CN101395230B - 聚合物封装的颗粒的含水分散体、相关的涂料组合物和涂覆的基材 - Google Patents
聚合物封装的颗粒的含水分散体、相关的涂料组合物和涂覆的基材 Download PDFInfo
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- CN101395230B CN101395230B CN200780007782XA CN200780007782A CN101395230B CN 101395230 B CN101395230 B CN 101395230B CN 200780007782X A CN200780007782X A CN 200780007782XA CN 200780007782 A CN200780007782 A CN 200780007782A CN 101395230 B CN101395230 B CN 101395230B
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Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K9/00—Use of pretreated ingredients
- C08K9/10—Encapsulated ingredients
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82B—NANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
- B82B3/00—Manufacture or treatment of nanostructures by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/0804—Manufacture of polymers containing ionic or ionogenic groups
- C08G18/0819—Manufacture of polymers containing ionic or ionogenic groups containing anionic or anionogenic groups
- C08G18/0823—Manufacture of polymers containing ionic or ionogenic groups containing anionic or anionogenic groups containing carboxylate salt groups or groups forming them
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/10—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step
- C08G18/12—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step using two or more compounds having active hydrogen in the first polymerisation step
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/67—Unsaturated compounds having active hydrogen
- C08G18/671—Unsaturated compounds having only one group containing active hydrogen
- C08G18/672—Esters of acrylic or alkyl acrylic acid having only one group containing active hydrogen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
- C08G18/75—Polyisocyanates or polyisothiocyanates cyclic cycloaliphatic
- C08G18/758—Polyisocyanates or polyisothiocyanates cyclic cycloaliphatic containing two or more cycloaliphatic rings
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
- C09D175/14—Polyurethanes having carbon-to-carbon unsaturated bonds
- C09D175/16—Polyurethanes having carbon-to-carbon unsaturated bonds having terminal carbon-to-carbon unsaturated bonds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
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- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
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- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
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- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C48/00—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
- B29C48/03—Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor characterised by the shape of the extruded material at extrusion
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Abstract
Description
组分 | 重量(g) |
进料I | |
聚(新戊二醇己二酸酯)1 | 780.0 |
二羟甲基丙酸(DMPA) | 280.7 |
三乙胺 | 127.1 |
丁基化羟基甲苯 | 2.5 |
亚磷酸三苯酯 | 2.5 |
进料II | |
甲基丙烯酸羟乙酯(HEMA) | 116.7 |
甲基丙烯酸丁酯 | 791.2 |
进料III | |
亚甲基双(4-环己基异氰酸酯) | 1175.1 |
进料IV | |
甲基丙烯酸丁酯 | 57.5 |
进料V | |
去离子水 | 4734.8 |
乙二胺 | 49.2 |
二甲基乙醇胺 | 40.6 |
进料VI | |
甲基丙烯酸丁酯 | 50 |
组分 | 重量(g) |
进料I | |
实施例1的聚氨酯分散体 | 4772.7 |
去离子水 | 2304.5 |
氢醌甲醚(MEHQ) | 1.36 |
PB 15:3颜料2 | 700.0 |
Shellsol OMS(Shell Chemical Co.) | 86.4 |
进料II | |
去离子水 | 71.5 |
叔丁基氢过氧化物(70%水溶液) | 5.8 |
进料III | |
去离子水 | 337.2 |
硫酸亚铁铵 | 0.13 |
偏亚硫酸氢钠 | 8.18 |
组分 | 重量(g) |
进料I | |
实施例1的聚氨酯分散体 | 4772.7 |
去离子水 | 2304.5 |
氢醌甲醚(MEHQ) | 1.36 |
PR 122颜料3 | 700.0 |
Shellsol OMS(Shell Chemical Co.) | 86.4 |
进料II | |
去离子水 | 71.5 |
叔丁基氢过氧化物(70%水溶液) | 5.8 |
进料III | |
去离子水 | 337.2 |
硫酸亚铁铵 | 0.13 |
偏亚硫酸氢钠 | 8.18 |
组分 | 重量(g) |
进料I | |
实施例1的聚氨酯分散体 | 4872.7 |
去离子水 | 2204.5 |
氢醌甲醚(MEHQ) | 1.36 |
PY 128颜料4 | 700.0 |
Shellsol OMS(Shell Chemical Co.) | 86.4 |
进料II | |
去离子水 | 71.5 |
叔丁基氢过氧化物(70%水溶液) | 5.8 |
进料III | |
去离子水 | 337.2 |
硫酸亚铁铵 | 0.13 |
偏亚硫酸氢钠 | 8.18 |
组分 | 重量(g) |
进料I | |
聚(环丁氧烷)5 | 355.6 |
二羟甲基丙酸(DMPA) | 119.2 |
三乙胺 | 54.0 |
丁基化羟基甲苯 | 2.2 |
亚磷酸三苯酯 | 1.1 |
进料II | |
甲基丙烯酸羟乙酯(HEMA) | 27.8 |
甲基丙烯酸丁酯 | 48.4 |
丙烯酸丁酯 | 319.2 |
进料III | |
亚甲基双(4-环己基异氰酸酯) | 558.9 |
进料IV | |
甲基丙烯酸丁酯 | 55.6 |
进料V | |
去离子水 | 2086.3 |
二乙醇胺 | 20.2 |
乙二胺 | 26.9 |
二甲基乙醇胺 | 19.7 |
进料VI | |
甲基丙烯酸丁酯 | 50.0 |
组分 | 重量(g) |
进料I | |
实施例6的聚氨酯分散体 | 7271.0 |
去离子水 | 3293.1 |
氢醌甲醚(MEHQ) | 2.0 |
PB 15:3颜料 | 1079.5 |
Shellsol OMS(Shell Chemical Co.) | 131.5 |
进料II | |
去离子水 | 102.4 |
叔丁基氢过氧化物(70%水溶液) | 12.3 |
进料III | |
去离子水 | 512.1 |
硫酸亚铁铵 | 0.15 |
偏亚硫酸氢钠 | 12.3 |
组分 | 重量(g) |
进料I | |
实施例6的聚氨酯分散体 | 7271.0 |
去离子水 | 3293.1 |
氢醌甲醚(MEHQ) | 2.0 |
PR 122颜料 | 1079.5 |
Shellsol OMS(Shell Chemical Co.) | 131.5 |
进料II | |
去离子水 | 102.4 |
叔丁基氢过氧化物(70%水溶液) | 12.3 |
进料III | |
去离子水 | 512.1 |
硫酸亚铁铵 | 0.15 |
偏亚硫酸氢钠 | 12.3 |
组分 | 重量(g) |
进料I | |
实施例6的聚氨酯分散体 | 7271.0 |
去离子水 | 3293.1 |
氢醌甲醚(MEHQ) | 2.0 |
PY 128颜料 | 1079.5 |
Shellsol OMS(Shell Chemical Co.) | 131.5 |
进料II | |
去离子水 | 102.4 |
叔丁基氢过氧化物(70%水溶液) | 12.3 |
进料III | |
去离子水 | 512.1 |
硫酸亚铁铵 | 0.15 |
偏亚硫酸氢钠 | 12.3 |
组分 | 成分 | 重量份 |
1 | Uralac P880树脂6 | 81.136 |
2 | Primid XL5527 | 11.064 |
3 | 树脂流PL 200A8 | 1 |
4 | 安息香9 | 0.7 |
5 | Irganox 107610 | 1.2 |
6 | 流动添加剂 | 1.3 |
7 | Tinuvin 14411 | 1 |
8 | Tinuvin 90011 | 2 |
9 | 透明氧化锌12 | 0.5 |
10 | 氧化铝C13 | 0.01 |
角度 | L | a | b | C | h |
15 | 9.2 | -14.6 | 8.53 | -15.6 | 6.53 |
25 | 6.27 | -7.94 | 5.68 | -8.46 | 4.86 |
45 | 8.19 | 5.16 | 5.71 | 5.35 | 5.53 |
75 | 10.03 | 17.53 | 6.73 | 18.34 | 4.05 |
110 | 10.69 | 22 | 7.24 | 22.97 | 2.95 |
角度 | L | a | b | C | h |
15 | -9.58 | -9.21 | -1.6 | -8.57 | -3.72 |
25 | -5.59 | -5.98 | -3.27 | -5.13 | -4.49 |
45 | 0.25 | 0.09 | -5.75 | 1.06 | -5.66 |
75 | 1.75 | 5.86 | -5.54 | 6.43 | -4.86 |
110 | 1.84 | 6.02 | -4.26 | 6.32 | -3.8 |
组分 | 重量(g) |
实施例6的聚氨酯分散体 | 6272.3 |
去离子水 | 4545.6 |
PR 179颜料14 | 1818.2 |
Shellsol OMS(Shell Chemical Co.) | 218.2 |
角度 | L | a | b | C | h |
15 | -1.76 | -3.2 | -2.64 | -4.08 | -0.77 |
25 | -3 | -5.02 | -4.05 | -6.33 | -1.21 |
45 | -4.05 | -8.41 | -5.9 | -10.2 | -1.23 |
75 | -4.5 | -10.17 | -6.52 | -12.06 | -0.65 |
110 | -4.59 | -10.85 | -6.68 | -12.74 | -0.18 |
Claims (23)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
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US11/337,062 | 2006-01-20 | ||
US11/337,062 US7605194B2 (en) | 2003-06-24 | 2006-01-20 | Aqueous dispersions of polymer-enclosed particles, related coating compositions and coated substrates |
PCT/US2007/000637 WO2008033154A2 (en) | 2006-01-20 | 2007-01-10 | Aqueous dispersions of polymer-enclosed particles, related coating compositions and coated substrates |
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CN101395230A CN101395230A (zh) | 2009-03-25 |
CN101395230B true CN101395230B (zh) | 2012-05-30 |
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CN200780007782XA Active CN101395230B (zh) | 2006-01-20 | 2007-01-10 | 聚合物封装的颗粒的含水分散体、相关的涂料组合物和涂覆的基材 |
Country Status (18)
Country | Link |
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US (4) | US7605194B2 (zh) |
EP (1) | EP1973977B1 (zh) |
JP (2) | JP5507849B2 (zh) |
KR (2) | KR101233467B1 (zh) |
CN (1) | CN101395230B (zh) |
AR (1) | AR059856A1 (zh) |
AU (2) | AU2007295068B2 (zh) |
BR (1) | BRPI0706937A2 (zh) |
CA (1) | CA2637409C (zh) |
HK (1) | HK1127509A1 (zh) |
MX (1) | MX2008009259A (zh) |
MY (3) | MY166592A (zh) |
NZ (1) | NZ569842A (zh) |
PL (1) | PL1973977T3 (zh) |
RU (1) | RU2432377C2 (zh) |
SG (1) | SG171585A1 (zh) |
TW (1) | TWI348475B (zh) |
WO (1) | WO2008033154A2 (zh) |
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