MX2017015723A - Procedimiento para la preparacion de una composicion purificada de acido. - Google Patents

Procedimiento para la preparacion de una composicion purificada de acido.

Info

Publication number
MX2017015723A
MX2017015723A MX2017015723A MX2017015723A MX2017015723A MX 2017015723 A MX2017015723 A MX 2017015723A MX 2017015723 A MX2017015723 A MX 2017015723A MX 2017015723 A MX2017015723 A MX 2017015723A MX 2017015723 A MX2017015723 A MX 2017015723A
Authority
MX
Mexico
Prior art keywords
fdca
ffca
esters
solution
oxidation product
Prior art date
Application number
MX2017015723A
Other languages
English (en)
Inventor
Sofia Vagueiro De Sousa Dias Ana
Rita Martins Guerreiro Rocha ALMEIDA Ana
Mathilda Pieter Zieverink Martinus
Dacil Gonzalez Jimenez Ines
Original Assignee
Synvina C V
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Synvina C V filed Critical Synvina C V
Publication of MX2017015723A publication Critical patent/MX2017015723A/es

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/56—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D307/68—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/32—Manganese, technetium or rhenium
    • B01J23/34—Manganese
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/75—Cobalt
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/06—Halogens; Compounds thereof
    • B01J27/08—Halides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B31/00—Reduction in general
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B33/00—Oxidation in general
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B41/00—Formation or introduction of functional groups containing oxygen
    • C07B41/02—Formation or introduction of functional groups containing oxygen of hydroxy or O-metal groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B63/00—Purification; Separation; Stabilisation; Use of additives
    • C07B63/02—Purification; Separation; Stabilisation; Use of additives by treatment giving rise to a chemical modification
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/66—Polyesters containing oxygen in the form of ether groups
    • C08G63/668—Polyesters containing oxygen in the form of ether groups derived from polycarboxylic acids and polyhydroxy compounds
    • C08G63/672—Dicarboxylic acids and dihydroxy compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00027—Process aspects
    • B01J2219/00033—Continuous processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00162—Controlling or regulating processes controlling the pressure
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/13—Crystalline forms, e.g. polymorphs

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Furan Compounds (AREA)

Abstract

Se prepara una composición ácida purificada que comprende ácido 2,5-furanodicarboxílico en un procedimiento, que comprende (i) oxidar una materia prima que contiene 5-alcoximetilfurfural a un producto de oxidación que comprende ácido 2,5-furanodicarboxílico (FDCA) y ácido 2-formil-furan-5-carboxílico (FFCA), y ésteres de FDCA y, opcionalmente, ésteres de FFCA; (ii) opcionalmente, disolver al menos parte del producto de oxidación en un solvente polar para obtener una solución del producto de oxidación, que comprende FDCA, FFCA y ésteres de FDCA y, opcionalmente, ésteres de FFCA; (iii) hidrolizar la al menos parte del producto de oxidación en presencia de agua, hidrolizando de este modo al menos ésteres de FDCA y, opcionalmente, ésteres de FFCA para obtener una solución acuosa de una composición ácida que comprende FDCA, FFCA y éster de FDCA en una cantidad por debajo de la cantidad de éster de FDCA en la solución del producto de oxidación; (iv) poner en contacto al menos parte de la solución de la composición ácida obtenida en la etapa (iii) con hidrógeno en presencia de un catalizador de hidrogenación para hidrogenar FFCA a productos de hidrogenación, produciendo una solución hidrogenada; y (v) separar al menos una porción del FDCA de al menos parte de la solución hidrogenada mediante cristalización.
MX2017015723A 2015-06-05 2016-06-06 Procedimiento para la preparacion de una composicion purificada de acido. MX2017015723A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
NL2014923 2015-06-05
PCT/NL2016/050405 WO2016195500A1 (en) 2015-06-05 2016-06-06 Process for the preparation of a purified acid composition

Publications (1)

Publication Number Publication Date
MX2017015723A true MX2017015723A (es) 2018-04-24

Family

ID=53502805

Family Applications (2)

Application Number Title Priority Date Filing Date
MX2017015720A MX2017015720A (es) 2015-06-05 2016-06-06 Procedimiento para la preparacion de una composicion purificada de acido.
MX2017015723A MX2017015723A (es) 2015-06-05 2016-06-06 Procedimiento para la preparacion de una composicion purificada de acido.

Family Applications Before (1)

Application Number Title Priority Date Filing Date
MX2017015720A MX2017015720A (es) 2015-06-05 2016-06-06 Procedimiento para la preparacion de una composicion purificada de acido.

Country Status (11)

Country Link
US (2) US10351544B2 (es)
EP (2) EP3303311B1 (es)
JP (2) JP6615231B2 (es)
KR (2) KR102067718B1 (es)
CN (2) CN107848998B (es)
AU (2) AU2016271835B2 (es)
BR (2) BR112017025910B1 (es)
CA (2) CA2988307C (es)
ES (2) ES2833165T3 (es)
MX (2) MX2017015720A (es)
WO (2) WO2016195500A1 (es)

Families Citing this family (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3402787A4 (en) 2016-01-13 2019-11-27 Stora Enso Oyj PROCESSES FOR PREPARING 2,5-FURANDICARBOXYLIC ACID AND INTERMEDIATES AND DERIVATIVES THEREOF
JP2017190316A (ja) * 2016-04-15 2017-10-19 三菱ケミカル株式会社 ２，５−フランジカルボン酸の精製方法
AU2018301662B2 (en) * 2017-07-12 2022-06-30 Stora Enso Oyj Purified 2,5-furandicarboxylic acid pathway products
EP3444354A1 (en) * 2017-08-16 2019-02-20 Basf Se Process of separating 2,5-diformylfuran from an aqueous mixture by cooling
TWI650318B (zh) 2017-10-30 2019-02-11 財團法人工業技術研究院 以結晶法純化２，５－呋喃二甲酸的粗產物之方法與聚酯之形成方法
US11236199B2 (en) * 2018-06-25 2022-02-01 Eastman Chemical Company Oxidation process to produce 5-(alkoxycarbonyl)furan-2-carboxylic acids (ACFC)
US11440895B2 (en) 2018-06-25 2022-09-13 Eastman Chemical Company Oxidation process to produce 5-(alkoxycarbonyl)furan-2-carboxylic acids (ACFC)
CN109293608B (zh) * 2018-09-21 2023-06-16 中国科学技术大学 一种5-甲酰基糠酸的制备方法
TWI697488B (zh) * 2019-07-02 2020-07-01 遠東新世紀股份有限公司 粗製2,5-呋喃二甲酸的純化方法
TWI697487B (zh) * 2019-07-02 2020-07-01 遠東新世紀股份有限公司 粗製2,5-呋喃二甲酸的純化方法
CN114364662A (zh) 2019-09-05 2022-04-15 伊士曼化工公司 用于生产5-(烷氧基羰基)-呋喃-2-甲酸的有效方法
KR20220118461A (ko) 2019-12-20 2022-08-25 퓨라닉스 테크놀러지스 비.브이. 정제된 2,5-후란디카복실릭 에시드 (2,5-furandicarboxylic acid) 의 유기산 및 열 처리
MX2022007653A (es) 2019-12-20 2022-07-19 Furanix Technologies Bv Tratamiento termico y con agua de acido 2,5-furandicarboxilico purificado.
CA3162304A1 (en) * 2019-12-20 2021-06-24 Hendrikus Jacob Baars Process for producing 2,5-furandicarboxylic acid from ethers of 5-hydroxymethylfurfural
BR112023024159A2 (pt) * 2021-05-20 2024-01-30 Eastman Chem Co Processo de purga para ácido 5-(alcoxicarbonil)furan-2-carboxílico (acfc)
KR20240012466A (ko) * 2021-05-20 2024-01-29 이스트만 케미칼 컴파니 Mcfc 공정에서 생성된 모액 조성물
EP4341250A1 (en) * 2021-05-20 2024-03-27 Eastman Chemical Company Purge process for 5-(methoxycarbonyl)furan-2-carboxylic acid (mcfc)
CN115028610B (zh) * 2022-05-07 2024-03-05 浙江恒逸石化研究院有限公司 一种2,5-呋喃二甲酸的纯化方法
WO2023242152A1 (en) 2022-06-14 2023-12-21 Furanix Technologies B.V. Producing 2,5-furandicarboxylic acid from mixed feed
WO2023242150A1 (en) 2022-06-14 2023-12-21 Furanix Technologies B.V. Producing 2,5-furandicarboxylic acid in the presence of modifying acid
WO2023242151A1 (en) 2022-06-14 2023-12-21 Furanix Technologies B.V. Producing 2,5-furandicarboxylic acid with recovery of acid
WO2024062084A1 (en) 2022-09-23 2024-03-28 Furanix Technologies B.V. Oxidation of furan derivative
CN115894411A (zh) * 2022-12-29 2023-04-04 厦门大学 低沸点溶液在2,5-呋喃二甲酸纯化中的应用及其纯化方法

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2893860B2 (ja) * 1990-05-17 1999-05-24 三菱瓦斯化学株式会社 高純度イソフタル酸の製造法
JPH05190908A (ja) 1992-01-13 1993-07-30 Nec Corp 光電変換装置
DE4334100C2 (de) 1992-10-13 2003-02-13 Mitsubishi Chem Corp Verfahren zur Herstellung hochreiner Terephthalsäure
JPH09151162A (ja) 1995-11-30 1997-06-10 Sekiyu Sangyo Kasseika Center ナフタレンジカルボン酸の精製法
US6265608B1 (en) 1998-06-30 2001-07-24 Eastman Chemical Company Method of purifying aromatic dicarboxylic acids
US6455742B1 (en) 1999-09-02 2002-09-24 Wisconsin Alumni Research Foundation Method for catalytically reducing carboxylic acid groups to hydroxyl groups in hydroxycarboxylic acids
ES2278267T3 (es) 2004-12-15 2007-08-01 Saudi Basic Industries Corporation Proceso para preparar acido tereftalico purificado.
PL2430010T3 (pl) 2009-05-14 2015-10-30 Archer Daniels Midland Co Utlenianie związków furfuralu
SG179041A1 (en) 2009-10-07 2012-04-27 Furanix Technologies Bv Method for the preparation of 2,5-furandicarboxylic acid and esters thereof
MX338371B (es) 2009-10-07 2016-04-12 Furanix Technologies Bv Metodo para la preparacion de acido 2,5-furandicarboxilico y para la preparacion del dialquilester de acido 2,5-furandicarboxilico.
US20120302773A1 (en) 2011-05-24 2012-11-29 Eastman Chemical Company Oxidation process to produce a crude and/or purified carboxylic acid product
US8969404B2 (en) 2012-06-22 2015-03-03 Eastman Chemical Company Purifying crude furan 2,5-dicarboxylic acid by hydrogenation
US8748479B2 (en) 2012-06-22 2014-06-10 Eastman Chemical Company Process for purifying crude furan 2,5-dicarboxylic acid using hydrogenation
US9006470B2 (en) * 2012-11-08 2015-04-14 Eastman Chemical Company Method of synthesizing low color furan diesters
US9156805B2 (en) 2012-11-20 2015-10-13 Eastman Chemical Company Oxidative purification method for producing purified dry furan-2,5-dicarboxylic acid
NL2010572C2 (en) 2013-04-05 2014-10-07 Furanix Technologies Bv Process for the preaparation of 2,5-furan-dicarboxylic acid.
EP3038997B1 (en) 2013-08-30 2018-02-21 Synvina C.V. Process for purifying an acid composition comprising 2-formyl-furan-5-carboxylic acid and 2,5-furandicarboxylic acid

Also Published As

Publication number Publication date
BR112017025913B1 (pt) 2022-08-23
CN107848998A (zh) 2018-03-27
CA2988307C (en) 2020-04-14
CN107848999B (zh) 2022-02-01
MX2017015720A (es) 2018-04-24
JP2018521980A (ja) 2018-08-09
US10351544B2 (en) 2019-07-16
CA2988392A1 (en) 2016-12-08
AU2016271835A1 (en) 2018-01-18
JP2018521978A (ja) 2018-08-09
JP6615230B2 (ja) 2019-12-04
JP6615231B2 (ja) 2019-12-04
US20180155308A1 (en) 2018-06-07
CN107848998B (zh) 2022-02-01
ES2833164T3 (es) 2021-06-14
CN107848999A (zh) 2018-03-27
WO2016195500A1 (en) 2016-12-08
BR112017025913A2 (pt) 2018-08-14
BR112017025910B1 (pt) 2022-08-23
EP3303310A1 (en) 2018-04-11
US10464913B2 (en) 2019-11-05
BR112017025910A2 (pt) 2018-08-14
KR20180014816A (ko) 2018-02-09
AU2016271834A1 (en) 2018-01-18
EP3303311B1 (en) 2020-08-26
WO2016195499A1 (en) 2016-12-08
CA2988307A1 (en) 2016-12-08
KR20180015720A (ko) 2018-02-13
KR102067718B1 (ko) 2020-01-30
US20180155309A1 (en) 2018-06-07
AU2016271835B2 (en) 2019-02-21
AU2016271834B2 (en) 2019-02-21
EP3303310B1 (en) 2020-08-26
KR102072002B1 (ko) 2020-01-31
CA2988392C (en) 2020-04-14
ES2833165T3 (es) 2021-06-14
EP3303311A1 (en) 2018-04-11

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