CA2398452C - Color stable pigmented polymeric films - Google Patents
Color stable pigmented polymeric films Download PDFInfo
- Publication number
- CA2398452C CA2398452C CA2398452A CA2398452A CA2398452C CA 2398452 C CA2398452 C CA 2398452C CA 2398452 A CA2398452 A CA 2398452A CA 2398452 A CA2398452 A CA 2398452A CA 2398452 C CA2398452 C CA 2398452C
- Authority
- CA
- Canada
- Prior art keywords
- film
- layer
- percent
- particulate pigment
- pigment
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000000049 pigment Substances 0.000 claims abstract description 72
- 239000010410 layer Substances 0.000 claims abstract description 71
- 229920001169 thermoplastic Polymers 0.000 claims abstract description 21
- 230000005540 biological transmission Effects 0.000 claims abstract description 19
- 239000002861 polymer material Substances 0.000 claims abstract description 19
- 238000001429 visible spectrum Methods 0.000 claims abstract description 12
- 239000002356 single layer Substances 0.000 claims abstract description 9
- 239000010408 film Substances 0.000 claims description 93
- 239000006185 dispersion Substances 0.000 claims description 53
- -1 laminate Substances 0.000 claims description 43
- 239000000203 mixture Substances 0.000 claims description 38
- 238000000034 method Methods 0.000 claims description 32
- 229920000642 polymer Polymers 0.000 claims description 27
- 229920000139 polyethylene terephthalate Polymers 0.000 claims description 23
- 239000005020 polyethylene terephthalate Substances 0.000 claims description 23
- 229920000728 polyester Polymers 0.000 claims description 20
- 230000008569 process Effects 0.000 claims description 18
- 239000006229 carbon black Substances 0.000 claims description 15
- 238000009833 condensation Methods 0.000 claims description 12
- 230000005494 condensation Effects 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 12
- 238000006243 chemical reaction Methods 0.000 claims description 11
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 9
- 238000000576 coating method Methods 0.000 claims description 9
- 230000003746 surface roughness Effects 0.000 claims description 7
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 6
- 239000012788 optical film Substances 0.000 claims description 6
- 229910052726 zirconium Inorganic materials 0.000 claims description 5
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 4
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 4
- VTYYLEPIZMXCLO-UHFFFAOYSA-L calcium carbonate Substances [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 4
- 229910017052 cobalt Inorganic materials 0.000 claims description 4
- 239000010941 cobalt Substances 0.000 claims description 4
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 4
- 229910052802 copper Inorganic materials 0.000 claims description 4
- 239000010949 copper Substances 0.000 claims description 4
- 229910052708 sodium Inorganic materials 0.000 claims description 4
- 239000011734 sodium Substances 0.000 claims description 4
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims description 3
- 229910052782 aluminium Inorganic materials 0.000 claims description 3
- 229910052793 cadmium Inorganic materials 0.000 claims description 3
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 claims description 3
- ZCDOYSPFYFSLEW-UHFFFAOYSA-N chromate(2-) Chemical class [O-][Cr]([O-])(=O)=O ZCDOYSPFYFSLEW-UHFFFAOYSA-N 0.000 claims description 3
- 239000011248 coating agent Substances 0.000 claims description 3
- 150000001875 compounds Chemical class 0.000 claims description 3
- 235000019239 indanthrene blue RS Nutrition 0.000 claims description 3
- 150000002484 inorganic compounds Chemical class 0.000 claims description 3
- 229910010272 inorganic material Inorganic materials 0.000 claims description 3
- 229910052742 iron Inorganic materials 0.000 claims description 3
- 239000011133 lead Substances 0.000 claims description 3
- 229910052719 titanium Inorganic materials 0.000 claims description 3
- 239000010936 titanium Substances 0.000 claims description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 2
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims description 2
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 2
- 229910000323 aluminium silicate Inorganic materials 0.000 claims description 2
- 150000004056 anthraquinones Chemical class 0.000 claims description 2
- 229910052787 antimony Inorganic materials 0.000 claims description 2
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 claims description 2
- 229910000410 antimony oxide Inorganic materials 0.000 claims description 2
- 125000000751 azo group Chemical group [*]N=N[*] 0.000 claims description 2
- 229910052788 barium Inorganic materials 0.000 claims description 2
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 claims description 2
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical class [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 claims description 2
- HFACYLZERDEVSX-UHFFFAOYSA-N benzidine Chemical class C1=CC(N)=CC=C1C1=CC=C(N)C=C1 HFACYLZERDEVSX-UHFFFAOYSA-N 0.000 claims description 2
- 150000008641 benzimidazolones Chemical class 0.000 claims description 2
- 239000001045 blue dye Substances 0.000 claims description 2
- FRLJSGOEGLARCA-UHFFFAOYSA-N cadmium sulfide Chemical class [S-2].[Cd+2] FRLJSGOEGLARCA-UHFFFAOYSA-N 0.000 claims description 2
- UHYPYGJEEGLRJD-UHFFFAOYSA-N cadmium(2+);selenium(2-) Chemical class [Se-2].[Cd+2] UHYPYGJEEGLRJD-UHFFFAOYSA-N 0.000 claims description 2
- 229910052791 calcium Inorganic materials 0.000 claims description 2
- 239000011575 calcium Substances 0.000 claims description 2
- 235000010216 calcium carbonate Nutrition 0.000 claims description 2
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical class [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 claims description 2
- 235000011132 calcium sulphate Nutrition 0.000 claims description 2
- 229910052804 chromium Inorganic materials 0.000 claims description 2
- 239000011651 chromium Substances 0.000 claims description 2
- UOUJSJZBMCDAEU-UHFFFAOYSA-N chromium(3+);oxygen(2-) Chemical class [O-2].[O-2].[O-2].[Cr+3].[Cr+3] UOUJSJZBMCDAEU-UHFFFAOYSA-N 0.000 claims description 2
- 125000000664 diazo group Chemical group [N-]=[N+]=[*] 0.000 claims description 2
- 150000005125 dioxazines Chemical class 0.000 claims description 2
- 229910021432 inorganic complex Inorganic materials 0.000 claims description 2
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims description 2
- 235000013980 iron oxide Nutrition 0.000 claims description 2
- VBMVTYDPPZVILR-UHFFFAOYSA-N iron(2+);oxygen(2-) Chemical class [O-2].[Fe+2] VBMVTYDPPZVILR-UHFFFAOYSA-N 0.000 claims description 2
- PXZQEOJJUGGUIB-UHFFFAOYSA-N isoindolin-1-one Chemical class C1=CC=C2C(=O)NCC2=C1 PXZQEOJJUGGUIB-UHFFFAOYSA-N 0.000 claims description 2
- GWVMLCQWXVFZCN-UHFFFAOYSA-N isoindoline Chemical class C1=CC=C2CNCC2=C1 GWVMLCQWXVFZCN-UHFFFAOYSA-N 0.000 claims description 2
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 229910052750 molybdenum Inorganic materials 0.000 claims description 2
- 239000011733 molybdenum Substances 0.000 claims description 2
- VTRUBDSFZJNXHI-UHFFFAOYSA-N oxoantimony Chemical class [Sb]=O VTRUBDSFZJNXHI-UHFFFAOYSA-N 0.000 claims description 2
- SOQBVABWOPYFQZ-UHFFFAOYSA-N oxygen(2-);titanium(4+) Chemical class [O-2].[O-2].[Ti+4] SOQBVABWOPYFQZ-UHFFFAOYSA-N 0.000 claims description 2
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical class [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 claims description 2
- 150000002979 perylenes Chemical class 0.000 claims description 2
- 230000019612 pigmentation Effects 0.000 claims description 2
- FYNROBRQIVCIQF-UHFFFAOYSA-N pyrrolo[3,2-b]pyrrole-5,6-dione Chemical class C1=CN=C2C(=O)C(=O)N=C21 FYNROBRQIVCIQF-UHFFFAOYSA-N 0.000 claims description 2
- 150000003839 salts Chemical class 0.000 claims description 2
- 150000004760 silicates Chemical class 0.000 claims description 2
- 229910052710 silicon Inorganic materials 0.000 claims description 2
- 239000010703 silicon Substances 0.000 claims description 2
- 239000000377 silicon dioxide Substances 0.000 claims description 2
- 150000003467 sulfuric acid derivatives Chemical class 0.000 claims description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titanium dioxide Inorganic materials O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 2
- 235000010215 titanium dioxide Nutrition 0.000 claims description 2
- 229910052725 zinc Inorganic materials 0.000 claims description 2
- 239000011701 zinc Substances 0.000 claims description 2
- 235000014692 zinc oxide Nutrition 0.000 claims description 2
- RNWHGQJWIACOKP-UHFFFAOYSA-N zinc;oxygen(2-) Chemical class [O-2].[Zn+2] RNWHGQJWIACOKP-UHFFFAOYSA-N 0.000 claims description 2
- DRDVZXDWVBGGMH-UHFFFAOYSA-N zinc;sulfide Chemical class [S-2].[Zn+2] DRDVZXDWVBGGMH-UHFFFAOYSA-N 0.000 claims description 2
- 229910001928 zirconium oxide Inorganic materials 0.000 claims description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims 1
- 239000001055 blue pigment Substances 0.000 claims 1
- 230000003287 optical effect Effects 0.000 abstract description 54
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 87
- 239000002245 particle Substances 0.000 description 41
- 239000004594 Masterbatch (MB) Substances 0.000 description 28
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 15
- 238000011068 loading method Methods 0.000 description 15
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 14
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 13
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 description 13
- 239000001267 polyvinylpyrrolidone Substances 0.000 description 13
- 235000019241 carbon black Nutrition 0.000 description 12
- 238000010276 construction Methods 0.000 description 12
- 238000005266 casting Methods 0.000 description 11
- DTQVDTLACAAQTR-UHFFFAOYSA-N Trifluoroacetic acid Chemical compound OC(=O)C(F)(F)F DTQVDTLACAAQTR-UHFFFAOYSA-N 0.000 description 10
- WOZVHXUHUFLZGK-UHFFFAOYSA-N dimethyl terephthalate Chemical compound COC(=O)C1=CC=C(C(=O)OC)C=C1 WOZVHXUHUFLZGK-UHFFFAOYSA-N 0.000 description 10
- 239000003921 oil Substances 0.000 description 9
- 239000011324 bead Substances 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- 238000000386 microscopy Methods 0.000 description 7
- 230000007935 neutral effect Effects 0.000 description 7
- 229910052757 nitrogen Inorganic materials 0.000 description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
- 238000005054 agglomeration Methods 0.000 description 6
- 230000002776 aggregation Effects 0.000 description 6
- 238000013019 agitation Methods 0.000 description 6
- 238000004458 analytical method Methods 0.000 description 6
- 229910052751 metal Inorganic materials 0.000 description 6
- 239000002184 metal Substances 0.000 description 6
- 238000006116 polymerization reaction Methods 0.000 description 6
- 239000000080 wetting agent Substances 0.000 description 6
- 238000010521 absorption reaction Methods 0.000 description 5
- 229940011182 cobalt acetate Drugs 0.000 description 5
- QAHREYKOYSIQPH-UHFFFAOYSA-L cobalt(II) acetate Chemical compound [Co+2].CC([O-])=O.CC([O-])=O QAHREYKOYSIQPH-UHFFFAOYSA-L 0.000 description 5
- 230000003247 decreasing effect Effects 0.000 description 5
- JVLRYPRBKSMEBF-UHFFFAOYSA-K diacetyloxystibanyl acetate Chemical compound [Sb+3].CC([O-])=O.CC([O-])=O.CC([O-])=O JVLRYPRBKSMEBF-UHFFFAOYSA-K 0.000 description 5
- 239000002270 dispersing agent Substances 0.000 description 5
- 239000004576 sand Substances 0.000 description 5
- 239000002002 slurry Substances 0.000 description 5
- GGUBFICZYGKNTD-UHFFFAOYSA-N triethyl phosphonoacetate Chemical compound CCOC(=O)CP(=O)(OCC)OCC GGUBFICZYGKNTD-UHFFFAOYSA-N 0.000 description 5
- ZOIORXHNWRGPMV-UHFFFAOYSA-N acetic acid;zinc Chemical compound [Zn].CC(O)=O.CC(O)=O ZOIORXHNWRGPMV-UHFFFAOYSA-N 0.000 description 4
- 239000000975 dye Substances 0.000 description 4
- 239000011521 glass Substances 0.000 description 4
- 238000003801 milling Methods 0.000 description 4
- 239000011112 polyethylene naphthalate Substances 0.000 description 4
- 229910001220 stainless steel Inorganic materials 0.000 description 4
- 239000010935 stainless steel Substances 0.000 description 4
- 239000004246 zinc acetate Substances 0.000 description 4
- UHHXUPJJDHEMGX-UHFFFAOYSA-K azanium;manganese(3+);phosphonato phosphate Chemical compound [NH4+].[Mn+3].[O-]P([O-])(=O)OP([O-])([O-])=O UHHXUPJJDHEMGX-UHFFFAOYSA-K 0.000 description 3
- 229920001577 copolymer Polymers 0.000 description 3
- HNMCSUXJLGGQFO-UHFFFAOYSA-N hexaaluminum;hexasodium;tetrathietane;hexasilicate Chemical class [Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].S1SSS1.S1SSS1.[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-] HNMCSUXJLGGQFO-UHFFFAOYSA-N 0.000 description 3
- 229920003207 poly(ethylene-2,6-naphthalate) Polymers 0.000 description 3
- 229920000515 polycarbonate Polymers 0.000 description 3
- 239000004417 polycarbonate Substances 0.000 description 3
- 239000004698 Polyethylene Substances 0.000 description 2
- 230000004075 alteration Effects 0.000 description 2
- 238000000149 argon plasma sintering Methods 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 2
- 230000001419 dependent effect Effects 0.000 description 2
- 230000006866 deterioration Effects 0.000 description 2
- DGXKDBWJDQHNCI-UHFFFAOYSA-N dioxido(oxo)titanium nickel(2+) Chemical compound [Ni++].[O-][Ti]([O-])=O DGXKDBWJDQHNCI-UHFFFAOYSA-N 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 238000005305 interferometry Methods 0.000 description 2
- 125000005487 naphthalate group Chemical group 0.000 description 2
- 229920001707 polybutylene terephthalate Polymers 0.000 description 2
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- 238000012545 processing Methods 0.000 description 2
- 238000002310 reflectometry Methods 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- KKEYFWRCBNTPAC-UHFFFAOYSA-L terephthalate(2-) Chemical compound [O-]C(=O)C1=CC=C(C([O-])=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-L 0.000 description 2
- 239000012815 thermoplastic material Substances 0.000 description 2
- 238000000411 transmission spectrum Methods 0.000 description 2
- JRBJSXQPQWSCCF-UHFFFAOYSA-N 3,3'-Dimethoxybenzidine Chemical compound C1=C(N)C(OC)=CC(C=2C=C(OC)C(N)=CC=2)=C1 JRBJSXQPQWSCCF-UHFFFAOYSA-N 0.000 description 1
- IYHIFXGFKVJNBB-UHFFFAOYSA-N 5-chloro-2-[(2-hydroxynaphthalen-1-yl)diazenyl]-4-methylbenzenesulfonic acid Chemical compound C1=C(Cl)C(C)=CC(N=NC=2C3=CC=CC=C3C=CC=2O)=C1S(O)(=O)=O IYHIFXGFKVJNBB-UHFFFAOYSA-N 0.000 description 1
- CGLVZFOCZLHKOH-UHFFFAOYSA-N 8,18-dichloro-5,15-diethyl-5,15-dihydrodiindolo(3,2-b:3',2'-m)triphenodioxazine Chemical compound CCN1C2=CC=CC=C2C2=C1C=C1OC3=C(Cl)C4=NC(C=C5C6=CC=CC=C6N(C5=C5)CC)=C5OC4=C(Cl)C3=NC1=C2 CGLVZFOCZLHKOH-UHFFFAOYSA-N 0.000 description 1
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- AUNAPVYQLLNFOI-UHFFFAOYSA-L [Pb++].[Pb++].[Pb++].[O-]S([O-])(=O)=O.[O-][Cr]([O-])(=O)=O.[O-][Mo]([O-])(=O)=O Chemical compound [Pb++].[Pb++].[Pb++].[O-]S([O-])(=O)=O.[O-][Cr]([O-])(=O)=O.[O-][Mo]([O-])(=O)=O AUNAPVYQLLNFOI-UHFFFAOYSA-L 0.000 description 1
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- TUFZVLHKHTYNTN-UHFFFAOYSA-N antimony;nickel Chemical compound [Sb]#[Ni] TUFZVLHKHTYNTN-UHFFFAOYSA-N 0.000 description 1
- IRERQBUNZFJFGC-UHFFFAOYSA-L azure blue Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[S-]S[S-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-] IRERQBUNZFJFGC-UHFFFAOYSA-L 0.000 description 1
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- XJUNRGGMKUAPAP-UHFFFAOYSA-N dioxido(dioxo)molybdenum;lead(2+) Chemical compound [Pb+2].[O-][Mo]([O-])(=O)=O XJUNRGGMKUAPAP-UHFFFAOYSA-N 0.000 description 1
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- RBTKNAXYKSUFRK-UHFFFAOYSA-N heliogen blue Chemical compound [Cu].[N-]1C2=C(C=CC=C3)C3=C1N=C([N-]1)C3=CC=CC=C3C1=NC([N-]1)=C(C=CC=C3)C3=C1N=C([N-]1)C3=CC=CC=C3C1=N2 RBTKNAXYKSUFRK-UHFFFAOYSA-N 0.000 description 1
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- PYUYQYBDJFMFTH-WMMMYUQOSA-N naphthol red Chemical compound CCOC1=CC=CC=C1NC(=O)C(C1=O)=CC2=CC=CC=C2\C1=N\NC1=CC=C(C(N)=O)C=C1 PYUYQYBDJFMFTH-WMMMYUQOSA-N 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 1
- 239000012860 organic pigment Substances 0.000 description 1
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- 230000002035 prolonged effect Effects 0.000 description 1
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- JEXVQSWXXUJEMA-UHFFFAOYSA-N pyrazol-3-one Chemical compound O=C1C=CN=N1 JEXVQSWXXUJEMA-UHFFFAOYSA-N 0.000 description 1
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- VVNRQZDDMYBBJY-UHFFFAOYSA-M sodium 1-[(1-sulfonaphthalen-2-yl)diazenyl]naphthalen-2-olate Chemical compound [Na+].C1=CC=CC2=C(S([O-])(=O)=O)C(N=NC3=C4C=CC=CC4=CC=C3O)=CC=C21 VVNRQZDDMYBBJY-UHFFFAOYSA-M 0.000 description 1
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Classifications
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- B32B27/08—Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material of synthetic resin
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
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Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Materials Engineering (AREA)
- General Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Manufacture Of Macromolecular Shaped Articles (AREA)
- Laminated Bodies (AREA)
- Optical Filters (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Printing Methods (AREA)
- Road Signs Or Road Markings (AREA)
- Shaping By String And By Release Of Stress In Plastics And The Like (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US50359700A | 2000-02-10 | 2000-02-10 | |
| US09/503,597 | 2000-02-10 | ||
| PCT/US2000/031854 WO2001058989A1 (en) | 2000-02-10 | 2000-11-20 | Color stable pigmented polymeric films |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2398452A1 CA2398452A1 (en) | 2001-08-16 |
| CA2398452C true CA2398452C (en) | 2010-03-30 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2398452A Expired - Fee Related CA2398452C (en) | 2000-02-10 | 2000-11-20 | Color stable pigmented polymeric films |
Country Status (11)
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|---|---|
| US (2) | US6811867B1 (https=) |
| EP (1) | EP1257594B1 (https=) |
| JP (1) | JP4943617B2 (https=) |
| KR (1) | KR100743754B1 (https=) |
| CN (2) | CN100371371C (https=) |
| AT (1) | ATE353350T1 (https=) |
| AU (1) | AU2001217813A1 (https=) |
| BR (1) | BR0017100B1 (https=) |
| CA (1) | CA2398452C (https=) |
| DE (1) | DE60033319T2 (https=) |
| WO (1) | WO2001058989A1 (https=) |
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| EP1127381B1 (en) | 1998-11-02 | 2015-09-23 | 3M Innovative Properties Company | Transparent conductive oxides for plastic flat panel displays |
| US6811867B1 (en) * | 2000-02-10 | 2004-11-02 | 3M Innovative Properties Company | Color stable pigmented polymeric films |
| US6797396B1 (en) | 2000-06-09 | 2004-09-28 | 3M Innovative Properties Company | Wrinkle resistant infrared reflecting film and non-planar laminate articles made therefrom |
| EP1201767B1 (en) * | 2000-10-25 | 2010-07-21 | FUJIFILM Corporation | Method of analyzing double stranded DNA |
| KR100905142B1 (ko) * | 2001-01-15 | 2009-06-29 | 쓰리엠 이노베이티브 프로퍼티즈 컴파니 | 가시 파장 영역에서의 높고 평활한 투과율을 가진 다층적외선 반사 필름 및 그로부터 제조된 라미네이트 제품 |
| US20030017326A1 (en) * | 2001-06-01 | 2003-01-23 | 3M Innovative Properties Company | Color stable pigmented polymeric films having dyes for color adjustment |
| US7189447B2 (en) * | 2002-01-04 | 2007-03-13 | 3M Innovative Properties Company | Laminates |
| EP1378337A1 (en) * | 2002-07-02 | 2004-01-07 | SOLVAY POLYOLEFINS EUROPE - BELGIUM (Société Anonyme) | Radiation screening materials |
| US6929864B2 (en) | 2002-08-17 | 2005-08-16 | 3M Innovative Properties Company | Extensible, visible light-transmissive and infrared-reflective film and methods of making and using the film |
| US6818291B2 (en) | 2002-08-17 | 2004-11-16 | 3M Innovative Properties Company | Durable transparent EMI shielding film |
| US7215473B2 (en) | 2002-08-17 | 2007-05-08 | 3M Innovative Properties Company | Enhanced heat mirror films |
| US6933051B2 (en) | 2002-08-17 | 2005-08-23 | 3M Innovative Properties Company | Flexible electrically conductive film |
| US7652736B2 (en) * | 2005-10-25 | 2010-01-26 | 3M Innovative Properties Company | Infrared light reflecting film |
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| US20090093578A1 (en) * | 2006-03-08 | 2009-04-09 | Carlos Guerra | Transparent stretched acrylic sheets for aircraft window systems having controlled solar transmittance properties |
| US20070210287A1 (en) * | 2006-03-08 | 2007-09-13 | Spartech Corporation | Transparent plastic articles having controlled solar energy transmittance properties and methods of making |
| US7952805B2 (en) * | 2006-08-22 | 2011-05-31 | 3M Innovative Properties Company | Solar control film |
| US8120854B2 (en) | 2006-12-28 | 2012-02-21 | 3M Innovative Properties Company | Interference films having acrylamide layer and method of making same |
| WO2008083308A1 (en) | 2006-12-28 | 2008-07-10 | 3M Innovative Properties Company | Nucleation layer for thin film metal layer formation |
| BRPI0720867A2 (pt) * | 2006-12-29 | 2014-03-04 | 3M Innovative Properties Company. | Método para fabricação de filmes inorgânicos ou híbridos inorgânicos/orgânicos |
| CN101573471A (zh) | 2006-12-29 | 2009-11-04 | 3M创新有限公司 | 固化含有金属烷氧化物的膜的方法 |
| SG185934A1 (en) * | 2007-10-30 | 2012-12-28 | 3M Innovative Properties Co | Multi-stack optical bandpass film with electro magnetic interference shielding for optical display filters |
| CN104327758A (zh) | 2007-12-28 | 2015-02-04 | 3M创新有限公司 | 柔性封装膜系统 |
| US9034459B2 (en) * | 2007-12-28 | 2015-05-19 | 3M Innovative Properties Company | Infrared reflecting films for solar control and other uses |
| EP2177354B1 (en) | 2008-05-05 | 2012-08-08 | A. Schulman, Inc. | Layered backing structure |
| JP5624033B2 (ja) | 2008-06-30 | 2014-11-12 | スリーエム イノベイティブプロパティズカンパニー | 無機又は無機／有機ハイブリッドバリアフィルムの製造方法 |
| KR20110110240A (ko) | 2008-12-30 | 2011-10-06 | 쓰리엠 이노베이티브 프로퍼티즈 컴파니 | 반사방지 용품 및 이의 제조 방법 |
| WO2010123528A2 (en) | 2008-12-30 | 2010-10-28 | 3M Innovative Properties Company | Nanostructured articles and methods of making nanostructured articles |
| EP2379442A4 (en) | 2008-12-30 | 2014-02-26 | 3M Innovative Properties Co | METHOD FOR PRODUCING NANOSTRUCTURED SURFACES |
| US9012044B2 (en) | 2009-08-03 | 2015-04-21 | 3M Innovative Properties Company | Process for forming optically clear conductive metal or metal alloy thin films and films made therefrom |
| WO2011017039A2 (en) | 2009-08-03 | 2011-02-10 | 3M Innovative Properties Company | Antireflective transparent emi shielding optical filter |
| SG183850A1 (en) | 2010-03-03 | 2012-10-30 | 3M Innovative Properties Co | Composite with nano-structured layer |
| KR20130014525A (ko) | 2010-03-03 | 2013-02-07 | 쓰리엠 이노베이티브 프로퍼티즈 컴파니 | 나노구조화된 표면을 갖는 코팅된 편광기 및 이의 제조 방법 |
| DE102010018028A1 (de) * | 2010-04-23 | 2011-10-27 | Osram Opto Semiconductors Gmbh | Flächenlichtleiter und Leuchte |
| CN103229079B (zh) | 2010-12-10 | 2016-10-12 | 3M创新有限公司 | 减少炫光的窗用制品 |
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| JP5977260B2 (ja) | 2011-02-02 | 2016-08-24 | スリーエム イノベイティブ プロパティズ カンパニー | 暗い多層導電体トレースを有するパターン化基材 |
| WO2012112624A2 (en) | 2011-02-15 | 2012-08-23 | Svaya Nanotechnologies, Inc. | Methods and materials for functional polyionic species and deposition thereof |
| US20140004304A1 (en) | 2011-03-14 | 2014-01-02 | 3M Innovative Properties Company | Multilayer nanostructured articles |
| BR112013023128A2 (pt) | 2011-03-14 | 2019-09-24 | 3M Innovative Properties Co | artigos nanoestruturados |
| US20130344345A1 (en) * | 2011-07-08 | 2013-12-26 | Toray Plastics (America), Inc. | Biaxially oriented bio-based polyester window films and laminates |
| US10137625B2 (en) | 2011-07-08 | 2018-11-27 | Toray Plastics (America), Inc. | Biaxially oriented bio-based polyester films and laminates |
| WO2013052927A2 (en) | 2011-10-07 | 2013-04-11 | Svaya Nanotechnologies, Inc. | Broadband solar control film |
| CN102558792A (zh) * | 2011-12-31 | 2012-07-11 | 四川虹欧显示器件有限公司 | 用于滤光膜的pet基材、制备方法及包括其的滤光膜和显示屏 |
| CN103293580A (zh) * | 2011-12-31 | 2013-09-11 | 四川虹欧显示器件有限公司 | 滤光膜及包括其的显示屏 |
| CN102627783B (zh) * | 2012-04-20 | 2014-04-02 | 北京化工大学 | 一种交联聚乙烯吡咯烷酮基荧光复合薄膜及其制备方法 |
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| KR102130700B1 (ko) * | 2013-05-30 | 2020-07-07 | 삼성디스플레이 주식회사 | 표시장치용 윈도우 및 이를 포함하는 표시 장치 |
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| JP2016527341A (ja) | 2013-06-24 | 2016-09-08 | スリーエム イノベイティブ プロパティズ カンパニー | 自己濡れ性（Ｓｅｌｆ−Ｗｅｔｔｉｎｇ）接着剤組成物 |
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-
2000
- 2000-08-08 US US09/633,911 patent/US6811867B1/en not_active Expired - Lifetime
- 2000-11-20 CN CNB2004100978275A patent/CN100371371C/zh not_active Expired - Fee Related
- 2000-11-20 AT AT00980565T patent/ATE353350T1/de not_active IP Right Cessation
- 2000-11-20 DE DE60033319T patent/DE60033319T2/de not_active Expired - Lifetime
- 2000-11-20 WO PCT/US2000/031854 patent/WO2001058989A1/en not_active Ceased
- 2000-11-20 JP JP2001558133A patent/JP4943617B2/ja not_active Expired - Fee Related
- 2000-11-20 AU AU2001217813A patent/AU2001217813A1/en not_active Abandoned
- 2000-11-20 EP EP00980565A patent/EP1257594B1/en not_active Expired - Lifetime
- 2000-11-20 KR KR1020027010375A patent/KR100743754B1/ko not_active Expired - Fee Related
- 2000-11-20 CN CNB00818917XA patent/CN1252155C/zh not_active Expired - Fee Related
- 2000-11-20 BR BRPI0017100-0A patent/BR0017100B1/pt not_active IP Right Cessation
- 2000-11-20 CA CA2398452A patent/CA2398452C/en not_active Expired - Fee Related
-
2004
- 2004-08-23 US US10/923,901 patent/US7368161B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| WO2001058989A1 (en) | 2001-08-16 |
| BR0017100A (pt) | 2003-01-14 |
| CA2398452A1 (en) | 2001-08-16 |
| AU2001217813A1 (en) | 2001-08-20 |
| CN1252155C (zh) | 2006-04-19 |
| CN1631947A (zh) | 2005-06-29 |
| JP4943617B2 (ja) | 2012-05-30 |
| CN1434837A (zh) | 2003-08-06 |
| US7368161B2 (en) | 2008-05-06 |
| BR0017100B1 (pt) | 2011-06-14 |
| KR100743754B1 (ko) | 2007-08-01 |
| US6811867B1 (en) | 2004-11-02 |
| KR20020076302A (ko) | 2002-10-09 |
| JP2003522268A (ja) | 2003-07-22 |
| EP1257594A1 (en) | 2002-11-20 |
| US20050019550A1 (en) | 2005-01-27 |
| CN100371371C (zh) | 2008-02-27 |
| DE60033319D1 (de) | 2007-03-22 |
| EP1257594B1 (en) | 2007-02-07 |
| ATE353350T1 (de) | 2007-02-15 |
| DE60033319T2 (de) | 2007-07-12 |
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