BR112017025910A2 - processo para preparação de uma composição de ácido purificado - Google Patents

processo para preparação de uma composição de ácido purificado

Info

Publication number
BR112017025910A2
BR112017025910A2 BR112017025910A BR112017025910A BR112017025910A2 BR 112017025910 A2 BR112017025910 A2 BR 112017025910A2 BR 112017025910 A BR112017025910 A BR 112017025910A BR 112017025910 A BR112017025910 A BR 112017025910A BR 112017025910 A2 BR112017025910 A2 BR 112017025910A2
Authority
BR
Brazil
Prior art keywords
acid composition
acid
solution
preparing
fdca
Prior art date
Application number
BR112017025910A
Other languages
English (en)
Other versions
BR112017025910B1 (pt
Inventor
Rita Martins Guerreiro Rocha ALMEIDA Ana
Sofia Vagueiro De Sousa Dias Ana
Mathilda Pieter Zieverink Martinus
Original Assignee
Synvina C V
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Synvina C V filed Critical Synvina C V
Publication of BR112017025910A2 publication Critical patent/BR112017025910A2/pt
Publication of BR112017025910B1 publication Critical patent/BR112017025910B1/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/56—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D307/68—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/32—Manganese, technetium or rhenium
    • B01J23/34—Manganese
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/75—Cobalt
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/06—Halogens; Compounds thereof
    • B01J27/08—Halides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B31/00—Reduction in general
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B33/00—Oxidation in general
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B41/00—Formation or introduction of functional groups containing oxygen
    • C07B41/02—Formation or introduction of functional groups containing oxygen of hydroxy or O-metal groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B63/00—Purification; Separation; Stabilisation; Use of additives
    • C07B63/02—Purification; Separation; Stabilisation; Use of additives by treatment giving rise to a chemical modification
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/66—Polyesters containing oxygen in the form of ether groups
    • C08G63/668—Polyesters containing oxygen in the form of ether groups derived from polycarboxylic acids and polyhydroxy compounds
    • C08G63/672—Dicarboxylic acids and dihydroxy compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00027—Process aspects
    • B01J2219/00033—Continuous processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00162—Controlling or regulating processes controlling the pressure
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/13—Crystalline forms, e.g. polymorphs

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Furan Compounds (AREA)

Abstract

uma composição de ácido purificado compreendendo ácido 2,5-furandicarboxílico é preparada por um processo compreendendo a) prover uma solução de composição ácida de uma composição ácida bruto em um solvente polar, a composição ácida bruto compreende ácido 2,5-furandicarboxílico (fdca) e ácido 2-formil-furan-5-carboxílico (ffca); b) colocar a solução de composição ácida em contato com hidrogênio na presença de um catalisador de hidrogenação para hidrogenar ffca em produtos de hidrogenação, de maneira que os produtos de hidrogenação contenham uma pequena quantidade de ácido 2-metil-furan-5-carboxílico (mfa) ou não mfa, produzindo uma solução hidrogenada; c) separar pelo menos uma porção do fdca da solução hidrogenada por cristalização.
BR112017025910-9A 2015-06-05 2016-06-06 Processo para preparação de uma composição de ácido purificado BR112017025910B1 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
NL2014923 2015-06-05
NL2014923 2015-06-05
PCT/NL2016/050404 WO2016195499A1 (en) 2015-06-05 2016-06-06 Process for the preparation of a purified acid composition

Publications (2)

Publication Number Publication Date
BR112017025910A2 true BR112017025910A2 (pt) 2018-08-14
BR112017025910B1 BR112017025910B1 (pt) 2022-08-23

Family

ID=53502805

Family Applications (2)

Application Number Title Priority Date Filing Date
BR112017025913-3A BR112017025913B1 (pt) 2015-06-05 2016-06-06 Processo para preparação de uma composição de ácido purificado
BR112017025910-9A BR112017025910B1 (pt) 2015-06-05 2016-06-06 Processo para preparação de uma composição de ácido purificado

Family Applications Before (1)

Application Number Title Priority Date Filing Date
BR112017025913-3A BR112017025913B1 (pt) 2015-06-05 2016-06-06 Processo para preparação de uma composição de ácido purificado

Country Status (11)

Country Link
US (2) US10464913B2 (pt)
EP (2) EP3303311B1 (pt)
JP (2) JP6615230B2 (pt)
KR (2) KR102072002B1 (pt)
CN (2) CN107848998B (pt)
AU (2) AU2016271835B2 (pt)
BR (2) BR112017025913B1 (pt)
CA (2) CA2988392C (pt)
ES (2) ES2833164T3 (pt)
MX (2) MX2017015720A (pt)
WO (2) WO2016195499A1 (pt)

Families Citing this family (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20180107143A (ko) 2016-01-13 2018-10-01 스토라 엔소 오와이제이 2,5-푸란디카르복실산 및 그의 중간체 및 유도체의 제조 방법
JP2017190316A (ja) * 2016-04-15 2017-10-19 三菱ケミカル株式会社 ２，５−フランジカルボン酸の精製方法
EP3652161A1 (en) * 2017-07-12 2020-05-20 Stora Enso Oyj Purified 2,5-furandicarboxylic acid pathway products
EP3444354A1 (en) * 2017-08-16 2019-02-20 Basf Se Process of separating 2,5-diformylfuran from an aqueous mixture by cooling
TWI650318B (zh) 2017-10-30 2019-02-11 財團法人工業技術研究院 以結晶法純化２，５－呋喃二甲酸的粗產物之方法與聚酯之形成方法
US11655334B2 (en) 2018-06-25 2023-05-23 Eastman Chemical Company Oxidation process to produce 5 methyl 5-methylfuran-2-carboxylate (MMFC)
US11440895B2 (en) 2018-06-25 2022-09-13 Eastman Chemical Company Oxidation process to produce 5-(alkoxycarbonyl)furan-2-carboxylic acids (ACFC)
CN109293608B (zh) * 2018-09-21 2023-06-16 中国科学技术大学 一种5-甲酰基糠酸的制备方法
TWI697488B (zh) * 2019-07-02 2020-07-01 遠東新世紀股份有限公司 粗製2,5-呋喃二甲酸的純化方法
TWI697487B (zh) * 2019-07-02 2020-07-01 遠東新世紀股份有限公司 粗製2,5-呋喃二甲酸的純化方法
WO2021045927A1 (en) 2019-09-05 2021-03-11 Eastman Chemical Company Efficient process for producing 5-(alkoxycarbonyl)-furan-2-carboxylic acids
CN114901648A (zh) 2019-12-20 2022-08-12 福兰尼克斯科技公司 由5-羟甲基糠醛的醚生产2,5-呋喃二甲酸的工艺
JP2023507469A (ja) 2019-12-20 2023-02-22 フラニックス・テクノロジーズ・ベーフェー 精製２，５－フランジカルボン酸の水及び熱による処理
MX2022007644A (es) 2019-12-20 2022-07-19 Furanix Technologies Bv Tratamiento termico y con acido organico de acido 2,5-furandicarboxilico purificado.
WO2022245623A1 (en) * 2021-05-20 2022-11-24 Eastman Chemical Company Purge process for 5-(alkoxycarbonyl)furan-2-carboylic acid (acfc)
EP4341250A1 (en) * 2021-05-20 2024-03-27 Eastman Chemical Company Purge process for 5-(methoxycarbonyl)furan-2-carboxylic acid (mcfc)
EP4341249A1 (en) * 2021-05-20 2024-03-27 Eastman Chemical Company Mother liquor compositiion generated in mcfc process
CN115028610B (zh) * 2022-05-07 2024-03-05 浙江恒逸石化研究院有限公司 一种2,5-呋喃二甲酸的纯化方法
WO2023242152A1 (en) 2022-06-14 2023-12-21 Furanix Technologies B.V. Producing 2,5-furandicarboxylic acid from mixed feed
WO2023242151A1 (en) 2022-06-14 2023-12-21 Furanix Technologies B.V. Producing 2,5-furandicarboxylic acid with recovery of acid
WO2023242150A1 (en) 2022-06-14 2023-12-21 Furanix Technologies B.V. Producing 2,5-furandicarboxylic acid in the presence of modifying acid
WO2024062084A1 (en) 2022-09-23 2024-03-28 Furanix Technologies B.V. Oxidation of furan derivative
CN115894411A (zh) * 2022-12-29 2023-04-04 厦门大学 低沸点溶液在2,5-呋喃二甲酸纯化中的应用及其纯化方法

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2893860B2 (ja) * 1990-05-17 1999-05-24 三菱瓦斯化学株式会社 高純度イソフタル酸の製造法
JPH05190908A (ja) 1992-01-13 1993-07-30 Nec Corp 光電変換装置
DE4334100C2 (de) 1992-10-13 2003-02-13 Mitsubishi Chem Corp Verfahren zur Herstellung hochreiner Terephthalsäure
JPH09151162A (ja) 1995-11-30 1997-06-10 Sekiyu Sangyo Kasseika Center ナフタレンジカルボン酸の精製法
US6265608B1 (en) 1998-06-30 2001-07-24 Eastman Chemical Company Method of purifying aromatic dicarboxylic acids
US6455742B1 (en) 1999-09-02 2002-09-24 Wisconsin Alumni Research Foundation Method for catalytically reducing carboxylic acid groups to hydroxyl groups in hydroxycarboxylic acids
ATE348093T1 (de) 2004-12-15 2007-01-15 Saudi Basic Ind Corp Verfahren zur herstellung gereinigter terephtalsäure
TR201908177T4 (tr) 2009-05-14 2019-06-21 Archer Daniels Midland Co Bir co(ıı) veya ce(ııı) katalizörü, bir bromür tuzu ve bir solvent varlığında 5-(alkiloksimetil)furfuralin (AMF) oksijen ile oksidasyonu aracılığıyla 2,5-furandikarboksilik asidin (FDCA) hazırlanışına yönelik proses.
US8865921B2 (en) 2009-10-07 2014-10-21 Furanix Technologies B.V. Method for the preparation of 2,5-furandicarboxylic acid and for the preparation of the dialkyl ester of 2,5-furandicarboxylic acid
WO2011043660A2 (en) 2009-10-07 2011-04-14 Furanix Technologies B.V. Method for the preparation of 2,5-furandicarboxylic acid and esters thereof
US20120302773A1 (en) * 2011-05-24 2012-11-29 Eastman Chemical Company Oxidation process to produce a crude and/or purified carboxylic acid product
US8748479B2 (en) * 2012-06-22 2014-06-10 Eastman Chemical Company Process for purifying crude furan 2,5-dicarboxylic acid using hydrogenation
US8969404B2 (en) * 2012-06-22 2015-03-03 Eastman Chemical Company Purifying crude furan 2,5-dicarboxylic acid by hydrogenation
US9006470B2 (en) * 2012-11-08 2015-04-14 Eastman Chemical Company Method of synthesizing low color furan diesters
US9156805B2 (en) * 2012-11-20 2015-10-13 Eastman Chemical Company Oxidative purification method for producing purified dry furan-2,5-dicarboxylic acid
NL2010572C2 (en) 2013-04-05 2014-10-07 Furanix Technologies Bv Process for the preaparation of 2,5-furan-dicarboxylic acid.
US9896425B2 (en) * 2013-08-30 2018-02-20 Synvina C.V. Process for purifying an acid composition comprising 2-formyl-furan-5-carboxylic acid and 2,5-furandicarboxylic acid

Also Published As

Publication number Publication date
EP3303311A1 (en) 2018-04-11
ES2833165T3 (es) 2021-06-14
MX2017015720A (es) 2018-04-24
WO2016195500A1 (en) 2016-12-08
BR112017025910B1 (pt) 2022-08-23
KR20180015720A (ko) 2018-02-13
ES2833164T3 (es) 2021-06-14
CA2988307A1 (en) 2016-12-08
US20180155308A1 (en) 2018-06-07
JP6615231B2 (ja) 2019-12-04
AU2016271834B2 (en) 2019-02-21
JP2018521980A (ja) 2018-08-09
US10351544B2 (en) 2019-07-16
AU2016271835B2 (en) 2019-02-21
AU2016271835A1 (en) 2018-01-18
AU2016271834A1 (en) 2018-01-18
EP3303310A1 (en) 2018-04-11
EP3303311B1 (en) 2020-08-26
KR102067718B1 (ko) 2020-01-30
JP2018521978A (ja) 2018-08-09
CN107848999A (zh) 2018-03-27
CA2988307C (en) 2020-04-14
BR112017025913B1 (pt) 2022-08-23
CN107848998A (zh) 2018-03-27
KR102072002B1 (ko) 2020-01-31
CA2988392A1 (en) 2016-12-08
MX2017015723A (es) 2018-04-24
WO2016195499A1 (en) 2016-12-08
JP6615230B2 (ja) 2019-12-04
US20180155309A1 (en) 2018-06-07
CN107848998B (zh) 2022-02-01
CN107848999B (zh) 2022-02-01
CA2988392C (en) 2020-04-14
KR20180014816A (ko) 2018-02-09
US10464913B2 (en) 2019-11-05
BR112017025913A2 (pt) 2018-08-14
EP3303310B1 (en) 2020-08-26

Similar Documents

Publication Publication Date Title
BR112017025910A2 (pt) processo para preparação de uma composição de ácido purificado
BR112015017606A2 (pt) composição, método de produzir a composição, utilização da composição e combustível obtido a partir da composição
BR112016015496A2 (pt) composição e processo para a produção da composição
BR112018010229A2 (pt) sistema catalisador e processo para a produção de glicóis
AR110460A1 (es) Proceso para preparar terpinen-4-ol
BR112018011705A2 (pt) processo para a preparação de glicóis
BR112018006403A2 (pt) processo para a preparação de glicóis
BR112014016687A8 (pt) processo para fazer hidroximetilfurfural a partir de uma solução aquosa que inclui uma ou mais hexoses e processo para fazer um éter de hidroximetilfurfural a partir de uma solução aquosa que inclui uma ou mais hexoses
BRPI1015324A2 (pt) sistema curável, método para a fabricação de um produto curado, produto curado, e, usos do produto curado e do sistema curável
BR112014031051A2 (pt) processo para produção de uma composição contendo folistatina ativa
BR112017014623A2 (pt) ?processo para preparar tetraidrofurano e/ou butano-1,4-diol e/ou gama-butirolactona?
BR112016008352A2 (pt) processo para a produção de polibutadienos catalisados com neodímio (ndbr), misturas de borracha que contêm polibutadienos catalisados com neodímio (ndbr), e usos de misturas de borracha
BR112015029399A2 (pt) produção em etapa única de uma composição de polipropileno
BR112018010230A2 (pt) sistema catalisador e processo para a produção de glicóis
UY35571A (es) (ciano-dimetil-metil)-isoxazoles y -[1,3,4]tiadiazoles como agonistas del receptor cannabinoide 2 (cb2)
AR106950A1 (es) Compuesto moldeable y procedimiento para producir productos de gelatina
BR112017011750A2 (pt) processo para a produção de 1,4-butanodiol e tetraidrofurano a partir de furano
BR112017013025A2 (pt) recuperação de óleo da lama de palma
BR112018016284A2 (pt) processo para a produção de alquileno glicóis
BR112018007709A2 (pt) processo de produção de 5-hidroximetilfurfural na presença de um catalisador tipo ácido de lewis e/ou de um catalisador tipo base heterogêneo e de um catalisador orgânico homogêneo tipo ácido de brønsted na presença de pelo menos um solvente polar aprótico
BR112018067996A2 (pt) método para preparar um derivado de polietileno glicol dialdeído
BR112018007801A2 (pt) processo para produção de glicóis.
BR112018010232A2 (pt) sistema catalisador e processo para a produção de glicóis
BR112018007692A2 (pt) processo de produção de 5-hidroximetilfurfural na presença de catalisadores da família de ácidos sulfônicos homogêneos na presença de pelo menos um solvente polar aprótico
BR112018016160A2 (pt) processo para a hidrogenação de glicoladeído

Legal Events

Date Code Title Description
B25A Requested transfer of rights approved

Owner name: FURANIX TECHNOLOGIES B.V. (NL)

B350 Update of information on the portal [chapter 15.35 patent gazette]
B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 06/06/2016, OBSERVADAS AS CONDICOES LEGAIS