AR054777A1 - Modificaciones cristalinas de piraclostrobina - Google Patents

Modificaciones cristalinas de piraclostrobina

Info

Publication number
AR054777A1
AR054777A1 ARP060102535A ARP060102535A AR054777A1 AR 054777 A1 AR054777 A1 AR 054777A1 AR P060102535 A ARP060102535 A AR P060102535A AR P060102535 A ARP060102535 A AR P060102535A AR 054777 A1 AR054777 A1 AR 054777A1
Authority
AR
Argentina
Prior art keywords
piraclostrobine
pyraclostrobin
crystal modifications
modifications
demonstrates
Prior art date
Application number
ARP060102535A
Other languages
English (en)
Inventor
H Ziegler
W Mayer
T Krohl
K-H Schneider
G Cox
P Erk
U J Vogelbacher
R Noack
R Gotz
J Wuckelt
M Rauls
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=37570793&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=AR054777(A1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Basf Ag filed Critical Basf Ag
Publication of AR054777A1 publication Critical patent/AR054777A1/es

Links

Classifications

    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/10Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof
    • A01N47/24Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof containing the groups, or; Thio analogues thereof
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D231/00Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/18One oxygen or sulfur atom
    • C07D231/20One oxygen atom attached in position 3 or 5
    • C07D231/22One oxygen atom attached in position 3 or 5 with aryl radicals attached to ring nitrogen atoms

Abstract

La presente se refiere a las modificaciones cristalinas de piraclostrobina, a los procedimientos para su preparacion y la utilizacion de las modificaciones para preparar composiciones para proteccion de cultivo. Reivindicacion 1: Una modificacion cristalina IV de piraclostrobina caracterizada porque, en un difractograma de polvo de rayos X a 25°C, demuestra por lo menos tres de los reflejos siguientes: d = 6,02 +- 0,01 L, d = 4,78 +- 0,01 L; d = 4,01 +- 0,01 L; d = 3,55 +- 0,01 L, d = 3,01 +- 0,01 L. Reivindicacion 15. Una modificacion cristalina II de piraclostrobina caracterizada porque, en un difractograma de polvo de rayos X a 25°C, demuestra por lo menos cuatro de los reflejos siguientes: d = 5,93 +- 0,01 L; d = 5,82 +- 0,01 L; d = 4,89 +- 0,01 L; d = 4,78 +- 0,01 L; d = 4,71 +- 0,01 L; d = 3,97 +- 0,01 L; d = 3,89 +- 0,01 L; d = 3,77 +- 0,01 L, d = 3,75 +- 0,01 L; d = 3,57 +- 0,01 L; d = 3,43 +- 0,01 L.
ARP060102535A 2005-06-20 2006-06-15 Modificaciones cristalinas de piraclostrobina AR054777A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102005028493 2005-06-20

Publications (1)

Publication Number Publication Date
AR054777A1 true AR054777A1 (es) 2007-07-18

Family

ID=37570793

Family Applications (2)

Application Number Title Priority Date Filing Date
ARP060102535A AR054777A1 (es) 2005-06-20 2006-06-15 Modificaciones cristalinas de piraclostrobina
ARP140102502A AR096819A2 (es) 2005-06-20 2014-07-04 Modificaciones cristalinas de piraclostrobina

Family Applications After (1)

Application Number Title Priority Date Filing Date
ARP140102502A AR096819A2 (es) 2005-06-20 2014-07-04 Modificaciones cristalinas de piraclostrobina

Country Status (34)

Country Link
US (2) US7816392B2 (es)
EP (2) EP2305033A1 (es)
JP (2) JP4997231B2 (es)
KR (1) KR101323051B1 (es)
CN (1) CN101203136B (es)
AP (1) AP2443A (es)
AR (2) AR054777A1 (es)
AT (1) ATE521238T1 (es)
AU (1) AU2006261191B2 (es)
BR (1) BRPI0612246B1 (es)
CA (1) CA2612075C (es)
CR (1) CR9569A (es)
CY (1) CY1112653T1 (es)
DK (1) DK1937071T3 (es)
EA (1) EA012454B1 (es)
EC (2) ECSP078032A (es)
ES (1) ES2371270T3 (es)
GT (1) GT200600264A (es)
HR (1) HRP20110802T1 (es)
IL (2) IL188240A0 (es)
MA (1) MA29627B1 (es)
ME (1) ME01961B (es)
MX (1) MX2007016271A (es)
NZ (1) NZ564023A (es)
PE (1) PE20070090A1 (es)
PL (1) PL1937071T3 (es)
PT (1) PT1937071E (es)
RS (1) RS51954B (es)
SI (1) SI1937071T1 (es)
TW (1) TWI393707B (es)
UA (1) UA89830C2 (es)
UY (1) UY29611A1 (es)
WO (1) WO2006136357A2 (es)
ZA (2) ZA200800504B (es)

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TW200901889A (en) * 2007-02-09 2009-01-16 Basf Se Crystalline complexes of agriculturally active organic compounds
RU2011106359A (ru) * 2008-07-24 2012-08-27 Басф Се (De) Эмульсия масло-в-воде, содержащая растворитель, воду, поверхностно-активное вещество и пестицид
WO2010015578A1 (en) * 2008-08-04 2010-02-11 Basf Se Method for controlling fungal diseases in legumes
TW201018400A (en) 2008-10-10 2010-05-16 Basf Se Liquid aqueous plant protection formulations
UA106213C2 (ru) * 2008-10-10 2014-08-11 Басф Се Жидкие препараты для защиты растений, содержащие пираклостробин
WO2011006896A2 (en) * 2009-07-14 2011-01-20 Basf Se A process for preparing an aqueous suspension of an organic pesticide compound
KR20120115492A (ko) 2009-11-06 2012-10-18 바스프 에스이 4―히드록시 벤조산 및 선택된 살충제의 결정질 복합체
CN103237451A (zh) * 2010-12-08 2013-08-07 巴斯夫欧洲公司 杀真菌混合物
CN102177902A (zh) * 2011-03-19 2011-09-14 陕西汤普森生物科技有限公司 一种含有吡唑醚菌酯的增效杀菌组合物
CN102100234B (zh) * 2011-03-23 2014-03-05 陕西汤普森生物科技有限公司 一种含吡唑醚菌酯与氨基甲酸酯类的杀菌组合物
CN102177912A (zh) * 2011-03-23 2011-09-14 陕西汤普森生物科技有限公司 一种含有吡唑醚菌酯的农药组合物
CN102273474A (zh) * 2011-08-22 2011-12-14 吴元林 一种含春雷霉素与吡唑醚菌酯的杀菌剂组合物及其应用
CN102399190A (zh) * 2011-12-20 2012-04-04 河南中医学院 一种经济型合成吡唑醚菌酯及其方法
CN102428953A (zh) * 2012-01-14 2012-05-02 陕西美邦农药有限公司 一种含硅噻菌胺与甲氧基丙烯酸酯类化合物的杀菌组合物
CN102669137A (zh) * 2012-05-17 2012-09-19 广东中迅农科股份有限公司 一种杀菌药肥颗粒剂
CN102805090A (zh) * 2012-07-11 2012-12-05 广东中迅农科股份有限公司 一种吡唑醚菌酯水悬浮剂及其制备方法
MX2015014010A (es) * 2013-04-03 2016-07-08 Fmc Corp Suspoemulsion de fomesafen y flutiacet-metilo.
CN104365590B (zh) * 2014-12-01 2016-03-30 山东省联合农药工业有限公司 一种连续化的吡唑醚菌酯悬浮剂制备方法
CN104872160A (zh) * 2015-05-14 2015-09-02 京博农化科技股份有限公司 一种吡唑醚菌酯制剂及其制备方法
CA2994399C (en) 2015-08-10 2023-10-17 Basf Se A process for preparing crystalline methyl n-[2-[[[1-(4-chlorophen yl)-1h-pyrazol-3-yl]oxy]methyl]phenyl]-n-methoxycarbamate
GB2552694B (en) * 2016-08-04 2020-03-04 Rotam Agrochem Int Co Ltd A Synergistic fungicidal composition and use thereof
CN106928144A (zh) * 2017-03-16 2017-07-07 上海晓明检测技术服务有限公司 一种高纯度吡唑醚菌酯标准品的制备方法
CN106977459B (zh) * 2017-03-28 2019-11-29 天津大学 一种提高吡唑醚菌酯堆密度和流动性的结晶方法
CN107021927B (zh) * 2017-03-28 2020-05-29 天津大学 一种吡唑醚菌酯晶型及其制备方法
CN106866533B (zh) * 2017-03-28 2022-03-11 天津大学 吡唑醚菌酯晶型及制备方法
CN108117521A (zh) * 2018-03-05 2018-06-05 安徽国星生物化学有限公司 一种吡唑醚菌酯的反向重结晶方法
CN110041258A (zh) * 2019-04-26 2019-07-23 永农生物科学有限公司 一种吡唑醚菌酯的混合晶型及其制备方法
CN110590672A (zh) * 2019-09-09 2019-12-20 海利尔药业集团股份有限公司 一种吡唑醚菌酯ⅱ型晶型的制备方法

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DE4423612A1 (de) 1994-07-06 1996-01-11 Basf Ag 2-[(Dihydro)pyrazolyl-3'-oxymethylen]-anilide, Verfahren zu ihrer Herstelung und ihre Verwendung
TW460476B (en) 1997-04-14 2001-10-21 American Cyanamid Co Fungicidal trifluoromethylalkylamino-triazolopyrimidines
CN1114606C (zh) 1998-02-11 2003-07-16 美国氰胺公司 具有杀真菌活性的7-烷基-三唑并嘧啶化合物
ES2281535T3 (es) 2001-07-05 2007-10-01 Basf Aktiengesellschaft Triazolopirimidinas fungicidas, metodo para la produccion de las mismas y su uso para el control de hongos nocivos y de agentes que contienen a dichos compuestos.
NZ535337A (en) * 2002-03-28 2006-03-31 Basf Ag Method of purifying a pesticide
DE10233171A1 (de) * 2002-07-22 2004-02-12 Bayer Cropscience Ag Kristallmodifikation II des 2-[2-(Chlor-cyclopropyl)-3-(2-chlorphenyl)-2-hydroxy-propyl]-2,4dihydro-3H-1,2,4-triazol-3-thions

Also Published As

Publication number Publication date
IL188240A0 (en) 2008-04-13
ECSP078032A (es) 2008-01-23
AU2006261191B2 (en) 2012-03-08
CN101203136B (zh) 2012-09-26
UY29611A1 (es) 2007-01-31
AP2443A (en) 2012-08-31
BRPI0612246A2 (pt) 2011-01-04
CA2612075C (en) 2013-09-17
CA2612075A1 (en) 2006-12-28
US20080234350A1 (en) 2008-09-25
PT1937071E (pt) 2011-10-03
ZA201008744B (en) 2012-02-29
ECSP11008032A (es) 2012-01-31
EP2305033A1 (de) 2011-04-06
EP1937071B1 (de) 2011-08-24
HRP20110802T1 (hr) 2011-11-30
PE20070090A1 (es) 2007-02-09
GT200600264A (es) 2007-01-23
JP2012067107A (ja) 2012-04-05
IL215015A0 (en) 2011-11-30
US8404734B2 (en) 2013-03-26
MX2007016271A (es) 2008-03-07
ATE521238T1 (de) 2011-09-15
WO2006136357A3 (de) 2007-03-29
ZA200800504B (en) 2011-02-23
UA89830C2 (ru) 2010-03-10
SI1937071T1 (sl) 2011-12-30
AP2007004294A0 (en) 2007-12-31
JP4997231B2 (ja) 2012-08-08
RS51954B (en) 2012-02-29
DK1937071T3 (da) 2011-11-28
BRPI0612246B1 (pt) 2022-08-30
US7816392B2 (en) 2010-10-19
MA29627B1 (fr) 2008-07-01
AU2006261191A1 (en) 2006-12-28
JP2008543804A (ja) 2008-12-04
CR9569A (es) 2008-04-09
AR096819A2 (es) 2016-02-03
KR20080027776A (ko) 2008-03-28
KR101323051B1 (ko) 2013-11-25
CN101203136A (zh) 2008-06-18
EA200702586A1 (ru) 2008-06-30
ES2371270T3 (es) 2011-12-29
NZ564023A (en) 2010-11-26
ME01961B (me) 2012-02-29
CY1112653T1 (el) 2016-02-10
US20110054000A1 (en) 2011-03-03
TWI393707B (zh) 2013-04-21
EP1937071A2 (de) 2008-07-02
WO2006136357A2 (de) 2006-12-28
TW200740765A (en) 2007-11-01
PL1937071T3 (pl) 2012-01-31
EA012454B1 (ru) 2009-10-30

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