ATE511504T1 - Verfahren zur herstellung von hochreinem melamin aus harnstoff - Google Patents
Verfahren zur herstellung von hochreinem melamin aus harnstoffInfo
- Publication number
- ATE511504T1 ATE511504T1 AT09716759T AT09716759T ATE511504T1 AT E511504 T1 ATE511504 T1 AT E511504T1 AT 09716759 T AT09716759 T AT 09716759T AT 09716759 T AT09716759 T AT 09716759T AT E511504 T1 ATE511504 T1 AT E511504T1
- Authority
- AT
- Austria
- Prior art keywords
- melamine
- obtaining
- polycondensates
- ammeline
- ammelide
- Prior art date
Links
- 229920000877 Melamine resin Polymers 0.000 title abstract 14
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 title abstract 14
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 title 1
- 239000004202 carbamide Substances 0.000 title 1
- MASBWURJQFFLOO-UHFFFAOYSA-N ammeline Chemical compound NC1=NC(N)=NC(O)=N1 MASBWURJQFFLOO-UHFFFAOYSA-N 0.000 abstract 3
- 238000002425 crystallisation Methods 0.000 abstract 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
- YSKUZVBSHIWEFK-UHFFFAOYSA-N ammelide Chemical compound NC1=NC(O)=NC(O)=N1 YSKUZVBSHIWEFK-UHFFFAOYSA-N 0.000 abstract 2
- 230000008025 crystallization Effects 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 239000012452 mother liquor Substances 0.000 abstract 2
- 239000000243 solution Substances 0.000 abstract 2
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 230000003197 catalytic effect Effects 0.000 abstract 1
- 239000013078 crystal Substances 0.000 abstract 1
- 239000007789 gas Substances 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 238000010791 quenching Methods 0.000 abstract 1
- 230000000171 quenching effect Effects 0.000 abstract 1
- 238000003786 synthesis reaction Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/40—Nitrogen atoms
- C07D251/54—Three nitrogen atoms
- C07D251/62—Purification of melamine
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0004—Crystallisation cooling by heat exchange
- B01D9/0013—Crystallisation cooling by heat exchange by indirect heat exchange
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/006—Baffles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/1862—Stationary reactors having moving elements inside placed in series
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/1868—Stationary reactors having moving elements inside resulting in a loop-type movement
- B01J19/1881—Stationary reactors having moving elements inside resulting in a loop-type movement externally, i.e. the mixture leaving the vessel and subsequently re-entering it
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/40—Nitrogen atoms
- C07D251/54—Three nitrogen atoms
- C07D251/56—Preparation of melamine
- C07D251/60—Preparation of melamine from urea or from carbon dioxide and ammonia
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
- B01J2219/00083—Coils
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00761—Details of the reactor
- B01J2219/00763—Baffles
- B01J2219/00765—Baffles attached to the reactor wall
- B01J2219/00768—Baffles attached to the reactor wall vertical
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/40—Nitrogen atoms
- C07D251/42—One nitrogen atom
- C07D251/46—One nitrogen atom with oxygen or sulfur atoms attached to the two other ring carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/40—Nitrogen atoms
- C07D251/48—Two nitrogen atoms
- C07D251/52—Two nitrogen atoms with an oxygen or sulfur atom attached to the third ring carbon atom
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Removal Of Specific Substances (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP08004013A EP2098516A1 (de) | 2008-03-04 | 2008-03-04 | Verfahren zur Herstellung hochreinen Melamins aus Harnstoff |
| PCT/EP2009/001294 WO2009109314A1 (en) | 2008-03-04 | 2009-02-24 | Process for the production of high purity melamine from urea |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE511504T1 true ATE511504T1 (de) | 2011-06-15 |
Family
ID=39473225
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT09716759T ATE511504T1 (de) | 2008-03-04 | 2009-02-24 | Verfahren zur herstellung von hochreinem melamin aus harnstoff |
Country Status (15)
| Country | Link |
|---|---|
| US (2) | US9073877B2 (de) |
| EP (2) | EP2098516A1 (de) |
| JP (1) | JP5612488B2 (de) |
| KR (1) | KR101582307B1 (de) |
| CN (2) | CN102850286B (de) |
| AT (1) | ATE511504T1 (de) |
| AU (1) | AU2009221276B2 (de) |
| BR (1) | BRPI0909420B1 (de) |
| CA (1) | CA2716505C (de) |
| DK (1) | DK2254874T3 (de) |
| ES (1) | ES2367411T3 (de) |
| PL (1) | PL2254874T3 (de) |
| RU (1) | RU2515885C2 (de) |
| SA (1) | SA109300154B1 (de) |
| WO (1) | WO2009109314A1 (de) |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2308856A1 (de) | 2009-10-09 | 2011-04-13 | Borealis Agrolinz Melamine GmbH | Wasserrecycling in einem Melaminherstellungsprozess |
| CN103102319B (zh) * | 2011-11-11 | 2016-02-24 | 北京勤邦生物技术有限公司 | 三聚氰胺半抗原及其制备方法和应用 |
| CN102908802A (zh) * | 2012-11-07 | 2013-02-06 | 袁哲 | 一种新型三聚氰胺干捕器 |
| EP2907567A1 (de) * | 2014-02-18 | 2015-08-19 | Casale Sa | Kombinierter Reaktor für Hochdrucksynthese von Melamin |
| WO2016104446A1 (ja) * | 2014-12-26 | 2016-06-30 | 旭硝子株式会社 | ガラス及び化学強化ガラス |
| EP3279224A4 (de) * | 2015-03-31 | 2018-09-26 | Prime Polymer Co., Ltd. | Polypropylenharzzusammensetzung und herstellungsverfahren dafür, biaxal gestreckter film und herstellungsverfahren dafür und kondensatorfilm für filmkondensator |
| CN105289721B (zh) * | 2015-10-15 | 2018-01-02 | 广东工业大学 | 一种制备能降解多种染料的蜜勒胺的方法 |
| EP3272743A1 (de) | 2016-07-22 | 2018-01-24 | Casale SA | Verfahren zur reinigung von melamin |
| IT201700014505A1 (it) * | 2017-02-09 | 2018-08-09 | Eurotecnica Melamine Luxemburg Zweigniederlassung In Ittigen | Apparato di cristallizzazione di melammina e impianto di melammina impiegante lo stesso |
| RU2771242C2 (ru) | 2018-01-26 | 2022-04-28 | Касале Са | Установка синтеза меламина с использованием отходящего газа в присоединенной установке синтеза мочевины |
| CN108465288A (zh) * | 2018-05-07 | 2018-08-31 | 河南省中原大化集团有限责任公司 | 一种物料之间热能交换装置及应用方法 |
| IT201800005382A1 (it) * | 2018-05-15 | 2019-11-15 | Procedimento e dispositivo per separare cristalli di melammina in un processo di produzione di melammina da urea | |
| IT201800007367A1 (it) * | 2018-07-20 | 2020-01-20 | Procedimento a basso consumo energetico e ridotto consumo di ammoniaca per la produzione di melammina a elevata purezza tramite pirolisi dell’urea, e relativo impianto | |
| CN113663606A (zh) * | 2021-08-06 | 2021-11-19 | 四川金象赛瑞化工股份有限公司 | 一种单氰胺二聚反应器及其工艺 |
| CN114100494B (zh) * | 2021-11-08 | 2023-07-04 | 江西睿达新能源科技有限公司 | 一种三元前驱体的生产设备及生产工艺 |
| EP4605381A1 (de) | 2022-11-22 | 2025-08-27 | Stamicarbon B.V. | Gekoppelte harnstoffmelaminanlage |
| CN118341113B (zh) * | 2024-05-22 | 2026-04-17 | 东营市赫邦化工有限公司 | 基于盐酸羟胺母液设计的结晶设备 |
| EP4717692A1 (de) | 2024-09-26 | 2026-04-01 | Casale Sa | Verfahren zur herstellung von melamin durch harnstoffpyrolyse |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3161638A (en) | 1964-12-15 | Filter | ||
| US3161368A (en) | 1962-10-18 | 1964-12-15 | Inta Roto Machine Company Inc | Butt splicer |
| US3637686A (en) * | 1969-02-10 | 1972-01-25 | Nissan Chemical Ind Ltd | Process for recovering purified melamine |
| JPS5679678A (en) * | 1979-12-04 | 1981-06-30 | Mitsui Toatsu Chem Inc | Utilization and recovery of ammelide and ammeline |
| NL8201479A (nl) * | 1982-04-07 | 1983-11-01 | Stamicarbon | Werkwijze voor het bereiden van melamine. |
| IT1261841B (it) * | 1993-08-23 | 1996-06-03 | Conser Spa | Procedimento per la produzione di melammina ad alta purezza. |
| AT402294B (de) * | 1994-12-23 | 1997-03-25 | Agrolinz Melamin Gmbh | Verfahren zur herstellung von hochreinem melamin |
| CA2201224C (en) * | 1997-03-27 | 2004-12-07 | Annette Lynn Burke | Dual shear mixing element |
| JPH11209353A (ja) * | 1998-01-23 | 1999-08-03 | Nissan Chem Ind Ltd | メラミン工程廃液からのメラミン、アンメリン及びアンメリドの回収方法 |
| CZ20011625A3 (cs) * | 1998-11-13 | 2001-08-15 | Agrolinz Melamin Gmbh | Způsob výroby čistého melaminu |
| BR9916562A (pt) * | 1998-12-23 | 2001-10-09 | Agrolinz Melamin Gmbh | Processo para purificação de melamina |
| IT1315255B1 (it) * | 1999-11-16 | 2003-02-03 | Eurotecnica Dev And Licensing | Procedimento di purificazione della melammina. |
| EP1138676A1 (de) * | 2000-03-27 | 2001-10-04 | Casale Chemicals SA | Verfahren zur Herstellung von Melamin hoher Reinheit |
| AT410210B (de) * | 2000-08-07 | 2003-03-25 | Agrolinz Melamin Gmbh | Verfahren zur herstellung von melamin |
| EP1188751A1 (de) * | 2000-09-13 | 2002-03-20 | Casale Chemicals SA | Verfahren zur Herstellung von von hochreinem Melamin aus Harnstoff |
| ITMI20011216A1 (it) | 2001-06-08 | 2002-12-08 | Eurotecnica Dev And Licensing | Procedimento migliorato per la produzione con alte rese di melanina |
| PL209035B1 (pl) * | 2001-11-16 | 2011-07-29 | Ami Agrolinz Melamine Int Gmbh | Sposób wytwarzania melaminy pozbawionej melemu oraz bezprzeponowa chłodnica do stosowania tego sposobu |
| EP1716111B2 (de) * | 2004-02-20 | 2022-06-08 | Casale Sa | Integriertes verfahren zur herstellung von harnstoff und melamin |
| DE102004018784A1 (de) * | 2004-04-14 | 2005-11-03 | Ami-Agrolinz Melamine International Gmbh | Verfahren zur Herstellung von reinem Melamin |
| AT414239B (de) | 2004-07-29 | 2006-10-15 | Ami Agrolinz Melamine Int Gmbh | Hochdruckverfahren zur herstellung von reinem melamin |
-
2008
- 2008-03-04 EP EP08004013A patent/EP2098516A1/de not_active Withdrawn
-
2009
- 2009-02-24 EP EP09716759A patent/EP2254874B1/de active Active
- 2009-02-24 RU RU2010140444/04A patent/RU2515885C2/ru active
- 2009-02-24 CN CN201210362614.5A patent/CN102850286B/zh not_active Expired - Fee Related
- 2009-02-24 ES ES09716759T patent/ES2367411T3/es active Active
- 2009-02-24 US US12/920,730 patent/US9073877B2/en active Active
- 2009-02-24 JP JP2010549038A patent/JP5612488B2/ja active Active
- 2009-02-24 AT AT09716759T patent/ATE511504T1/de active
- 2009-02-24 CN CN2009801078284A patent/CN101959869B/zh not_active Expired - Fee Related
- 2009-02-24 KR KR1020107022190A patent/KR101582307B1/ko active Active
- 2009-02-24 CA CA2716505A patent/CA2716505C/en active Active
- 2009-02-24 WO PCT/EP2009/001294 patent/WO2009109314A1/en not_active Ceased
- 2009-02-24 PL PL09716759T patent/PL2254874T3/pl unknown
- 2009-02-24 AU AU2009221276A patent/AU2009221276B2/en not_active Ceased
- 2009-02-24 DK DK09716759.7T patent/DK2254874T3/da active
- 2009-02-24 BR BRPI0909420-2A patent/BRPI0909420B1/pt not_active IP Right Cessation
- 2009-03-04 SA SA109300154A patent/SA109300154B1/ar unknown
-
2012
- 2012-09-25 US US13/626,539 patent/US9045439B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| SA109300154B1 (ar) | 2012-01-24 |
| CN101959869A (zh) | 2011-01-26 |
| JP2011513348A (ja) | 2011-04-28 |
| US9073877B2 (en) | 2015-07-07 |
| CN102850286A (zh) | 2013-01-02 |
| KR101582307B1 (ko) | 2016-01-04 |
| US20110003990A1 (en) | 2011-01-06 |
| PL2254874T3 (pl) | 2011-10-31 |
| EP2254874B1 (de) | 2011-06-01 |
| US9045439B2 (en) | 2015-06-02 |
| JP5612488B2 (ja) | 2014-10-22 |
| RU2515885C2 (ru) | 2014-05-20 |
| WO2009109314A1 (en) | 2009-09-11 |
| CA2716505C (en) | 2016-06-21 |
| AU2009221276A1 (en) | 2009-09-11 |
| EP2254874A1 (de) | 2010-12-01 |
| EP2098516A1 (de) | 2009-09-09 |
| ES2367411T3 (es) | 2011-11-03 |
| KR20100123752A (ko) | 2010-11-24 |
| DK2254874T3 (da) | 2011-09-19 |
| CA2716505A1 (en) | 2009-09-11 |
| BRPI0909420B1 (pt) | 2019-10-15 |
| CN102850286B (zh) | 2015-01-14 |
| US20130028800A1 (en) | 2013-01-31 |
| RU2010140444A (ru) | 2012-04-10 |
| CN101959869B (zh) | 2013-03-27 |
| AU2009221276B2 (en) | 2012-11-15 |
| BRPI0909420A2 (pt) | 2019-02-26 |
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