879A1 (en) | 2010-10-28 |
| BRPI0819337A2 (pt) | 2015-05-12 |
| WO2009065530A2 (de) | 2009-05-28 |
| ES2530217T3 (es) | 2015-02-27 |
| DE102007055265A1 (de) | 2009-05-28 |
| US8338483B2 (en) | 2012-12-25 |
| EP2212278A2 (de) | 2010-08-04 |
| EP2248512A3 (de) | 2012-01-25 |
| JP5496905B2 (ja) | 2014-05-21 |
| CN101903336A (zh) | 2010-12-01 |
| JP2011503218A (ja) | 2011-01-27 |
| EP2248512A2 (de) | 2010-11-10 |
| WO2009065530A3 (de) | 2009-09-03 |
| EP2212278B1 (de) | 2015-01-07 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C35 | Partial or whole invalidation of patent or utility model | ||
| IP01 | Partial invalidation of patent right |
Commission number: 4W103995 Conclusion of examination: The patent right of the invention of section 200880121606.3 is invalid and shall continue to be maintained on the basis of the right of claim 1-50 submitted by the patent owner in October 23, 2015. Decision date of declaring invalidation: 20160321 Decision number of declaring invalidation: 28492 Denomination of invention: Method for producing acylglycinates Granted publication date: 20140625 Patentee: Clariant Finance (BVI) Ltd. |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20180712 Address after: Mu Tengci, Switzerland Patentee after: BAYER INTELLECTUAL PROPERTY GmbH Address before: The British Virgin Islands of Tortola Patentee before: Clariant Finance (BVI) Ltd. |
|
| IP01 | Partial invalidation of patent right | ||
| IP01 | Partial invalidation of patent right |
Commission number: 4W105269 Conclusion of examination: On the basis of clauses 1-49 filed by the patentee on April 21, 2017, claims 14-49 are declared null and void, and the patent right for invention 2008 80121606.3 is maintained valid on the basis of claims 1-13. Decision date of declaring invalidation: 20171207 Decision number of declaring invalidation: 34082 Denomination of invention: Method for producing acylglycinates Granted publication date: 20140625 Patentee: BAYER INTELLECTUAL PROPERTY GmbH |