CH557298A - Verfahren zur herstellung von magnesiumphosphid. - Google Patents
Verfahren zur herstellung von magnesiumphosphid.Info
- Publication number
- CH557298A CH557298A CH144071A CH144071A CH557298A CH 557298 A CH557298 A CH 557298A CH 144071 A CH144071 A CH 144071A CH 144071 A CH144071 A CH 144071A CH 557298 A CH557298 A CH 557298A
- Authority
- CH
- Switzerland
- Prior art keywords
- magnesium
- phosphide
- reaction
- magnesium phosphide
- food
- Prior art date
Links
- 239000005953 Magnesium phosphide Substances 0.000 title claims description 23
- 238000000034 method Methods 0.000 title claims description 22
- 238000006243 chemical reaction Methods 0.000 claims description 26
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 15
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 14
- 229910052749 magnesium Inorganic materials 0.000 claims description 13
- 239000011777 magnesium Substances 0.000 claims description 13
- 239000000126 substance Substances 0.000 claims description 13
- 235000013305 food Nutrition 0.000 claims description 11
- 238000004519 manufacturing process Methods 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 8
- 239000005662 Paraffin oil Substances 0.000 claims description 6
- 230000000694 effects Effects 0.000 claims description 4
- 229930195733 hydrocarbon Natural products 0.000 claims description 4
- 150000002430 hydrocarbons Chemical class 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 4
- 239000007787 solid Substances 0.000 claims description 4
- 239000004215 Carbon black (E152) Substances 0.000 claims description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 3
- 239000001301 oxygen Substances 0.000 claims description 3
- 229910052760 oxygen Inorganic materials 0.000 claims description 3
- 241000607479 Yersinia pestis Species 0.000 claims description 2
- 239000012188 paraffin wax Substances 0.000 claims description 2
- 229930195734 saturated hydrocarbon Natural products 0.000 claims description 2
- 230000001419 dependent effect Effects 0.000 claims 4
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims 1
- 229910000287 alkaline earth metal oxide Inorganic materials 0.000 claims 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims 1
- 239000000654 additive Substances 0.000 description 6
- IHGSAQHSAGRWNI-UHFFFAOYSA-N 1-(4-bromophenyl)-2,2,2-trifluoroethanone Chemical compound FC(F)(F)C(=O)C1=CC=C(Br)C=C1 IHGSAQHSAGRWNI-UHFFFAOYSA-N 0.000 description 5
- 239000002360 explosive Substances 0.000 description 4
- 229910052698 phosphorus Inorganic materials 0.000 description 4
- 239000011574 phosphorus Substances 0.000 description 4
- 229910001385 heavy metal Inorganic materials 0.000 description 3
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 2
- 241000283984 Rodentia Species 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 239000003085 diluting agent Substances 0.000 description 2
- 239000002316 fumigant Substances 0.000 description 2
- 238000003958 fumigation Methods 0.000 description 2
- 239000000395 magnesium oxide Substances 0.000 description 2
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 238000010943 off-gassing Methods 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 231100000331 toxic Toxicity 0.000 description 2
- 230000002588 toxic effect Effects 0.000 description 2
- YLZOPXRUQYQQID-UHFFFAOYSA-N 3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)-1-[4-[2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidin-5-yl]piperazin-1-yl]propan-1-one Chemical compound N1N=NC=2CN(CCC=21)CCC(=O)N1CCN(CC1)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F YLZOPXRUQYQQID-UHFFFAOYSA-N 0.000 description 1
- PGYDGBCATBINCB-UHFFFAOYSA-N 4-diethoxyphosphoryl-n,n-dimethylaniline Chemical compound CCOP(=O)(OCC)C1=CC=C(N(C)C)C=C1 PGYDGBCATBINCB-UHFFFAOYSA-N 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 239000006009 Calcium phosphide Substances 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- XYFCBTPGUUZFHI-UHFFFAOYSA-N Phosphine Chemical compound P XYFCBTPGUUZFHI-UHFFFAOYSA-N 0.000 description 1
- 239000006011 Zinc phosphide Substances 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000007133 aluminothermic reaction Methods 0.000 description 1
- 235000019270 ammonium chloride Nutrition 0.000 description 1
- 230000002238 attenuated effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- WMWXXXSCZVGQAR-UHFFFAOYSA-N dialuminum;oxygen(2-);hydrate Chemical compound O.[O-2].[O-2].[O-2].[Al+3].[Al+3] WMWXXXSCZVGQAR-UHFFFAOYSA-N 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 230000007717 exclusion Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 description 1
- 239000001095 magnesium carbonate Substances 0.000 description 1
- 229910000021 magnesium carbonate Inorganic materials 0.000 description 1
- GVALZJMUIHGIMD-UHFFFAOYSA-H magnesium phosphate Chemical compound [Mg+2].[Mg+2].[Mg+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O GVALZJMUIHGIMD-UHFFFAOYSA-H 0.000 description 1
- 239000004137 magnesium phosphate Substances 0.000 description 1
- 229960002261 magnesium phosphate Drugs 0.000 description 1
- 229910000157 magnesium phosphate Inorganic materials 0.000 description 1
- 235000010994 magnesium phosphates Nutrition 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000010534 mechanism of action Effects 0.000 description 1
- 238000010309 melting process Methods 0.000 description 1
- 238000013021 overheating Methods 0.000 description 1
- HOKBIQDJCNTWST-UHFFFAOYSA-N phosphanylidenezinc;zinc Chemical compound [Zn].[Zn]=P.[Zn]=P HOKBIQDJCNTWST-UHFFFAOYSA-N 0.000 description 1
- 150000003016 phosphoric acids Chemical class 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 239000003128 rodenticide Substances 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 229940048462 zinc phosphide Drugs 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/26—Phosphorus; Compounds thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/06—Hydrogen phosphides
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Dentistry (AREA)
- Zoology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Pest Control & Pesticides (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Environmental Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Fireproofing Substances (AREA)
- Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEF0048910 | 1966-04-07 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH557298A true CH557298A (de) | 1974-12-31 |
Family
ID=7102567
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH144071A CH557298A (de) | 1966-04-07 | 1967-04-07 | Verfahren zur herstellung von magnesiumphosphid. |
| CH495067A CH507872A (de) | 1966-04-07 | 1967-04-07 | Verfahren zur Herstellung von Magnesiumphosphid |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH495067A CH507872A (de) | 1966-04-07 | 1967-04-07 | Verfahren zur Herstellung von Magnesiumphosphid |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US3532464A (OSRAM) |
| AT (4) | AT324278B (OSRAM) |
| BE (1) | BE695703A (OSRAM) |
| CA (1) | CA924479A (OSRAM) |
| CH (2) | CH557298A (OSRAM) |
| DE (1) | DE1567520B2 (OSRAM) |
| ES (1) | ES338377A1 (OSRAM) |
| FR (1) | FR1514622A (OSRAM) |
| GB (1) | GB1146955A (OSRAM) |
| NL (1) | NL158761B (OSRAM) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2400842A1 (fr) * | 1977-07-01 | 1979-03-23 | Freyberg Chem Fab Werner | Produit a base de phosphure metallique pour la lutte contre les parasites et les animaux nuisibles et son procede d'obtention |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4013756A (en) * | 1971-10-12 | 1977-03-22 | Hooker Chemicals & Plastics Corporation | Process for preparing phosphine |
| DD112744A1 (OSRAM) * | 1973-11-14 | 1975-05-05 | ||
| DE2825534C2 (de) * | 1978-06-10 | 1983-11-24 | Degesch Gmbh, 6000 Frankfurt | Tablette zur Bekämpfung von Wirbeltieren |
| DE2945647C2 (de) * | 1979-11-12 | 1990-01-04 | Degesch Gmbh, 6000 Frankfurt | Verfahren zur Herstellung von Aluminiumphosphid und/oder Magnesiumphosphid |
| DE3117393A1 (de) * | 1981-05-02 | 1982-11-11 | Degesch Gmbh, 6000 Frankfurt | Verfahren zur herstellung der phosphide von aluminium oder magnesium |
| WO1993025075A1 (en) * | 1992-06-05 | 1993-12-23 | Commonwealth Scientific And Industrial Research Organisation | Formulations, method and apparatus for the controlled generation of phosphine |
| GB9511495D0 (en) * | 1995-06-07 | 1995-08-02 | Degesch De Chile Ltda | Composition, process and apparatus for producing phosphine - containing gas |
| DE19831987A1 (de) | 1998-07-16 | 2000-01-20 | Bayer Ag | Diphenylimidazoline |
| CN1107447C (zh) * | 1999-04-27 | 2003-05-07 | 华仁沈阳农药有限公司 | 仓储熏蒸杀虫剂磷化镁的合成工艺 |
| CN102083764B (zh) * | 2008-06-26 | 2016-11-09 | 卡利克斯有限公司 | 粘结剂组合物 |
| CN104058376B (zh) * | 2013-03-21 | 2016-08-03 | 中国科学院物理研究所 | 一种铁磁半导体材料Li(Zn,Mn)P及其制备方法 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA538958A (en) * | 1957-04-02 | Deutsche Gold- Und Silber-Scheideanstalt | Process for the production of phosphides not spontaneously inflammable | |
| US1599618A (en) * | 1923-02-28 | 1926-09-14 | Koehler William | Process for forming metal compounds and mixtures involving phosphorus |
-
1966
- 1966-04-07 DE DE1567520A patent/DE1567520B2/de not_active Ceased
-
1967
- 1967-03-03 NL NL6703480.A patent/NL158761B/xx not_active IP Right Cessation
- 1967-03-07 AT AT78971A patent/AT324278B/de not_active IP Right Cessation
- 1967-03-07 AT AT216567A patent/AT294008B/de not_active IP Right Cessation
- 1967-03-07 AT AT78871*7A patent/AT329518B/de not_active IP Right Cessation
- 1967-03-07 AT AT78871*A patent/ATA78871A/de unknown
- 1967-03-14 FR FR98770A patent/FR1514622A/fr not_active Expired
- 1967-03-17 BE BE695703D patent/BE695703A/xx not_active IP Right Cessation
- 1967-03-21 CA CA985785A patent/CA924479A/en not_active Expired
- 1967-03-22 ES ES338377A patent/ES338377A1/es not_active Expired
- 1967-04-04 US US628308A patent/US3532464A/en not_active Expired - Lifetime
- 1967-04-06 GB GB15818/67A patent/GB1146955A/en not_active Expired
- 1967-04-07 CH CH144071A patent/CH557298A/de not_active IP Right Cessation
- 1967-04-07 CH CH495067A patent/CH507872A/de not_active IP Right Cessation
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2400842A1 (fr) * | 1977-07-01 | 1979-03-23 | Freyberg Chem Fab Werner | Produit a base de phosphure metallique pour la lutte contre les parasites et les animaux nuisibles et son procede d'obtention |
Also Published As
| Publication number | Publication date |
|---|---|
| FR1514622A (fr) | 1968-02-23 |
| ES338377A1 (es) | 1968-04-01 |
| GB1146955A (en) | 1969-03-26 |
| ATA78871A (de) | 1975-08-15 |
| CH507872A (de) | 1971-05-31 |
| AT294008B (de) | 1971-11-10 |
| AT329518B (de) | 1976-05-10 |
| DE1567520B2 (de) | 1973-01-04 |
| CA924479A (en) | 1973-04-17 |
| AT324278B (de) | 1975-08-25 |
| US3532464A (en) | 1970-10-06 |
| NL158761B (nl) | 1978-12-15 |
| DE1567520A1 (de) | 1970-04-16 |
| NL6703480A (OSRAM) | 1967-10-09 |
| BE695703A (OSRAM) | 1967-09-18 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PL | Patent ceased |