CN101044268A - 通过熔融盐电解制造金属的方法和制造装置 - Google Patents
通过熔融盐电解制造金属的方法和制造装置 Download PDFInfo
- Publication number
- CN101044268A CN101044268A CNA2005800349261A CN200580034926A CN101044268A CN 101044268 A CN101044268 A CN 101044268A CN A2005800349261 A CNA2005800349261 A CN A2005800349261A CN 200580034926 A CN200580034926 A CN 200580034926A CN 101044268 A CN101044268 A CN 101044268A
- Authority
- CN
- China
- Prior art keywords
- mentioned
- metal
- negative electrode
- interior region
- fusion electrolysis
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229910052751 metal Inorganic materials 0.000 title claims abstract description 157
- 239000002184 metal Substances 0.000 title claims abstract description 157
- 238000005868 electrolysis reaction Methods 0.000 title claims abstract description 66
- 150000003839 salts Chemical class 0.000 title claims abstract description 37
- 238000000034 method Methods 0.000 title claims abstract description 32
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims abstract description 41
- 239000001110 calcium chloride Substances 0.000 claims abstract description 41
- 229910001628 calcium chloride Inorganic materials 0.000 claims abstract description 41
- 238000004891 communication Methods 0.000 claims abstract description 28
- 229910052791 calcium Inorganic materials 0.000 claims description 91
- 239000011575 calcium Substances 0.000 claims description 91
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 87
- 238000004519 manufacturing process Methods 0.000 claims description 52
- 230000004927 fusion Effects 0.000 claims description 51
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 36
- 239000010936 titanium Substances 0.000 claims description 36
- 229910052719 titanium Inorganic materials 0.000 claims description 35
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 claims description 33
- 238000002844 melting Methods 0.000 claims description 30
- 230000008018 melting Effects 0.000 claims description 30
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 2
- 229910052799 carbon Inorganic materials 0.000 claims description 2
- KWGKDLIKAYFUFQ-UHFFFAOYSA-M lithium chloride Chemical compound [Li+].[Cl-] KWGKDLIKAYFUFQ-UHFFFAOYSA-M 0.000 claims 2
- CPRPMYXKLMPQOB-UHFFFAOYSA-K [Na+].[Cl-].[Cl-].[Cl-].[Ba+2] Chemical compound [Na+].[Cl-].[Cl-].[Cl-].[Ba+2] CPRPMYXKLMPQOB-UHFFFAOYSA-K 0.000 claims 1
- 239000000155 melt Substances 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 description 19
- 239000000460 chlorine Substances 0.000 description 17
- 229910052801 chlorine Inorganic materials 0.000 description 17
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 11
- 238000010438 heat treatment Methods 0.000 description 6
- 238000006722 reduction reaction Methods 0.000 description 6
- 238000003287 bathing Methods 0.000 description 5
- 125000001309 chloro group Chemical group Cl* 0.000 description 5
- 230000032696 parturition Effects 0.000 description 5
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 3
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 3
- 150000001669 calcium Chemical class 0.000 description 3
- 238000005660 chlorination reaction Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000000605 extraction Methods 0.000 description 3
- 238000009434 installation Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 150000002739 metals Chemical class 0.000 description 3
- 238000005325 percolation Methods 0.000 description 3
- 230000002829 reductive effect Effects 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 3
- 229910000975 Carbon steel Inorganic materials 0.000 description 2
- 239000010962 carbon steel Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- 239000012141 concentrate Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- -1 calcium metals Chemical class 0.000 description 1
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical group [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
- 239000000292 calcium oxide Substances 0.000 description 1
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 230000008602 contraction Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910001510 metal chloride Inorganic materials 0.000 description 1
- 229910001092 metal group alloy Inorganic materials 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000003609 titanium compounds Chemical class 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/129—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds by dissociation, e.g. thermic dissociation of titanium tetraiodide, or by electrolysis or with the use of an electric arc
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C3/00—Electrolytic production, recovery or refining of metals by electrolysis of melts
- C25C3/02—Electrolytic production, recovery or refining of metals by electrolysis of melts of alkali or alkaline earth metals
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C3/00—Electrolytic production, recovery or refining of metals by electrolysis of melts
- C25C3/26—Electrolytic production, recovery or refining of metals by electrolysis of melts of titanium, zirconium, hafnium, tantalum or vanadium
- C25C3/28—Electrolytic production, recovery or refining of metals by electrolysis of melts of titanium, zirconium, hafnium, tantalum or vanadium of titanium
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C7/00—Constructional parts, or assemblies thereof, of cells; Servicing or operating of cells
- C25C7/02—Electrodes; Connections thereof
- C25C7/025—Electrodes; Connections thereof used in cells for the electrolysis of melts
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Electrochemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Manufacturing & Machinery (AREA)
- Mechanical Engineering (AREA)
- Electrolytic Production Of Metals (AREA)
- Manufacture And Refinement Of Metals (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2004297865A JP4247792B2 (ja) | 2004-10-12 | 2004-10-12 | 溶融塩電解による金属の製造方法および製造装置 |
JP297865/2004 | 2004-10-12 |
Publications (1)
Publication Number | Publication Date |
---|---|
CN101044268A true CN101044268A (zh) | 2007-09-26 |
Family
ID=36148273
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNA2005800349261A Pending CN101044268A (zh) | 2004-10-12 | 2005-10-05 | 通过熔融盐电解制造金属的方法和制造装置 |
Country Status (9)
Country | Link |
---|---|
US (1) | US20080078679A1 (de) |
EP (1) | EP1811062A4 (de) |
JP (1) | JP4247792B2 (de) |
CN (1) | CN101044268A (de) |
AU (1) | AU2005293038A1 (de) |
CA (1) | CA2582035A1 (de) |
EA (1) | EA011903B1 (de) |
NO (1) | NO20072241L (de) |
WO (1) | WO2006040978A1 (de) |
Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101649472B (zh) * | 2008-08-15 | 2012-06-06 | 攀钢集团钢铁钒钛股份有限公司 | 一种制备金属钛的方法 |
CN103237926A (zh) * | 2010-11-18 | 2013-08-07 | 金属电解有限公司 | 用于电解还原固体进料的方法和系统 |
CN103774180A (zh) * | 2014-01-28 | 2014-05-07 | 东北大学 | 一种集氯化-电解为一体的制取金属和合金的装置与方法 |
CN103898553A (zh) * | 2014-03-25 | 2014-07-02 | 中国科学院过程工程研究所 | 一种电积和精炼同步进行生产金属钙的方法 |
CN104668557A (zh) * | 2015-02-06 | 2015-06-03 | 池州博瑞德钙业有限公司 | 一种金属钙压锭成型设备 |
CN105531401A (zh) * | 2014-06-30 | 2016-04-27 | 东邦钛株式会社 | 制造金属的方法以及制造高熔点金属的方法 |
CN106835203A (zh) * | 2016-12-26 | 2017-06-13 | 宝纳资源控股(集团)有限公司 | 一种熔盐的净化装置及方法 |
US9725815B2 (en) | 2010-11-18 | 2017-08-08 | Metalysis Limited | Electrolysis apparatus |
CN107532236A (zh) * | 2015-02-09 | 2018-01-02 | 国立大学法人北海道大学 | 金属钒的制造方法 |
CN109881200A (zh) * | 2019-04-10 | 2019-06-14 | 深圳市铿东科技有限公司 | 一种碱性蚀刻液再生及其铜回收方法 |
Families Citing this family (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP4193984B2 (ja) * | 2003-08-28 | 2008-12-10 | 株式会社大阪チタニウムテクノロジーズ | 金属製造装置 |
EP1878814A4 (de) * | 2005-04-25 | 2010-01-20 | Toho Titanium Co Ltd | Schmelzflusselektrolysezelle und verfahren zur herstellung von metall damit |
JP2007063585A (ja) * | 2005-08-30 | 2007-03-15 | Sumitomo Titanium Corp | 溶融塩電解方法および電解槽並びにそれを用いたTiの製造方法 |
WO2008038405A1 (fr) * | 2006-09-28 | 2008-04-03 | Toho Titanium Co., Ltd. | Récipient d'électrolyse de sel fondu pour la fabrication de métal et procédé de fabrication de métal à l'aide de celui-ci |
AU2008208040B2 (en) | 2007-01-22 | 2012-03-01 | Ats Mer, Llc | Metallothermic reduction of in-situ generated titanium chloride |
JPWO2008102520A1 (ja) * | 2007-02-19 | 2010-05-27 | 東邦チタニウム株式会社 | 溶融塩電解による金属の製造装置およびこれを用いた金属の製造方法 |
CN101680100B (zh) | 2007-05-11 | 2011-12-07 | 株式会社慧武光·能源开发研究所 | 现场综合生产厂 |
JP2009019250A (ja) * | 2007-07-13 | 2009-01-29 | Osaka Titanium Technologies Co Ltd | 金属製造方法および装置 |
MD168Z (ro) * | 2009-06-04 | 2010-10-31 | Институт Прикладной Физики Академии Наук Молдовы | Dispozitiv pentru acoperirea galvanică a suprafeţei interioare a pieselor cilindrice cu un diametru mic şi mijlociu |
CN102517611B (zh) * | 2011-12-27 | 2015-08-26 | 宁波江丰电子材料股份有限公司 | 熔盐电解提炼设备及其提炼金属的方法 |
JP6270446B2 (ja) * | 2013-12-06 | 2018-01-31 | 東邦チタニウム株式会社 | 溶融塩電解による金属の製造方法 |
CN104928721B (zh) * | 2015-06-12 | 2017-09-22 | 中南大学 | 一种低价钛氯化物熔盐电解质的制备及精炼装置 |
CN107164781A (zh) * | 2017-06-05 | 2017-09-15 | 攀钢集团研究院有限公司 | 一种制备超细钛粉的方法 |
CN107059067A (zh) * | 2017-06-05 | 2017-08-18 | 攀钢集团研究院有限公司 | 一种制备超细钛合金粉的方法 |
US20240084468A1 (en) * | 2022-09-09 | 2024-03-14 | Phoenix Tailings, Inc. | Systems and methods for feeding solid material and a gas into an electrolytic cell |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ES257371A1 (es) * | 1959-05-13 | 1960-11-16 | Solvay | Procedimiento para la preparaciën de un metal alcalino-terreo por electrëlisis de banos de cloruros fundidos |
JPS61186489A (ja) * | 1985-02-13 | 1986-08-20 | Hiroshi Ishizuka | アルカリ金属または土金属の溶融塩化物電解装置 |
FR2589169B1 (fr) * | 1985-10-25 | 1990-08-31 | Commissariat Energie Atomique | Electrolyseur pour l'extraction d'une substance, notamment d'un metal alcalin, d'un bain electrolytique |
ITTO970080A1 (it) * | 1997-02-04 | 1998-08-04 | Marco Vincenzo Ginatta | Procedimento per la produzione elettrolitica di metalli |
JP2003129268A (ja) * | 2001-10-17 | 2003-05-08 | Katsutoshi Ono | 金属チタンの精錬方法及び精錬装置 |
JP3718691B2 (ja) * | 2002-04-18 | 2005-11-24 | 財団法人生産技術研究奨励会 | チタンの製造方法、純金属の製造方法、及び純金属の製造装置 |
-
2004
- 2004-10-12 JP JP2004297865A patent/JP4247792B2/ja not_active Expired - Fee Related
-
2005
- 2005-10-05 EP EP05790573A patent/EP1811062A4/de not_active Withdrawn
- 2005-10-05 US US11/576,887 patent/US20080078679A1/en not_active Abandoned
- 2005-10-05 AU AU2005293038A patent/AU2005293038A1/en not_active Abandoned
- 2005-10-05 CA CA002582035A patent/CA2582035A1/en not_active Abandoned
- 2005-10-05 CN CNA2005800349261A patent/CN101044268A/zh active Pending
- 2005-10-05 EA EA200700843A patent/EA011903B1/ru not_active IP Right Cessation
- 2005-10-05 WO PCT/JP2005/018449 patent/WO2006040978A1/ja active Application Filing
-
2007
- 2007-04-30 NO NO20072241A patent/NO20072241L/no not_active Application Discontinuation
Cited By (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101649472B (zh) * | 2008-08-15 | 2012-06-06 | 攀钢集团钢铁钒钛股份有限公司 | 一种制备金属钛的方法 |
US9725815B2 (en) | 2010-11-18 | 2017-08-08 | Metalysis Limited | Electrolysis apparatus |
CN103237926A (zh) * | 2010-11-18 | 2013-08-07 | 金属电解有限公司 | 用于电解还原固体进料的方法和系统 |
CN103774180A (zh) * | 2014-01-28 | 2014-05-07 | 东北大学 | 一种集氯化-电解为一体的制取金属和合金的装置与方法 |
CN103774180B (zh) * | 2014-01-28 | 2016-03-02 | 东北大学 | 一种集氯化-电解为一体的制取金属和合金的装置与方法 |
CN103898553A (zh) * | 2014-03-25 | 2014-07-02 | 中国科学院过程工程研究所 | 一种电积和精炼同步进行生产金属钙的方法 |
CN103898553B (zh) * | 2014-03-25 | 2016-06-22 | 中国科学院过程工程研究所 | 一种电积和精炼同步进行生产金属钙的方法 |
CN105531401A (zh) * | 2014-06-30 | 2016-04-27 | 东邦钛株式会社 | 制造金属的方法以及制造高熔点金属的方法 |
CN105531401B (zh) * | 2014-06-30 | 2018-09-04 | 东邦钛株式会社 | 制造金属的方法以及制造高熔点金属的方法 |
CN104668557B (zh) * | 2015-02-06 | 2018-12-28 | 安徽腾拓新材料科技有限公司 | 一种金属钙压锭成型设备 |
CN104668557A (zh) * | 2015-02-06 | 2015-06-03 | 池州博瑞德钙业有限公司 | 一种金属钙压锭成型设备 |
CN107532236A (zh) * | 2015-02-09 | 2018-01-02 | 国立大学法人北海道大学 | 金属钒的制造方法 |
CN107532236B (zh) * | 2015-02-09 | 2019-09-17 | 国立大学法人北海道大学 | 金属钒的制造方法 |
CN106835203A (zh) * | 2016-12-26 | 2017-06-13 | 宝纳资源控股(集团)有限公司 | 一种熔盐的净化装置及方法 |
CN106835203B (zh) * | 2016-12-26 | 2019-05-31 | 宝纳资源控股(集团)有限公司 | 一种熔盐的净化装置及方法 |
CN109881200A (zh) * | 2019-04-10 | 2019-06-14 | 深圳市铿东科技有限公司 | 一种碱性蚀刻液再生及其铜回收方法 |
Also Published As
Publication number | Publication date |
---|---|
EA200700843A1 (ru) | 2007-08-31 |
EA011903B1 (ru) | 2009-06-30 |
CA2582035A1 (en) | 2006-04-20 |
US20080078679A1 (en) | 2008-04-03 |
EP1811062A4 (de) | 2009-04-29 |
EP1811062A1 (de) | 2007-07-25 |
JP4247792B2 (ja) | 2009-04-02 |
JP2006111895A (ja) | 2006-04-27 |
AU2005293038A1 (en) | 2006-04-20 |
NO20072241L (no) | 2007-04-30 |
WO2006040978A1 (ja) | 2006-04-20 |
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