CH634109A5 - Verfahren zur herstellung von dextrosepulver mit einem wesentlichen gehalt an beta-dextroseanhydrid. - Google Patents
Verfahren zur herstellung von dextrosepulver mit einem wesentlichen gehalt an beta-dextroseanhydrid. Download PDFInfo
- Publication number
- CH634109A5 CH634109A5 CH1201577A CH1201577A CH634109A5 CH 634109 A5 CH634109 A5 CH 634109A5 CH 1201577 A CH1201577 A CH 1201577A CH 1201577 A CH1201577 A CH 1201577A CH 634109 A5 CH634109 A5 CH 634109A5
- Authority
- CH
- Switzerland
- Prior art keywords
- dextrose
- concentrated
- solution
- anhydride
- powder
- Prior art date
Links
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 title claims description 62
- 239000008121 dextrose Substances 0.000 title claims description 36
- 239000000843 powder Substances 0.000 title claims description 33
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- 238000000034 method Methods 0.000 claims description 44
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims description 40
- -1 β-dextrose anhydride Chemical class 0.000 claims description 32
- 239000013078 crystal Substances 0.000 claims description 29
- 239000000243 solution Substances 0.000 claims description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 18
- 229920002472 Starch Polymers 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 7
- 235000019698 starch Nutrition 0.000 claims description 6
- 239000008107 starch Substances 0.000 claims description 6
- 239000007864 aqueous solution Substances 0.000 claims description 2
- 239000000126 substance Substances 0.000 claims 1
- 229960001031 glucose Drugs 0.000 description 29
- 238000002425 crystallisation Methods 0.000 description 17
- 230000008025 crystallization Effects 0.000 description 15
- 239000007787 solid Substances 0.000 description 9
- 230000015572 biosynthetic process Effects 0.000 description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
- 239000013081 microcrystal Substances 0.000 description 6
- GZCGUPFRVQAUEE-SLPGGIOYSA-N aldehydo-D-glucose Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O GZCGUPFRVQAUEE-SLPGGIOYSA-N 0.000 description 5
- 229940089206 anhydrous dextrose Drugs 0.000 description 5
- 238000010411 cooking Methods 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 229960000673 dextrose monohydrate Drugs 0.000 description 4
- 229920002261 Corn starch Polymers 0.000 description 3
- WQZGKKKJIJFFOK-DVKNGEFBSA-N alpha-D-glucose Chemical compound OC[C@H]1O[C@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-DVKNGEFBSA-N 0.000 description 3
- 239000008120 corn starch Substances 0.000 description 3
- 238000000227 grinding Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 239000003456 ion exchange resin Substances 0.000 description 3
- 229920003303 ion-exchange polymer Polymers 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 229940088598 enzyme Drugs 0.000 description 2
- 238000010899 nucleation Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 229920001592 potato starch Polymers 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 238000001694 spray drying Methods 0.000 description 2
- 238000010561 standard procedure Methods 0.000 description 2
- SPFMQWBKVUQXJV-BTVCFUMJSA-N (2r,3s,4r,5r)-2,3,4,5,6-pentahydroxyhexanal;hydrate Chemical compound O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O SPFMQWBKVUQXJV-BTVCFUMJSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 244000017020 Ipomoea batatas Species 0.000 description 1
- 235000002678 Ipomoea batatas Nutrition 0.000 description 1
- 150000008064 anhydrides Chemical class 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 229940079919 digestives enzyme preparation Drugs 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 230000009969 flowable effect Effects 0.000 description 1
- 238000011081 inoculation Methods 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000010327 methods by industry Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
- 229940100445 wheat starch Drugs 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K1/00—Glucose; Glucose-containing syrups
- C13K1/10—Crystallisation
Landscapes
- Chemical & Material Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Saccharide Compounds (AREA)
- Seasonings (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US05/729,325 US4297146A (en) | 1976-10-04 | 1976-10-04 | Method for the production of powdered dextrose |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH634109A5 true CH634109A5 (de) | 1983-01-14 |
Family
ID=24930534
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH1201577A CH634109A5 (de) | 1976-10-04 | 1977-09-30 | Verfahren zur herstellung von dextrosepulver mit einem wesentlichen gehalt an beta-dextroseanhydrid. |
Country Status (26)
| Country | Link |
|---|---|
| US (1) | US4297146A (enExample) |
| JP (1) | JPS5352637A (enExample) |
| AR (1) | AR212892A1 (enExample) |
| AT (1) | AT359446B (enExample) |
| AU (1) | AU511587B2 (enExample) |
| BE (1) | BE859296A (enExample) |
| CA (1) | CA1094058A (enExample) |
| CH (1) | CH634109A5 (enExample) |
| DE (1) | DE2744099A1 (enExample) |
| DK (1) | DK436577A (enExample) |
| ES (1) | ES462861A1 (enExample) |
| FI (1) | FI62337C (enExample) |
| FR (1) | FR2366361A1 (enExample) |
| GB (1) | GB1542167A (enExample) |
| HU (1) | HU176497B (enExample) |
| IT (1) | IT1087724B (enExample) |
| MX (1) | MX4373E (enExample) |
| MY (1) | MY8000082A (enExample) |
| NL (1) | NL7710831A (enExample) |
| NZ (1) | NZ185327A (enExample) |
| RO (1) | RO72591A (enExample) |
| SE (1) | SE7711022L (enExample) |
| SU (1) | SU751333A3 (enExample) |
| TR (1) | TR19659A (enExample) |
| YU (1) | YU237677A (enExample) |
| ZA (1) | ZA775869B (enExample) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4888060A (en) * | 1985-06-21 | 1989-12-19 | A. E. Staley Manufacturing Company | Enrichment of fructose syrups |
| DK159488A (da) * | 1988-03-23 | 1989-09-24 | Danske Sukkerfab | Fremgangsmaade til kontinuerlig toerring eller inddampning af et materiale og et apparat til udoevelse af fremgangsmaaden |
| FI97625C (fi) * | 1995-03-01 | 1997-01-27 | Xyrofin Oy | Menetelmä ksyloosin kiteyttämiseksi vesiliuoksista |
| FI952065A0 (fi) * | 1995-03-01 | 1995-04-28 | Xyrofin Oy | Foerfarande foer tillvaratagande av en kristalliserbar organisk foerening |
| FR2787811B1 (fr) * | 1998-12-24 | 2001-03-02 | Roquette Freres | Dextrose pulverulent et son procede de preparation |
| US6527868B2 (en) * | 1999-12-15 | 2003-03-04 | Roquette Freres | Dextrose in powder form and a process for the preparation thereof |
| FR2877186B1 (fr) * | 2004-10-29 | 2007-02-09 | Roquette Freres | Utilisation non alimentaire et non pharmaceutique d'une composition de dextrose anhydre selectionnee |
| RU2521510C1 (ru) * | 2012-12-29 | 2014-06-27 | Государственное научное учреждение Всероссийский научно-исследовательский институт крахмалопродуктов Российской академии сельскохозяйственных наук | Способ получения кристаллической ангидридной глюкозы |
| EP3886819A1 (en) | 2018-11-30 | 2021-10-06 | Amerilab Technologies, Inc. | Rapidly disintegrating effervescent tablets and methods of making the same |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2324113A (en) * | 1941-07-01 | 1943-07-13 | American Maize Prod Co | Method of making dextrose |
| FR1052692A (fr) * | 1951-09-22 | 1954-01-26 | Corn Prod Refining Co | Procédé de production de bêta-dextrose |
| US3085914A (en) * | 1959-06-30 | 1963-04-16 | Corn Products Co | Novel crystalline sugar products |
| US3197338A (en) * | 1962-06-21 | 1965-07-27 | Staley Mfg Co A E | Method of producing dried starch conversion product |
| NL300874A (enExample) * | 1962-11-23 | |||
| FR1384712A (fr) * | 1963-11-22 | 1965-01-08 | Corn Products Co | Nouveau procédé de fabrication du dextrose |
| GB1252523A (enExample) * | 1968-04-06 | 1971-11-03 | ||
| US3713978A (en) * | 1968-11-22 | 1973-01-30 | Hayashibara Co | Process for preparing powdery starch sugars |
| US3748175A (en) * | 1969-04-06 | 1973-07-24 | Tokai Togyo Kk | Process for preparing crystalline anhydrous beta dextrose |
| US3650829A (en) * | 1969-08-06 | 1972-03-21 | Cpc International Inc | Method of producing granular dextrose |
| US3752877A (en) * | 1969-08-27 | 1973-08-14 | Parsons Co Ralph M | Recovery of sulfur compounds from tail gases |
| GB1461070A (en) * | 1970-07-17 | 1977-01-13 | Shell Int Research | Process for reducing the total sulphur content of claus- off- gases |
| US3864460A (en) * | 1973-07-12 | 1975-02-04 | Nrg Inc | Method for removing hydrogen sulfide from hydrocarbon gas streams without pollution of the atmosphere |
| US3981739A (en) * | 1974-08-30 | 1976-09-21 | Amstar Corporation | Continuous crystallization |
| US4059460A (en) * | 1975-11-07 | 1977-11-22 | A. E. Staley Manufacturing Company | Solid anhydrous dextrose |
| US4041130A (en) * | 1975-12-29 | 1977-08-09 | The Ralph M. Parsons Company | Process for desulfurization of coke oven gas |
-
1976
- 1976-10-04 US US05/729,325 patent/US4297146A/en not_active Expired - Lifetime
-
1977
- 1977-09-30 HU HU77CE1141A patent/HU176497B/hu unknown
- 1977-09-30 CH CH1201577A patent/CH634109A5/de not_active IP Right Cessation
- 1977-09-30 DE DE19772744099 patent/DE2744099A1/de not_active Withdrawn
- 1977-10-01 RO RO7791723A patent/RO72591A/ro unknown
- 1977-10-03 SE SE7711022A patent/SE7711022L/ not_active Application Discontinuation
- 1977-10-03 GB GB7741020A patent/GB1542167A/en not_active Expired
- 1977-10-03 ES ES462861A patent/ES462861A1/es not_active Expired
- 1977-10-03 JP JP11798077A patent/JPS5352637A/ja active Granted
- 1977-10-03 SU SU772528901A patent/SU751333A3/ru active
- 1977-10-03 TR TR19659A patent/TR19659A/xx unknown
- 1977-10-03 BE BE2056309A patent/BE859296A/xx unknown
- 1977-10-03 FI FI772905A patent/FI62337C/fi not_active IP Right Cessation
- 1977-10-03 DK DK436577A patent/DK436577A/da not_active Application Discontinuation
- 1977-10-03 NL NL7710831A patent/NL7710831A/xx not_active Application Discontinuation
- 1977-10-03 IT IT28213/77A patent/IT1087724B/it active
- 1977-10-03 MX MX776448U patent/MX4373E/es unknown
- 1977-10-03 NZ NZ185327A patent/NZ185327A/xx unknown
- 1977-10-03 FR FR7729700A patent/FR2366361A1/fr active Granted
- 1977-10-03 AT AT702777A patent/AT359446B/de not_active IP Right Cessation
- 1977-10-03 ZA ZA00775869A patent/ZA775869B/xx unknown
- 1977-10-03 CA CA287,942A patent/CA1094058A/en not_active Expired
- 1977-10-04 AR AR269431A patent/AR212892A1/es active
- 1977-10-04 AU AU29341/77A patent/AU511587B2/en not_active Expired
- 1977-10-04 YU YU02376/77A patent/YU237677A/xx unknown
-
1980
- 1980-12-30 MY MY82/80A patent/MY8000082A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DE2744099A1 (de) | 1978-04-06 |
| NZ185327A (en) | 1979-10-25 |
| MX4373E (es) | 1982-04-19 |
| FR2366361B1 (enExample) | 1983-02-04 |
| AR212892A1 (es) | 1978-10-31 |
| RO72591A (ro) | 1981-06-26 |
| SE7711022L (sv) | 1978-04-05 |
| AU2934177A (en) | 1979-04-12 |
| BE859296A (fr) | 1978-04-03 |
| DK436577A (da) | 1978-04-05 |
| FI62337B (fi) | 1982-08-31 |
| NL7710831A (nl) | 1978-04-06 |
| JPS5719960B2 (enExample) | 1982-04-26 |
| AU511587B2 (en) | 1980-08-28 |
| US4297146A (en) | 1981-10-27 |
| IT1087724B (it) | 1985-06-04 |
| TR19659A (tr) | 1979-09-17 |
| MY8000082A (en) | 1980-12-31 |
| ATA702777A (de) | 1980-03-15 |
| FI772905A7 (fi) | 1978-04-05 |
| YU237677A (en) | 1982-10-31 |
| GB1542167A (en) | 1979-03-14 |
| FR2366361A1 (fr) | 1978-04-28 |
| CA1094058A (en) | 1981-01-20 |
| FI62337C (fi) | 1982-12-10 |
| JPS5352637A (en) | 1978-05-13 |
| ES462861A1 (es) | 1978-06-01 |
| ZA775869B (en) | 1978-11-29 |
| SU751333A3 (ru) | 1980-07-23 |
| AT359446B (de) | 1980-11-10 |
| HU176497B (en) | 1981-03-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PL | Patent ceased | ||
| PL | Patent ceased |