CN100360492C - 制备乙酸的方法 - Google Patents

制备乙酸的方法 Download PDF

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Publication number
CN100360492C
CN100360492C CNB971813620A CN97181362A CN100360492C CN 100360492 C CN100360492 C CN 100360492C CN B971813620 A CNB971813620 A CN B971813620A CN 97181362 A CN97181362 A CN 97181362A CN 100360492 C CN100360492 C CN 100360492C
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CN
China
Prior art keywords
water
acetate
methyl
light ends
stream
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Expired - Fee Related
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CNB971813620A
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English (en)
Chinese (zh)
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CN1244856A (zh
Inventor
D·J·瓦特森
B·L·威廉斯
M·J·穆斯克特
S·J·史密斯
C·T·恩古芸
L·I·巴克尔
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BP Chemicals Ltd
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BP Chemicals Ltd
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Publication of CN1244856A publication Critical patent/CN1244856A/zh
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/10—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
    • C07C51/12—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide on an oxygen-containing group in organic compounds, e.g. alcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
    • C07C51/493—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification whereby carboxylic acid esters are formed
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CNB971813620A 1996-11-19 1997-11-07 制备乙酸的方法 Expired - Fee Related CN100360492C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US08/752,330 1996-11-19
US08/752,330 US5831120A (en) 1996-11-19 1996-11-19 Process for the production of acetic acid

Publications (2)

Publication Number Publication Date
CN1244856A CN1244856A (zh) 2000-02-16
CN100360492C true CN100360492C (zh) 2008-01-09

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ID=25025848

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB971813620A Expired - Fee Related CN100360492C (zh) 1996-11-19 1997-11-07 制备乙酸的方法

Country Status (15)

Country Link
US (1) US5831120A (enExample)
EP (2) EP1114811B1 (enExample)
JP (1) JP4017673B2 (enExample)
KR (1) KR100588278B1 (enExample)
CN (1) CN100360492C (enExample)
AU (1) AU4878097A (enExample)
DE (2) DE69709164T2 (enExample)
ID (1) ID21753A (enExample)
MY (1) MY118914A (enExample)
RU (1) RU2187494C2 (enExample)
SG (1) SG86467A1 (enExample)
TW (1) TW460453B (enExample)
UA (1) UA56199C2 (enExample)
WO (1) WO1998022420A1 (enExample)
ZA (1) ZA9710214B (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101665424B (zh) * 2009-07-16 2012-04-25 北京泽华化学工程有限公司 一种甲醇低压羰基化合成醋酸的方法及其装置

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GB9802027D0 (en) * 1998-01-31 1998-03-25 Bp Chem Int Ltd Chemical process
GB9816385D0 (en) * 1998-07-29 1998-09-23 Bp Chem Int Ltd Process
ATE261426T1 (de) * 1998-08-06 2004-03-15 Haldor Topsoe As Reaktiv distillierungsverfahren zur herstellung von essigsäure auf der basis von dme/methanol carbonylierung
US6211405B1 (en) 1998-10-23 2001-04-03 Celanese International Corporation Addition of iridium to the rhodium/inorganic iodide catalyst system
GB9824011D0 (en) * 1998-11-03 1998-12-30 Bp Chem Int Ltd Process for the production of acetic acid
US6552221B1 (en) 1998-12-18 2003-04-22 Millenium Petrochemicals, Inc. Process control for acetic acid manufacture
US6013834A (en) * 1999-03-04 2000-01-11 Celanese International Corporation Production of vinyl acetate in a catalytic reactor equipped with filter and distribution bed
FR2795410B1 (fr) * 1999-06-22 2002-12-27 Acetex Chimie Procede pour ameliorer la stabilite et/ou eviter la desactivation du catalyseur lors de la fabrication d'acide acetique et/ou d'acetate de methyle
US7115772B2 (en) * 2002-01-11 2006-10-03 Celanese International Corporation Integrated process for producing carbonylation acetic acid, acetic anhydride, or coproduction of each from a methyl acetate by-product stream
GB0222618D0 (en) * 2002-09-30 2002-11-06 Bp Chem Int Ltd Process
US7005541B2 (en) * 2002-12-23 2006-02-28 Celanese International Corporation Low water methanol carbonylation process for high acetic acid production and for water balance control
GB0316756D0 (en) * 2003-07-17 2003-08-20 Bp Chem Int Ltd Process
US7208624B2 (en) * 2004-03-02 2007-04-24 Celanese International Corporation Process for producing acetic acid
US7767848B2 (en) 2005-02-08 2010-08-03 Celanese International Corporation Method of controlling acetic acid process
WO2007071902A1 (en) * 2005-12-21 2007-06-28 Bp Chemicals Limited Carbonylation process
GB0601865D0 (en) * 2006-01-30 2006-03-08 Bp Chem Int Ltd Process
US7989659B2 (en) * 2007-05-17 2011-08-02 Celanese International Corporation Method and apparatus for making acetic acid with improved light ends column productivity
US7902397B2 (en) 2007-10-11 2011-03-08 Celanese International Corporation Method and apparatus for making acetic acid with improved productivity
EP2093209A1 (en) * 2008-02-19 2009-08-26 BP Chemicals Limited Process for the production of acetic acid
CN101503346B (zh) * 2009-03-19 2012-01-11 北京泽华化学工程有限公司 一种甲醇低压羰基化合成醋酸的方法及其装置
JP6139024B2 (ja) 2014-10-02 2017-05-31 セラニーズ・インターナショナル・コーポレーション 酢酸の製造方法
RS59401B1 (sr) 2015-01-30 2019-11-29 Celanese Int Corp Postupci proizvodnje sirćetne kiseline
US9487464B2 (en) 2015-01-30 2016-11-08 Celanese International Corporation Processes for producing acetic acid
SG11201706008YA (en) 2015-01-30 2017-08-30 Celanese Int Corp Processes for producing acetic acid
US9561994B2 (en) 2015-01-30 2017-02-07 Celanese International Corporation Processes for producing acetic acid
US9505696B2 (en) 2015-02-04 2016-11-29 Celanese International Corporation Process to control HI concentration in residuum stream
US9512056B2 (en) 2015-02-04 2016-12-06 Celanese International Corporation Process to control HI concentration in residuum stream
US10413840B2 (en) 2015-02-04 2019-09-17 Celanese International Coporation Process to control HI concentration in residuum stream
US9908835B2 (en) 2015-11-13 2018-03-06 Celanese International Corporation Processes for purifying acetic and hydrating anhydride
KR102639480B1 (ko) 2016-03-01 2024-02-23 주식회사 다이셀 아세트산 제조 방법
GB201710508D0 (en) * 2017-06-30 2017-08-16 Johnson Matthey Davy Technologies Ltd Process
CN114644550B (zh) * 2020-12-21 2024-03-12 大连理工江苏研究院有限公司 一种甲醇羰基化制备乙酸的反应系统及工艺
EP4526656A1 (en) 2022-05-19 2025-03-26 LyondellBasell Acetyls, LLC Methods for improved control of glacial acetic acid processes

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1085540A (zh) * 1992-06-02 1994-04-20 英国石油化学品有限公司 乙酸的生产方法
CN1099378A (zh) * 1993-03-26 1995-03-01 英国石油化学品有限公司 羰基化产物的回收方法
CN1100087A (zh) * 1993-03-31 1995-03-15 罗纳·布朗克化学公司 在以铑和铱为基础的催化剂存在下制备羧酸或相应酯的方法
CN1109463A (zh) * 1993-03-31 1995-10-04 罗纳·布朗克化学公司 在基于铱的催化剂存在下制备羧酸或其酯的方法
WO1996031456A1 (en) * 1995-04-07 1996-10-10 Hoechst Celanese Corporation Recovery of acetic acid from dilute aqueous streams formed during a carbonylation process

Family Cites Families (12)

* Cited by examiner, † Cited by third party
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US3769177A (en) * 1971-11-10 1973-10-30 Monsanto Co Purification of carboxylic acids by plural stage distillation with side stream draw-offs
US3791935A (en) * 1971-11-10 1974-02-12 Monsanto Co Purification of carboxylic acids
US4102922A (en) * 1974-12-30 1978-07-25 Monsanto Company Purification of carbonylation products
US4039395A (en) * 1975-08-11 1977-08-02 Monsanto Company Purification of acetic acid
US4008131A (en) * 1975-12-11 1977-02-15 Monsanto Company Purification of acetic acid
US4435595A (en) * 1982-04-26 1984-03-06 Eastman Kodak Company Reactive distillation process for the production of methyl acetate
ZA853339B (en) * 1984-05-03 1985-12-24 Celanese Corp Methanol carbonylation process
US4939294A (en) * 1989-05-22 1990-07-03 Eastman Kodak Company Preparation of ultra high purity methyl acetate
US5672743A (en) * 1993-09-10 1997-09-30 Bp Chemicals Limited Process for the production of acetic acid
US5352415A (en) * 1993-09-29 1994-10-04 Hoechst Celanese Corporation Control system for acetic acid manufacturing process
GB9503385D0 (en) * 1995-02-21 1995-04-12 Bp Chem Int Ltd Process
AU2760597A (en) * 1996-05-24 1998-01-05 Governors Of The University Of Alberta, The Distillation process

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1085540A (zh) * 1992-06-02 1994-04-20 英国石油化学品有限公司 乙酸的生产方法
CN1099378A (zh) * 1993-03-26 1995-03-01 英国石油化学品有限公司 羰基化产物的回收方法
CN1100087A (zh) * 1993-03-31 1995-03-15 罗纳·布朗克化学公司 在以铑和铱为基础的催化剂存在下制备羧酸或相应酯的方法
CN1109463A (zh) * 1993-03-31 1995-10-04 罗纳·布朗克化学公司 在基于铱的催化剂存在下制备羧酸或其酯的方法
WO1996031456A1 (en) * 1995-04-07 1996-10-10 Hoechst Celanese Corporation Recovery of acetic acid from dilute aqueous streams formed during a carbonylation process

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101665424B (zh) * 2009-07-16 2012-04-25 北京泽华化学工程有限公司 一种甲醇低压羰基化合成醋酸的方法及其装置

Also Published As

Publication number Publication date
JP2001505199A (ja) 2001-04-17
TW460453B (en) 2001-10-21
ID21753A (id) 1999-07-22
CN1244856A (zh) 2000-02-16
UA56199C2 (uk) 2003-05-15
SG86467A1 (en) 2002-02-19
DE69734166T2 (de) 2006-06-29
RU2187494C2 (ru) 2002-08-20
WO1998022420A1 (en) 1998-05-28
DE69734166D1 (de) 2005-10-13
MY118914A (en) 2005-02-28
KR20000053339A (ko) 2000-08-25
EP0942897A1 (en) 1999-09-22
KR100588278B1 (ko) 2006-06-09
DE69709164D1 (de) 2002-01-24
EP1114811A1 (en) 2001-07-11
DE69709164T2 (de) 2002-07-11
ZA9710214B (en) 1999-05-12
JP4017673B2 (ja) 2007-12-05
AU4878097A (en) 1998-06-10
EP0942897B1 (en) 2001-12-12
EP1114811B1 (en) 2005-09-07
US5831120A (en) 1998-11-03

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Granted publication date: 20080109

Termination date: 20161107