BR112012009430B1 - gordura sólida de girassol, método para fracionamento a seco para obtenção de gordura sólida de girassol, método para fracionamento com solvente para obtenção de gordura sólida de girassol, utilização de uma gordura sólida de girassol, e produto de confeitaria - Google Patents
gordura sólida de girassol, método para fracionamento a seco para obtenção de gordura sólida de girassol, método para fracionamento com solvente para obtenção de gordura sólida de girassol, utilização de uma gordura sólida de girassol, e produto de confeitaria Download PDFInfo
- Publication number
- BR112012009430B1 BR112012009430B1 BR112012009430A BR112012009430A BR112012009430B1 BR 112012009430 B1 BR112012009430 B1 BR 112012009430B1 BR 112012009430 A BR112012009430 A BR 112012009430A BR 112012009430 A BR112012009430 A BR 112012009430A BR 112012009430 B1 BR112012009430 B1 BR 112012009430B1
- Authority
- BR
- Brazil
- Prior art keywords
- sunflower
- fat
- oil
- triacylglycerol
- acid
- Prior art date
Links
- 238000005194 fractionation Methods 0.000 title claims description 90
- 239000007787 solid Substances 0.000 title claims description 70
- 239000002904 solvent Substances 0.000 title claims description 57
- 235000009508 confectionery Nutrition 0.000 title claims description 34
- 241000208818 Helianthus Species 0.000 title claims description 31
- 235000003222 Helianthus annuus Nutrition 0.000 title claims description 31
- 238000000034 method Methods 0.000 title claims description 15
- DCXXMTOCNZCJGO-UHFFFAOYSA-N tristearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 claims description 114
- 239000003921 oil Substances 0.000 claims description 93
- 235000019198 oils Nutrition 0.000 claims description 93
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims description 71
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims description 57
- UKMSUNONTOPOIO-UHFFFAOYSA-N docosanoic acid Chemical group CCCCCCCCCCCCCCCCCCCCCC(O)=O UKMSUNONTOPOIO-UHFFFAOYSA-N 0.000 claims description 32
- VKOBVWXKNCXXDE-UHFFFAOYSA-N icosanoic acid Chemical group CCCCCCCCCCCCCCCCCCCC(O)=O VKOBVWXKNCXXDE-UHFFFAOYSA-N 0.000 claims description 32
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 29
- 239000000047 product Substances 0.000 claims description 28
- 235000019486 Sunflower oil Nutrition 0.000 claims description 27
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 27
- 239000000194 fatty acid Substances 0.000 claims description 27
- 229930195729 fatty acid Natural products 0.000 claims description 27
- 150000004665 fatty acids Chemical class 0.000 claims description 27
- 239000002600 sunflower oil Substances 0.000 claims description 27
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical group CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 26
- 235000021355 Stearic acid Nutrition 0.000 claims description 24
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims description 24
- 239000008117 stearic acid Substances 0.000 claims description 24
- 235000019219 chocolate Nutrition 0.000 claims description 23
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 claims description 17
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 claims description 17
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 claims description 17
- 239000005642 Oleic acid Substances 0.000 claims description 17
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 claims description 17
- 239000013078 crystal Substances 0.000 claims description 17
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 claims description 17
- 239000002244 precipitate Substances 0.000 claims description 17
- 150000004671 saturated fatty acids Chemical class 0.000 claims description 17
- 235000021357 Behenic acid Nutrition 0.000 claims description 15
- 229940116226 behenic acid Drugs 0.000 claims description 15
- 235000021122 unsaturated fatty acids Nutrition 0.000 claims description 14
- 239000000693 micelle Substances 0.000 claims description 13
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 12
- 238000010899 nucleation Methods 0.000 claims description 12
- 238000001914 filtration Methods 0.000 claims description 10
- PHYFQTYBJUILEZ-IUPFWZBJSA-N triolein Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CCCCCCCC)COC(=O)CCCCCCC\C=C/CCCCCCCC PHYFQTYBJUILEZ-IUPFWZBJSA-N 0.000 claims description 10
- 238000002360 preparation method Methods 0.000 claims description 8
- 150000004670 unsaturated fatty acids Chemical class 0.000 claims description 7
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 6
- 238000009331 sowing Methods 0.000 claims description 6
- 238000013019 agitation Methods 0.000 claims description 5
- 230000003247 decreasing effect Effects 0.000 claims description 5
- 239000003960 organic solvent Substances 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 4
- 238000000926 separation method Methods 0.000 claims description 4
- 230000000717 retained effect Effects 0.000 claims description 3
- 238000007906 compression Methods 0.000 claims description 2
- 230000006835 compression Effects 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims description 2
- 239000007790 solid phase Substances 0.000 claims description 2
- 238000005406 washing Methods 0.000 claims description 2
- 238000005292 vacuum distillation Methods 0.000 claims 1
- 239000003925 fat Substances 0.000 description 134
- 235000019197 fats Nutrition 0.000 description 134
- 239000000203 mixture Substances 0.000 description 73
- 150000003626 triacylglycerols Chemical class 0.000 description 61
- 235000019868 cocoa butter Nutrition 0.000 description 49
- 229940110456 cocoa butter Drugs 0.000 description 45
- 238000004090 dissolution Methods 0.000 description 33
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 30
- 244000299461 Theobroma cacao Species 0.000 description 23
- OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 description 20
- 235000020778 linoleic acid Nutrition 0.000 description 20
- OYHQOLUKZRVURQ-IXWMQOLASA-N linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 description 20
- 125000003203 triacylglycerol group Chemical group 0.000 description 16
- 235000019841 confectionery fat Nutrition 0.000 description 14
- 235000021314 Palmitic acid Nutrition 0.000 description 13
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 13
- 239000002253 acid Substances 0.000 description 11
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 10
- 238000001816 cooling Methods 0.000 description 7
- 238000000113 differential scanning calorimetry Methods 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 7
- 230000006911 nucleation Effects 0.000 description 7
- 125000005314 unsaturated fatty acid group Chemical group 0.000 description 7
- PZNPLUBHRSSFHT-RRHRGVEJSA-N 1-hexadecanoyl-2-octadecanoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCCCC(=O)O[C@@H](COP([O-])(=O)OCC[N+](C)(C)C)COC(=O)CCCCCCCCCCCCCCC PZNPLUBHRSSFHT-RRHRGVEJSA-N 0.000 description 6
- 235000018936 Vitellaria paradoxa Nutrition 0.000 description 5
- 241001135917 Vitellaria paradoxa Species 0.000 description 5
- 238000002425 crystallisation Methods 0.000 description 5
- 230000008025 crystallization Effects 0.000 description 5
- 229920006395 saturated elastomer Polymers 0.000 description 5
- 235000003441 saturated fatty acids Nutrition 0.000 description 5
- 238000009482 thermal adhesion granulation Methods 0.000 description 5
- 230000000875 corresponding effect Effects 0.000 description 4
- 230000007423 decrease Effects 0.000 description 4
- 239000008347 soybean phospholipid Substances 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 235000004936 Bromus mango Nutrition 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 3
- 240000007228 Mangifera indica Species 0.000 description 3
- 235000014826 Mangifera indica Nutrition 0.000 description 3
- 235000009184 Spondias indica Nutrition 0.000 description 3
- 230000005496 eutectics Effects 0.000 description 3
- 230000001747 exhibiting effect Effects 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 239000004033 plastic Substances 0.000 description 3
- 241000894007 species Species 0.000 description 3
- 235000015112 vegetable and seed oil Nutrition 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 240000002791 Brassica napus Species 0.000 description 2
- 235000004977 Brassica sinapistrum Nutrition 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 230000000923 atherogenic effect Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000004061 bleaching Methods 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 239000002775 capsule Substances 0.000 description 2
- 235000012000 cholesterol Nutrition 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000006386 neutralization reaction Methods 0.000 description 2
- 235000019861 non-lauric fat Nutrition 0.000 description 2
- 229940049964 oleate Drugs 0.000 description 2
- 238000010791 quenching Methods 0.000 description 2
- 230000000171 quenching effect Effects 0.000 description 2
- 229940057910 shea butter Drugs 0.000 description 2
- 235000010692 trans-unsaturated fatty acids Nutrition 0.000 description 2
- 235000019871 vegetable fat Nutrition 0.000 description 2
- 230000017260 vegetative to reproductive phase transition of meristem Effects 0.000 description 2
- FDCOHGHEADZEGF-UHFFFAOYSA-N (E)-Glycerol 1,3-dihexadecanoate 2-9-octadecenoate Natural products CCCCCCCCCCCCCCCC(=O)OCC(COC(=O)CCCCCCCCCCCCCCC)OC(=O)CCCCCCCC=CCCCCCCCC FDCOHGHEADZEGF-UHFFFAOYSA-N 0.000 description 1
- RBLADLVPSYELCA-UHFFFAOYSA-N (Z)-Glycerol 1,3-dioctadecanoate 2-9-octadecenoate Natural products CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCC=CCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC RBLADLVPSYELCA-UHFFFAOYSA-N 0.000 description 1
- RBLADLVPSYELCA-IKPAITLHSA-N 1,3-bis(octadecanoyloxy)propan-2-yl (9z)-octadec-9-enoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC RBLADLVPSYELCA-IKPAITLHSA-N 0.000 description 1
- FDCOHGHEADZEGF-QPLCGJKRSA-N 1,3-dipalmitoyl-2-oleoylglycerol Chemical compound CCCCCCCCCCCCCCCC(=O)OCC(COC(=O)CCCCCCCCCCCCCCC)OC(=O)CCCCCCC\C=C/CCCCCCCC FDCOHGHEADZEGF-QPLCGJKRSA-N 0.000 description 1
- QXPXMOHHFYONAC-FEKLXSIDSA-N 1-palmitoyl-2-oleoyl-3-stearoyl-sn-glycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCCCCCCCCC)OC(=O)CCCCCCC\C=C/CCCCCCCC QXPXMOHHFYONAC-FEKLXSIDSA-N 0.000 description 1
- 206010003210 Arteriosclerosis Diseases 0.000 description 1
- 244000060011 Cocos nucifera Species 0.000 description 1
- 235000013162 Cocos nucifera Nutrition 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 102000007330 LDL Lipoproteins Human genes 0.000 description 1
- 239000005639 Lauric acid Substances 0.000 description 1
- 235000021360 Myristic acid Nutrition 0.000 description 1
- 239000004677 Nylon Substances 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 235000019482 Palm oil Nutrition 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 235000009470 Theobroma cacao Nutrition 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- DTOSIQBPPRVQHS-PDBXOOCHSA-N alpha-linolenic acid Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCC(O)=O DTOSIQBPPRVQHS-PDBXOOCHSA-N 0.000 description 1
- 235000020661 alpha-linolenic acid Nutrition 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 208000011775 arteriosclerosis disease Diseases 0.000 description 1
- 239000007844 bleaching agent Substances 0.000 description 1
- 235000014121 butter Nutrition 0.000 description 1
- 230000036996 cardiovascular health Effects 0.000 description 1
- 239000012159 carrier gas Substances 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 238000004590 computer program Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000002596 correlated effect Effects 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- YSXLJTGZMRNQSG-UHFFFAOYSA-L disodium;6-amino-5-[[2-[4-[2-[4-[2-[(2-amino-5-sulfonatonaphthalen-1-yl)diazenyl]phenyl]sulfonyloxyphenyl]propan-2-yl]phenoxy]sulfonylphenyl]diazenyl]naphthalene-1-sulfonate Chemical compound [Na+].[Na+].C1=CC=C2C(N=NC3=CC=CC=C3S(=O)(=O)OC3=CC=C(C=C3)C(C)(C=3C=CC(OS(=O)(=O)C=4C(=CC=CC=4)N=NC=4C5=CC=CC(=C5C=CC=4N)S([O-])(=O)=O)=CC=3)C)=C(N)C=CC2=C1S([O-])(=O)=O YSXLJTGZMRNQSG-UHFFFAOYSA-L 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 239000000374 eutectic mixture Substances 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 235000021588 free fatty acids Nutrition 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000010353 genetic engineering Methods 0.000 description 1
- 239000002044 hexane fraction Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052738 indium Inorganic materials 0.000 description 1
- APFVFJFRJDLVQX-UHFFFAOYSA-N indium atom Chemical compound [In] APFVFJFRJDLVQX-UHFFFAOYSA-N 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 235000019860 lauric fat Nutrition 0.000 description 1
- 229960004488 linolenic acid Drugs 0.000 description 1
- KQQKGWQCNNTQJW-UHFFFAOYSA-N linolenic acid Natural products CC=CCCC=CCC=CCCCCCCCC(O)=O KQQKGWQCNNTQJW-UHFFFAOYSA-N 0.000 description 1
- 235000013310 margarine Nutrition 0.000 description 1
- 239000003264 margarine Substances 0.000 description 1
- 150000004667 medium chain fatty acids Chemical class 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 230000003446 memory effect Effects 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- LAQFLZHBVPULPL-UHFFFAOYSA-N methyl(phenyl)silicon Chemical compound C[Si]C1=CC=CC=C1 LAQFLZHBVPULPL-UHFFFAOYSA-N 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 235000019629 palatability Nutrition 0.000 description 1
- 239000002540 palm oil Substances 0.000 description 1
- 235000011837 pasties Nutrition 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 210000002381 plasma Anatomy 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- NGVDGCNFYWLIFO-UHFFFAOYSA-N pyridoxal 5'-phosphate Chemical compound CC1=NC=C(COP(O)(O)=O)C(C=O)=C1O NGVDGCNFYWLIFO-UHFFFAOYSA-N 0.000 description 1
- QXPXMOHHFYONAC-UHFFFAOYSA-N rac-glyceryl-1-palmitate-2-oleate-3-stearate Natural products CCCCCCCCCCCCCCCCCC(=O)OCC(COC(=O)CCCCCCCCCCCCCCC)OC(=O)CCCCCCCC=CCCCCCCCC QXPXMOHHFYONAC-UHFFFAOYSA-N 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 235000019615 sensations Nutrition 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 235000002316 solid fats Nutrition 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 235000020238 sunflower seed Nutrition 0.000 description 1
- TUNFSRHWOTWDNC-UHFFFAOYSA-N tetradecanoic acid Chemical class CCCCCCCCCCCCCC(O)=O TUNFSRHWOTWDNC-UHFFFAOYSA-N 0.000 description 1
- 238000012876 topography Methods 0.000 description 1
- 235000021081 unsaturated fats Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G1/00—Cocoa; Cocoa products, e.g. chocolate; Substitutes therefor
- A23G1/30—Cocoa products, e.g. chocolate; Substitutes therefor
- A23G1/32—Cocoa products, e.g. chocolate; Substitutes therefor characterised by the composition containing organic or inorganic compounds
- A23G1/36—Cocoa products, e.g. chocolate; Substitutes therefor characterised by the composition containing organic or inorganic compounds characterised by the fats used
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G1/00—Cocoa; Cocoa products, e.g. chocolate; Substitutes therefor
- A23G1/30—Cocoa products, e.g. chocolate; Substitutes therefor
- A23G1/32—Cocoa products, e.g. chocolate; Substitutes therefor characterised by the composition containing organic or inorganic compounds
- A23G1/36—Cocoa products, e.g. chocolate; Substitutes therefor characterised by the composition containing organic or inorganic compounds characterised by the fats used
- A23G1/38—Cocoa butter substitutes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B7/00—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B7/00—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
- C11B7/0008—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of solubilities, e.g. by extraction, by separation from a solution by means of anti-solvents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B7/00—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
- C11B7/0075—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of melting or solidifying points
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS OR COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings or cooking oils
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS OR COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings or cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings or cooking oils characterised by the production or working-up
- A23D9/04—Working-up
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Inorganic Chemistry (AREA)
- Analytical Chemistry (AREA)
- Edible Oils And Fats (AREA)
- Confectionery (AREA)
- Fats And Perfumes (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP09382222A EP2319329A1 (en) | 2009-10-22 | 2009-10-22 | High melting point sunflower fat for confectionary |
| PCT/EP2010/065842 WO2011048169A1 (en) | 2009-10-22 | 2010-10-21 | High melting point sunflower fat for confectionary |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| BR112012009430A2 BR112012009430A2 (pt) | 2017-05-09 |
| BR112012009430A8 BR112012009430A8 (pt) | 2018-06-26 |
| BR112012009430B1 true BR112012009430B1 (pt) | 2018-10-30 |
Family
ID=41820486
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BR112012009430A BR112012009430B1 (pt) | 2009-10-22 | 2010-10-21 | gordura sólida de girassol, método para fracionamento a seco para obtenção de gordura sólida de girassol, método para fracionamento com solvente para obtenção de gordura sólida de girassol, utilização de uma gordura sólida de girassol, e produto de confeitaria |
Country Status (21)
| Country | Link |
|---|---|
| US (1) | US9072309B2 (https=) |
| EP (2) | EP2319329A1 (https=) |
| JP (1) | JP5916616B2 (https=) |
| KR (1) | KR20120104211A (https=) |
| CN (1) | CN102655762A (https=) |
| AR (1) | AR078721A1 (https=) |
| BR (1) | BR112012009430B1 (https=) |
| CA (1) | CA2778388A1 (https=) |
| CO (1) | CO6551699A2 (https=) |
| DK (1) | DK2490550T3 (https=) |
| EC (1) | ECSP12011919A (https=) |
| ES (1) | ES2568607T3 (https=) |
| HU (1) | HUE029204T2 (https=) |
| IL (1) | IL219291A (https=) |
| MX (1) | MX2012004683A (https=) |
| PL (1) | PL2490550T3 (https=) |
| RS (1) | RS54816B1 (https=) |
| RU (1) | RU2533018C2 (https=) |
| UA (1) | UA107682C2 (https=) |
| WO (1) | WO2011048169A1 (https=) |
| ZA (1) | ZA201202889B (https=) |
Families Citing this family (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2519332B1 (en) | 2009-12-30 | 2014-03-05 | BASF Pharma (Callanish) Limited | Simulated moving bed chromatographic separation process for the purification of polyunsaturated fatty acids |
| EP2622966A4 (en) * | 2010-09-27 | 2014-06-04 | Nisshin Oillio Group Ltd | FAT AND OIL COMPOSITION AND MANUFACTURING METHOD THEREFOR |
| GB201111595D0 (en) | 2011-07-06 | 2011-08-24 | Equateq Ltd | Improved process |
| GB201111594D0 (en) | 2011-07-06 | 2011-08-24 | Equateq Ltd | New improved process |
| JP5901345B2 (ja) * | 2012-02-27 | 2016-04-06 | 日清オイリオグループ株式会社 | 冷菓用チョコレート |
| KR101979887B1 (ko) * | 2012-09-07 | 2019-05-17 | 에이에이케이 아베 (파블) | 가공 식물성 지방의 분리를 위한 방법 |
| WO2014037007A1 (en) * | 2012-09-07 | 2014-03-13 | Aarhuskarlshamn Ab | Chocolate comprising a transesterified shea olein fraction |
| WO2014071945A1 (en) * | 2012-11-07 | 2014-05-15 | Aarhuskarlshamn Denmark A/S | Method for obtaining bloom-retarding components for confectionary products |
| GB201300354D0 (en) | 2013-01-09 | 2013-02-20 | Basf Pharma Callanish Ltd | Multi-step separation process |
| AU2014316548B2 (en) * | 2013-09-06 | 2017-08-17 | The Nisshin Oillio Group, Ltd. | Chocolate |
| CN105848491B (zh) * | 2013-12-27 | 2020-05-19 | 日清奥利友集团株式会社 | 巧克力及其制法、酱胚粘度上升抑制法、糖骨架形成法 |
| CN106686986B (zh) * | 2014-09-24 | 2020-10-16 | 日清奥利友集团株式会社 | 耐热性巧克力及其制造方法 |
| JP6534512B2 (ja) * | 2014-10-10 | 2019-06-26 | 株式会社Adeka | ハードバターの製造方法 |
| AR105814A1 (es) * | 2015-06-10 | 2017-11-15 | Aak Ab | Proceso para producir una suspensión de semilla y aparato para el mismo |
| MX2017015309A (es) * | 2015-06-10 | 2018-07-06 | Aak Ab Publ | Producto de confiteria. |
| EP3547842A1 (en) * | 2016-12-01 | 2019-10-09 | AAK AB (Publ) | Heat stable chocolate |
| WO2018138335A1 (en) * | 2017-01-30 | 2018-08-02 | Loders Croklaan B.V. | Fat composition |
| PL3758498T3 (pl) | 2018-03-01 | 2025-03-17 | Bunge Növényolajipari Zártköruen Muködo Részvénytársaság | Nowy wysokostearynowy tłuszcz stearynowy z nasion oleistych i sposób jego wytwarzania |
| JP7294957B2 (ja) * | 2019-08-30 | 2023-06-20 | 株式会社カネカ | ラウリン系油脂高含有ノーテンパリング型チョコレート及びそれを含む食品 |
| EP4106535A1 (en) * | 2020-02-21 | 2022-12-28 | Cargill, Incorporated | Cocoa composition |
| CA3182932A1 (en) | 2020-06-19 | 2021-12-23 | Bunge Loders Croklaan B.V. | Process of preparing a fat composition |
| JP7160234B1 (ja) * | 2021-03-31 | 2022-10-25 | 不二製油株式会社 | 非ラウリン、非トランス、非テンパリング型チョコレート類用油脂 |
| WO2025231540A1 (en) | 2024-05-07 | 2025-11-13 | Instituto De Tecnologia De Alimentos - Ital | Structuring fat, food product with spreadable and/or soft texture comprising said fat and process for manufacturing same, and uses of said structuring fat |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4199611A (en) * | 1978-08-30 | 1980-04-22 | Asahi Denka Kogyo K.K. | Cacao butter substitute |
| US5395531A (en) * | 1992-09-28 | 1995-03-07 | Pall Corporation | Method for fractionating a fat composition |
| US6229033B1 (en) | 1998-05-11 | 2001-05-08 | E. I. Du Pont De Nemours And Company | Fat products from high stearic soybean oil and a method for the production thereof |
| EP1554925A1 (en) | 1999-06-04 | 2005-07-20 | Consejo Superior de Investigaciones Cientificas | Food and cosmetic products comprising high oleic high stearic oils |
| US6388113B1 (en) * | 1999-06-04 | 2002-05-14 | Consejo Superior De Investigaciones Cientificas ( Csic) | High oleic/high stearic sunflower oils |
| BR0111588B1 (pt) | 2000-06-15 | 2011-12-13 | processos para a preparação de uma gordura de triglicerìdeo adequada para a estruturação de um óleo vegetal lìquido e para a preparação de uma fase de gordura, produto alimentìcio, e, uso de uma mistura de gordura. | |
| AR061984A1 (es) | 2006-07-14 | 2008-08-10 | Consejo Superior Investigacion | Aceites fraccionados liquidos y estables |
| EP1878786A1 (en) * | 2006-07-14 | 2008-01-16 | Consejo Superior De Investigaciones Cientificas (Csic) | Liquid and stable oil fractions |
| JP4628351B2 (ja) * | 2006-12-26 | 2011-02-09 | 株式会社カネカ | チョコレ−ト用油脂 |
| EP1992231A1 (en) * | 2007-05-15 | 2008-11-19 | Fuji Oil Europe | Food products with low content of saturated and trans unsaturated fats |
-
2009
- 2009-10-22 EP EP09382222A patent/EP2319329A1/en not_active Withdrawn
-
2010
- 2010-10-21 BR BR112012009430A patent/BR112012009430B1/pt active IP Right Grant
- 2010-10-21 US US13/503,331 patent/US9072309B2/en active Active
- 2010-10-21 WO PCT/EP2010/065842 patent/WO2011048169A1/en not_active Ceased
- 2010-10-21 KR KR1020127013017A patent/KR20120104211A/ko not_active Withdrawn
- 2010-10-21 HU HUE10773028A patent/HUE029204T2/en unknown
- 2010-10-21 EP EP10773028.5A patent/EP2490550B1/en active Active
- 2010-10-21 CA CA2778388A patent/CA2778388A1/en not_active Abandoned
- 2010-10-21 RS RS20160313A patent/RS54816B1/sr unknown
- 2010-10-21 ES ES10773028.5T patent/ES2568607T3/es active Active
- 2010-10-21 UA UAA201206146A patent/UA107682C2/ru unknown
- 2010-10-21 RU RU2012120869/13A patent/RU2533018C2/ru active
- 2010-10-21 PL PL10773028.5T patent/PL2490550T3/pl unknown
- 2010-10-21 MX MX2012004683A patent/MX2012004683A/es not_active Application Discontinuation
- 2010-10-21 JP JP2012534697A patent/JP5916616B2/ja active Active
- 2010-10-21 CN CN2010800547687A patent/CN102655762A/zh active Pending
- 2010-10-21 DK DK10773028.5T patent/DK2490550T3/en active
- 2010-10-22 AR ARP100103863A patent/AR078721A1/es active IP Right Grant
-
2012
- 2012-04-19 ZA ZA2012/02889A patent/ZA201202889B/en unknown
- 2012-04-19 IL IL219291A patent/IL219291A/en not_active IP Right Cessation
- 2012-05-22 CO CO12084020A patent/CO6551699A2/es active IP Right Grant
- 2012-05-22 EC ECSP12011919 patent/ECSP12011919A/es unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EP2319329A1 (en) | 2011-05-11 |
| WO2011048169A1 (en) | 2011-04-28 |
| ECSP12011919A (es) | 2012-07-31 |
| CA2778388A1 (en) | 2011-04-28 |
| EP2490550A1 (en) | 2012-08-29 |
| HUE029204T2 (en) | 2017-02-28 |
| UA107682C2 (uk) | 2015-02-10 |
| RU2533018C2 (ru) | 2014-11-20 |
| RU2012120869A (ru) | 2013-11-27 |
| JP2013507940A (ja) | 2013-03-07 |
| US20120269951A1 (en) | 2012-10-25 |
| PL2490550T3 (pl) | 2016-09-30 |
| ES2568607T3 (es) | 2016-05-03 |
| AR078721A1 (es) | 2011-11-30 |
| US9072309B2 (en) | 2015-07-07 |
| BR112012009430A8 (pt) | 2018-06-26 |
| DK2490550T3 (en) | 2016-06-13 |
| CO6551699A2 (es) | 2012-10-31 |
| ZA201202889B (en) | 2013-06-26 |
| JP5916616B2 (ja) | 2016-05-11 |
| EP2490550B1 (en) | 2016-03-09 |
| RS54816B1 (sr) | 2016-10-31 |
| KR20120104211A (ko) | 2012-09-20 |
| MX2012004683A (es) | 2012-06-14 |
| IL219291A0 (en) | 2012-06-28 |
| BR112012009430A2 (pt) | 2017-05-09 |
| CN102655762A (zh) | 2012-09-05 |
| IL219291A (en) | 2016-03-31 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| BR112012009430B1 (pt) | gordura sólida de girassol, método para fracionamento a seco para obtenção de gordura sólida de girassol, método para fracionamento com solvente para obtenção de gordura sólida de girassol, utilização de uma gordura sólida de girassol, e produto de confeitaria | |
| Jahurul et al. | Cocoa butter fats and possibilities of substitution in food products concerning cocoa varieties, alternative sources, extraction methods, composition, and characteristics | |
| Biswas et al. | Physical, rheological and sensorial properties, and bloom formation of dark chocolate made with cocoa butter substitute (CBS) | |
| Jahurul et al. | Characterization of crystallization and melting profiles of blends of mango seed fat and palm oil mid-fraction as cocoa butter replacers using differential scanning calorimetry and pulse nuclear magnetic resonance | |
| RU2303363C2 (ru) | Не содержащая лауриновой кислоты и жирных кислот транс-изомерной структуры, не нуждающаяся в темперировании(не-лтт) жировая композиция, способ ее получения и применение, и жировая композиция, ее содержащая | |
| Jahurul et al. | Thermal properties, triglycerides and crystal morphology of bambangan (Mangifera pajang) kernel fat and palm stearin blends as cocoa butter alternatives | |
| CN101835386B (zh) | 用于耐热巧克力的脂肪混合物 | |
| JPS61209298A (ja) | パ−ム油から調質性製菓用脂肪を得る溶剤分別法 | |
| JPS60101197A (ja) | 脂肪の乾式分画方法 | |
| JP6395747B2 (ja) | 油脂 | |
| ES3000723T3 (en) | New high stearic oilseed stearin fat and process for its preparation | |
| ES2901890T3 (es) | Composiciones de grasa | |
| CN112931670A (zh) | 一种用于巧克力的油脂与甜味剂组合物及其制备方法 | |
| JPH0425776B2 (https=) | ||
| De Clercq | Changing the functionality of cocoa butter | |
| JP6519279B2 (ja) | 新規なロールインマーガリン | |
| Marty-Terrade et al. | Impact of cocoa butter origin on crystal behavior | |
| JPS61254143A (ja) | ハ−ドバタ−の品質改良方法 | |
| JP3502158B2 (ja) | カカオ脂の分別方法及び該方法によって得られる分別脂を含有するチョコレート | |
| Jeyarani et al. | Cocoa butter extender from Simarouba glauca fat | |
| JPS6250089B2 (https=) | ||
| CN109640678A (zh) | 油包水型乳化物 | |
| HK1174795A (en) | High melting point sunflower fat for confectionary | |
| Joshi et al. | Chocolate: Chocolates from around the World, Simple Physics, Complex Flavour | |
| WO2026009890A1 (ja) | 油脂組成物およびチョコレート |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B06F | Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette] | ||
| B06A | Patent application procedure suspended [chapter 6.1 patent gazette] | ||
| B06A | Patent application procedure suspended [chapter 6.1 patent gazette] | ||
| B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
| B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 21/10/2010, OBSERVADAS AS CONDICOES LEGAIS. |