ZA200401476B - Carotenoid extraction process. - Google Patents
Carotenoid extraction process. Download PDFInfo
- Publication number
- ZA200401476B ZA200401476B ZA200401476A ZA200401476A ZA200401476B ZA 200401476 B ZA200401476 B ZA 200401476B ZA 200401476 A ZA200401476 A ZA 200401476A ZA 200401476 A ZA200401476 A ZA 200401476A ZA 200401476 B ZA200401476 B ZA 200401476B
- Authority
- ZA
- South Africa
- Prior art keywords
- process according
- plant matter
- oleoresin
- carotenoid
- stage
- Prior art date
Links
- 235000021466 carotenoid Nutrition 0.000 title claims abstract description 47
- 150000001747 carotenoids Chemical class 0.000 title claims abstract description 47
- 238000000605 extraction Methods 0.000 title claims description 34
- 239000008601 oleoresin Substances 0.000 claims abstract description 47
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000000203 mixture Substances 0.000 claims abstract description 19
- 210000002966 serum Anatomy 0.000 claims abstract description 11
- 238000002156 mixing Methods 0.000 claims abstract description 3
- 241000196324 Embryophyta Species 0.000 claims description 45
- 238000000034 method Methods 0.000 claims description 44
- 239000002904 solvent Substances 0.000 claims description 43
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 39
- 230000008569 process Effects 0.000 claims description 39
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 21
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 17
- KBPHJBAIARWVSC-XQIHNALSSA-N trans-lutein Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CC(O)CC1(C)C)C=CC=C(/C)C=CC2C(=CC(O)CC2(C)C)C KBPHJBAIARWVSC-XQIHNALSSA-N 0.000 claims description 17
- 244000000626 Daucus carota Species 0.000 claims description 16
- 235000002767 Daucus carota Nutrition 0.000 claims description 16
- UPYKUZBSLRQECL-UKMVMLAPSA-N Lycopene Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1C(=C)CCCC1(C)C)C=CC=C(/C)C=CC2C(=C)CCCC2(C)C UPYKUZBSLRQECL-UKMVMLAPSA-N 0.000 claims description 15
- JEVVKJMRZMXFBT-XWDZUXABSA-N Lycophyll Natural products OC/C(=C/CC/C(=C\C=C\C(=C/C=C/C(=C\C=C\C=C(/C=C/C=C(\C=C\C=C(/CC/C=C(/CO)\C)\C)/C)\C)/C)\C)/C)/C JEVVKJMRZMXFBT-XWDZUXABSA-N 0.000 claims description 13
- 235000012661 lycopene Nutrition 0.000 claims description 13
- 239000001751 lycopene Substances 0.000 claims description 13
- OAIJSZIZWZSQBC-GYZMGTAESA-N lycopene Chemical compound CC(C)=CCC\C(C)=C\C=C\C(\C)=C\C=C\C(\C)=C\C=C\C=C(/C)\C=C\C=C(/C)\C=C\C=C(/C)CCC=C(C)C OAIJSZIZWZSQBC-GYZMGTAESA-N 0.000 claims description 13
- 229960004999 lycopene Drugs 0.000 claims description 13
- ZCIHMQAPACOQHT-ZGMPDRQDSA-N trans-isorenieratene Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/c1c(C)ccc(C)c1C)C=CC=C(/C)C=Cc2c(C)ccc(C)c2C ZCIHMQAPACOQHT-ZGMPDRQDSA-N 0.000 claims description 13
- JKQXZKUSFCKOGQ-LQFQNGICSA-N Z-zeaxanthin Natural products C([C@H](O)CC=1C)C(C)(C)C=1C=CC(C)=CC=CC(C)=CC=CC=C(C)C=CC=C(C)C=CC1=C(C)C[C@@H](O)CC1(C)C JKQXZKUSFCKOGQ-LQFQNGICSA-N 0.000 claims description 12
- QOPRSMDTRDMBNK-RNUUUQFGSA-N Zeaxanthin Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CCC(O)C1(C)C)C=CC=C(/C)C=CC2=C(C)CC(O)CC2(C)C QOPRSMDTRDMBNK-RNUUUQFGSA-N 0.000 claims description 12
- JKQXZKUSFCKOGQ-LOFNIBRQSA-N all-trans-Zeaxanthin Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CC(O)CC1(C)C)C=CC=C(/C)C=CC2=C(C)CC(O)CC2(C)C JKQXZKUSFCKOGQ-LOFNIBRQSA-N 0.000 claims description 12
- 235000010930 zeaxanthin Nutrition 0.000 claims description 12
- 239000001775 zeaxanthin Substances 0.000 claims description 12
- 229940043269 zeaxanthin Drugs 0.000 claims description 12
- 150000001746 carotenes Chemical class 0.000 claims description 11
- 235000005473 carotenes Nutrition 0.000 claims description 11
- 239000007787 solid Substances 0.000 claims description 11
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 10
- 244000241838 Lycium barbarum Species 0.000 claims description 10
- 235000015459 Lycium barbarum Nutrition 0.000 claims description 10
- JKQXZKUSFCKOGQ-JLGXGRJMSA-N (3R,3'R)-beta,beta-carotene-3,3'-diol Chemical compound C([C@H](O)CC=1C)C(C)(C)C=1/C=C/C(/C)=C/C=C/C(/C)=C/C=C/C=C(C)C=CC=C(C)C=CC1=C(C)C[C@@H](O)CC1(C)C JKQXZKUSFCKOGQ-JLGXGRJMSA-N 0.000 claims description 9
- 235000008210 xanthophylls Nutrition 0.000 claims description 9
- ANVAOWXLWRTKGA-XHGAXZNDSA-N all-trans-alpha-carotene Chemical compound CC=1CCCC(C)(C)C=1/C=C/C(/C)=C/C=C/C(/C)=C/C=C/C=C(C)C=CC=C(C)C=CC1C(C)=CCCC1(C)C ANVAOWXLWRTKGA-XHGAXZNDSA-N 0.000 claims description 8
- 235000013399 edible fruits Nutrition 0.000 claims description 6
- 238000007127 saponification reaction Methods 0.000 claims description 6
- 235000015113 tomato pastes and purées Nutrition 0.000 claims description 6
- 150000003735 xanthophylls Chemical class 0.000 claims description 6
- 235000003903 alpha-carotene Nutrition 0.000 claims description 5
- 235000013734 beta-carotene Nutrition 0.000 claims description 5
- 239000011648 beta-carotene Substances 0.000 claims description 5
- 229960004592 isopropanol Drugs 0.000 claims description 5
- 229960005375 lutein Drugs 0.000 claims description 5
- FJHBOVDFOQMZRV-XQIHNALSSA-N xanthophyll Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CC(O)CC1(C)C)C=CC=C(/C)C=CC2C=C(C)C(O)CC2(C)C FJHBOVDFOQMZRV-XQIHNALSSA-N 0.000 claims description 5
- -1 xanthophyll ester Chemical class 0.000 claims description 5
- YVLPJIGOMTXXLP-UHFFFAOYSA-N 15-cis-phytoene Chemical compound CC(C)=CCCC(C)=CCCC(C)=CCCC(C)=CC=CC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)C YVLPJIGOMTXXLP-UHFFFAOYSA-N 0.000 claims description 4
- OENHQHLEOONYIE-UKMVMLAPSA-N all-trans beta-carotene Natural products CC=1CCCC(C)(C)C=1/C=C/C(/C)=C/C=C/C(/C)=C/C=C/C=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C OENHQHLEOONYIE-UKMVMLAPSA-N 0.000 claims description 4
- 239000011795 alpha-carotene Substances 0.000 claims description 4
- ANVAOWXLWRTKGA-HLLMEWEMSA-N alpha-carotene Natural products C(=C\C=C\C=C(/C=C/C=C(\C=C\C=1C(C)(C)CCCC=1C)/C)\C)(\C=C\C=C(/C=C/[C@H]1C(C)=CCCC1(C)C)\C)/C ANVAOWXLWRTKGA-HLLMEWEMSA-N 0.000 claims description 4
- TUPZEYHYWIEDIH-WAIFQNFQSA-N beta-carotene Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CCCC1(C)C)C=CC=C(/C)C=CC2=CCCCC2(C)C TUPZEYHYWIEDIH-WAIFQNFQSA-N 0.000 claims description 4
- FDSDTBUPSURDBL-LOFNIBRQSA-N canthaxanthin Chemical compound CC=1C(=O)CCC(C)(C)C=1/C=C/C(/C)=C/C=C/C(/C)=C/C=C/C=C(C)C=CC=C(C)C=CC1=C(C)C(=O)CCC1(C)C FDSDTBUPSURDBL-LOFNIBRQSA-N 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 4
- KBPHJBAIARWVSC-RGZFRNHPSA-N lutein Chemical compound C([C@H](O)CC=1C)C(C)(C)C=1\C=C\C(\C)=C\C=C\C(\C)=C\C=C\C=C(/C)\C=C\C=C(/C)\C=C\[C@H]1C(C)=C[C@H](O)CC1(C)C KBPHJBAIARWVSC-RGZFRNHPSA-N 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 4
- OENHQHLEOONYIE-JLTXGRSLSA-N β-Carotene Chemical compound CC=1CCCC(C)(C)C=1\C=C\C(\C)=C\C=C\C(\C)=C\C=C\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C OENHQHLEOONYIE-JLTXGRSLSA-N 0.000 claims description 4
- 239000002028 Biomass Substances 0.000 claims description 3
- VYIRVAXUEZSDNC-TXDLOWMYSA-N (3R,3'S,5'R)-3,3'-dihydroxy-beta-kappa-caroten-6'-one Chemical compound C([C@H](O)CC=1C)C(C)(C)C=1/C=C/C(/C)=C/C=C/C(/C)=C/C=C/C=C(C)C=CC=C(C)C=CC(=O)[C@]1(C)C[C@@H](O)CC1(C)C VYIRVAXUEZSDNC-TXDLOWMYSA-N 0.000 claims description 2
- YVLPJIGOMTXXLP-UUKUAVTLSA-N 15,15'-cis-Phytoene Natural products C(=C\C=C/C=C(\CC/C=C(\CC/C=C(\CC/C=C(\C)/C)/C)/C)/C)(\CC/C=C(\CC/C=C(\CC/C=C(\C)/C)/C)/C)/C YVLPJIGOMTXXLP-UUKUAVTLSA-N 0.000 claims description 2
- YVLPJIGOMTXXLP-BAHRDPFUSA-N 15Z-phytoene Natural products CC(=CCCC(=CCCC(=CCCC(=CC=C/C=C(C)/CCC=C(/C)CCC=C(/C)CCC=C(C)C)C)C)C)C YVLPJIGOMTXXLP-BAHRDPFUSA-N 0.000 claims description 2
- JEBFVOLFMLUKLF-IFPLVEIFSA-N Astaxanthin Natural products CC(=C/C=C/C(=C/C=C/C1=C(C)C(=O)C(O)CC1(C)C)/C)C=CC=C(/C)C=CC=C(/C)C=CC2=C(C)C(=O)C(O)CC2(C)C JEBFVOLFMLUKLF-IFPLVEIFSA-N 0.000 claims description 2
- VYIRVAXUEZSDNC-LOFNIBRQSA-N Capsanthyn Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CC(O)CC1(C)C)C=CC=C(/C)C=CC(=O)C2(C)CC(O)CC2(C)C VYIRVAXUEZSDNC-LOFNIBRQSA-N 0.000 claims description 2
- OOUTWVMJGMVRQF-DOYZGLONSA-N Phoenicoxanthin Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)C(=O)C(O)CC1(C)C)C=CC=C(/C)C=CC2=C(C)C(=O)CCC2(C)C OOUTWVMJGMVRQF-DOYZGLONSA-N 0.000 claims description 2
- 235000013793 astaxanthin Nutrition 0.000 claims description 2
- 239000001168 astaxanthin Substances 0.000 claims description 2
- 229940022405 astaxanthin Drugs 0.000 claims description 2
- MQZIGYBFDRPAKN-ZWAPEEGVSA-N astaxanthin Chemical compound C([C@H](O)C(=O)C=1C)C(C)(C)C=1/C=C/C(/C)=C/C=C/C(/C)=C/C=C/C=C(C)C=CC=C(C)C=CC1=C(C)C(=O)[C@@H](O)CC1(C)C MQZIGYBFDRPAKN-ZWAPEEGVSA-N 0.000 claims description 2
- 235000012682 canthaxanthin Nutrition 0.000 claims description 2
- 239000001659 canthaxanthin Substances 0.000 claims description 2
- 229940008033 canthaxanthin Drugs 0.000 claims description 2
- 235000018889 capsanthin Nutrition 0.000 claims description 2
- WRANYHFEXGNSND-LOFNIBRQSA-N capsanthin Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CC(O)CC1(C)C)C=CC=C(/C)C=CC(=O)C2(C)CCC(O)C2(C)C WRANYHFEXGNSND-LOFNIBRQSA-N 0.000 claims description 2
- OVSVTCFNLSGAMM-KGBODLQUSA-N cis-phytofluene Natural products CC(=CCCC(=CCCC(=CCCC(=CC=C/C=C(C)/C=C/C=C(C)/CCC=C(/C)CCC=C(C)C)C)C)C)C OVSVTCFNLSGAMM-KGBODLQUSA-N 0.000 claims description 2
- 235000014666 liquid concentrate Nutrition 0.000 claims description 2
- 235000012680 lutein Nutrition 0.000 claims description 2
- 239000001656 lutein Substances 0.000 claims description 2
- ORAKUVXRZWMARG-WZLJTJAWSA-N lutein Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CCCC1(C)C)C=CC=C(/C)C=CC2C(=CC(O)CC2(C)C)C ORAKUVXRZWMARG-WZLJTJAWSA-N 0.000 claims description 2
- 235000012658 paprika extract Nutrition 0.000 claims description 2
- 239000001688 paprika extract Substances 0.000 claims description 2
- 235000011765 phytoene Nutrition 0.000 claims description 2
- 235000002677 phytofluene Nutrition 0.000 claims description 2
- OVSVTCFNLSGAMM-UZFNGAIXSA-N phytofluene Chemical compound CC(C)=CCCC(C)=CCCC(C)=CCCC(C)=CC=C\C=C(/C)\C=C\C=C(C)CCC=C(C)CCC=C(C)C OVSVTCFNLSGAMM-UZFNGAIXSA-N 0.000 claims description 2
- ZYSFBWMZMDHGOJ-SGKBLAECSA-N phytofluene Natural products CC(=CCCC(=CCCC(=CCCC(=CC=C/C=C(C)/CCC=C(/C)C=CC=C(/C)CCC=C(C)C)C)C)C)C ZYSFBWMZMDHGOJ-SGKBLAECSA-N 0.000 claims description 2
- ZIUDAKDLOLDEGU-UHFFFAOYSA-N trans-Phytofluen Natural products CC(C)=CCCC(C)CCCC(C)CC=CC(C)=CC=CC=C(C)C=CCC(C)CCCC(C)CCC=C(C)C ZIUDAKDLOLDEGU-UHFFFAOYSA-N 0.000 claims description 2
- 240000008042 Zea mays Species 0.000 claims 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 claims 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 claims 1
- 229960002747 betacarotene Drugs 0.000 claims 1
- 235000005822 corn Nutrition 0.000 claims 1
- 239000000284 extract Substances 0.000 description 21
- 241000227653 Lycopersicon Species 0.000 description 14
- 235000007688 Lycopersicon esculentum Nutrition 0.000 description 14
- 238000000926 separation method Methods 0.000 description 11
- 239000012071 phase Substances 0.000 description 10
- 235000015468 Lycium chinense Nutrition 0.000 description 8
- 235000008504 concentrate Nutrition 0.000 description 6
- 239000012141 concentrate Substances 0.000 description 6
- 238000001914 filtration Methods 0.000 description 6
- 150000004676 glycans Chemical class 0.000 description 5
- 239000005017 polysaccharide Substances 0.000 description 5
- 229920001282 polysaccharide Polymers 0.000 description 5
- 239000008346 aqueous phase Substances 0.000 description 4
- 238000005119 centrifugation Methods 0.000 description 4
- 238000010908 decantation Methods 0.000 description 4
- 238000001704 evaporation Methods 0.000 description 4
- 230000008020 evaporation Effects 0.000 description 4
- 238000002955 isolation Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- XACHQDDXHDTRLX-XLVVAOPESA-N Physalien Chemical compound CC1(C)C[C@H](OC(=O)CCCCCCCCCCCCCCC)CC(C)=C1\C=C\C(\C)=C\C=C\C(\C)=C\C=C\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)C[C@@H](OC(=O)CCCCCCCCCCCCCCC)CC1(C)C XACHQDDXHDTRLX-XLVVAOPESA-N 0.000 description 3
- XACHQDDXHDTRLX-GMPBGBGESA-N Physalien Natural products O=C(O[C@H]1CC(C)(C)C(/C=C/C(=C\C=C\C(=C/C=C/C=C(\C=C\C=C(/C=C/C=2C(C)(C)C[C@H](OC(=O)CCCCCCCCCCCCCCC)CC=2C)\C)/C)\C)/C)=C(C)C1)CCCCCCCCCCCCCCC XACHQDDXHDTRLX-GMPBGBGESA-N 0.000 description 3
- XACHQDDXHDTRLX-UHFFFAOYSA-N Zeaxanthin-dipalmitat Natural products CC1(C)CC(OC(=O)CCCCCCCCCCCCCCC)CC(C)=C1C=CC(C)=CC=CC(C)=CC=CC=C(C)C=CC=C(C)C=CC1=C(C)CC(OC(=O)CCCCCCCCCCCCCCC)CC1(C)C XACHQDDXHDTRLX-UHFFFAOYSA-N 0.000 description 3
- 235000010208 anthocyanin Nutrition 0.000 description 3
- 239000000470 constituent Substances 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- 150000008442 polyphenolic compounds Chemical class 0.000 description 3
- 235000013824 polyphenols Nutrition 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 150000005690 diesters Chemical class 0.000 description 2
- 238000007865 diluting Methods 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 150000002632 lipids Chemical class 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 239000007790 solid phase Substances 0.000 description 2
- NCYCYZXNIZJOKI-UHFFFAOYSA-N vitamin A aldehyde Natural products O=CC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C NCYCYZXNIZJOKI-UHFFFAOYSA-N 0.000 description 2
- MIDXCONKKJTLDX-UHFFFAOYSA-N 3,5-dimethylcyclopentane-1,2-dione Chemical compound CC1CC(C)C(=O)C1=O MIDXCONKKJTLDX-UHFFFAOYSA-N 0.000 description 1
- 241000195493 Cryptophyta Species 0.000 description 1
- 241001106041 Lycium Species 0.000 description 1
- 241001291279 Solanum galapagense Species 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
- 230000006978 adaptation Effects 0.000 description 1
- 150000001373 alpha-carotenes Chemical class 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 230000003466 anti-cipated effect Effects 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 235000021028 berry Nutrition 0.000 description 1
- 150000001579 beta-carotenes Chemical class 0.000 description 1
- 235000013736 caramel Nutrition 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 235000011869 dried fruits Nutrition 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 230000036571 hydration Effects 0.000 description 1
- 238000006703 hydration reaction Methods 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000010951 particle size reduction Methods 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- GOLXNESZZPUPJE-UHFFFAOYSA-N spiromesifen Chemical compound CC1=CC(C)=CC(C)=C1C(C(O1)=O)=C(OC(=O)CC(C)(C)C)C11CCCC1 GOLXNESZZPUPJE-UHFFFAOYSA-N 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C403/00—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone
- C07C403/24—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone having side-chains substituted by six-membered non-aromatic rings, e.g. beta-carotene
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Preparation Of Fruits And Vegetables (AREA)
- Medicines Containing Plant Substances (AREA)
- Extraction Or Liquid Replacement (AREA)
- Compounds Of Unknown Constitution (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Saccharide Compounds (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US09/944,105 US6797303B2 (en) | 2001-09-04 | 2001-09-04 | Carotenoid extraction process |
Publications (1)
Publication Number | Publication Date |
---|---|
ZA200401476B true ZA200401476B (en) | 2004-08-30 |
Family
ID=25480804
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ZA200401476A ZA200401476B (en) | 2001-09-04 | 2004-02-24 | Carotenoid extraction process. |
Country Status (19)
Country | Link |
---|---|
US (1) | US6797303B2 (ja) |
EP (1) | EP1423020B1 (ja) |
JP (2) | JP2005501541A (ja) |
KR (1) | KR20040040449A (ja) |
CN (1) | CN100358605C (ja) |
AT (1) | ATE448698T1 (ja) |
AU (1) | AU2002329028B2 (ja) |
BR (1) | BR0212639A (ja) |
CA (1) | CA2458789A1 (ja) |
DE (1) | DE60234455D1 (ja) |
ES (1) | ES2334648T3 (ja) |
IL (1) | IL160535A0 (ja) |
MA (1) | MA26285A1 (ja) |
MX (1) | MXPA04002083A (ja) |
NZ (1) | NZ531299A (ja) |
PL (1) | PL204551B1 (ja) |
RU (1) | RU2304163C2 (ja) |
WO (1) | WO2003020053A1 (ja) |
ZA (1) | ZA200401476B (ja) |
Families Citing this family (49)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2358862B (en) * | 1999-12-21 | 2004-07-21 | Fermentron Ltd | Processes for Extracting Carotenoids from Biomass Carotenoid Sources |
ITMI20040190A1 (it) * | 2004-02-06 | 2004-05-06 | Zanichelli Ricerche Srl | Prodotti di pomodoror e processo per la loro preparazione |
CA2555486C (en) * | 2004-02-10 | 2014-12-09 | Nestec S.A. | Compositions containing cis-isomers of a carotenoid compound and process |
MY142017A (en) | 2004-03-19 | 2010-08-16 | Nestec Sa | Composition comprising all essential nutrients of a fruit or a plant material with increased stability and bioavailability and process of forming the same |
WO2006032712A1 (es) * | 2004-11-05 | 2006-03-30 | Conservas Vegetales De Extremadura, S.A. | Procedimiento de obtención del licopeno a partir de pieles y semillas de tomate |
US9579298B2 (en) * | 2004-12-02 | 2017-02-28 | Piotr Chomczynski | Antioxidant dietary supplement compositions and methods for maintaining healthy skin |
AU2006227165B2 (en) | 2005-03-18 | 2011-11-10 | Microbia, Inc. | Production of carotenoids in oleaginous yeast and fungi |
MY147363A (en) * | 2005-09-20 | 2012-11-30 | Nestec Sa | Water dispersible composition and method for preparing same |
US8318453B2 (en) | 2006-07-21 | 2012-11-27 | Xyleco, Inc. | Conversion systems for biomass |
EP1886584A1 (en) * | 2006-08-08 | 2008-02-13 | Indena S.P.A. | Stable and bioavailable compositions of isomers of lycopene for skin and hair |
US8216619B2 (en) * | 2006-08-08 | 2012-07-10 | Indena S.P.A. | Stable and bioavailable compositions of isomers of carotenoids for skin and hair |
US8691555B2 (en) | 2006-09-28 | 2014-04-08 | Dsm Ip Assests B.V. | Production of carotenoids in oleaginous yeast and fungi |
EP2063701A2 (en) * | 2006-10-18 | 2009-06-03 | Seminis Vegetable Seeds, Inc. | Carrots having increased lycopene content |
KR100845317B1 (ko) * | 2007-01-23 | 2008-07-10 | 한국식품연구원 | 마이크로이멀젼 기법에 의한 라이코펜 회수 및 수용화 |
US8119860B2 (en) | 2007-04-16 | 2012-02-21 | E. I. Du Pont De Nemours And Company | Delta-9 elongases and their use in making polyunsaturated fatty acids |
US8716533B2 (en) | 2009-05-29 | 2014-05-06 | Kalamazoo Holdings, Inc. | Methods of saponifying xanthophyll esters and isolating xanthophylls |
US8247615B2 (en) | 2010-05-14 | 2012-08-21 | Kalamazoo Holdings, Inc. | Process of converting esterified xanthophylls from Capsicum to non-esterified xanthophylls in high yields and purities |
AU2010260234B2 (en) | 2009-06-16 | 2015-02-26 | E. I. Du Pont De Nemours And Company | High eicosapentaenoic acid oils from improved optimized strains of Yarrowia lipolytica |
CN102803289B (zh) | 2009-06-16 | 2015-07-22 | 纳幕尔杜邦公司 | 用于高水平生产二十碳五烯酸的改善的优化的解脂耶氏酵母菌株 |
IT1397198B1 (it) * | 2009-12-02 | 2013-01-04 | Arterra Bioscience S R L | Composizioni cosmetiche a base di estratti idro-e liposolubili derivati da cellule di pomodoro in coltura liquida. |
IT1397687B1 (it) | 2009-12-22 | 2013-01-24 | Biosphere S P A | Metodo per l'estrazione di sostanze carotenoidi da matrici vegetali. |
EP2571942B1 (en) | 2010-05-17 | 2014-05-21 | Dynadis Biotehc (India) Private Limited | Process for isolation and purification of carotenoids |
JP5733696B2 (ja) * | 2010-08-16 | 2015-06-10 | 二村 芳弘 | 脂肪分解作用を呈するカロチノイド誘導体の製造方法 |
CN103080238B (zh) * | 2010-08-25 | 2016-01-20 | 帝斯曼知识产权资产管理有限公司 | 用于制造含玉米黄质和/或其酯的高富集萃取物的方法 |
WO2012027698A1 (en) | 2010-08-26 | 2012-03-01 | E.I. Du Pont De Nemours And Company | Mutant hpgg motif and hdash motif delta-5 desaturases and their use in making polyunsaturated fatty acids |
DK2609201T3 (en) | 2010-08-26 | 2016-06-06 | Du Pont | Mutant DELTA-9 elongases AND USE THEREOF FOR THE PRODUCTION OF polyunsaturated fatty acids |
TWI398513B (zh) * | 2010-10-08 | 2013-06-11 | Nat Univ Chung Hsing | Crystallization purification of zeaxanthin palmitate with biological activity |
US9879284B2 (en) * | 2010-10-28 | 2018-01-30 | Alfonso José GONZALEZ MARÍN | Method for obtaining natural extracts, oleoresins, condiments, colorants, flavoring substances and aromas from aromatic plant substances, alfalfa, flowers with pigments, and vegetables |
CN102040548A (zh) * | 2010-12-09 | 2011-05-04 | 天津市尖峰天然产物研究开发有限公司 | 从枸杞皮渣中提取β-胡萝卜素、玉米黄素的方法 |
WO2012162368A1 (en) | 2011-05-26 | 2012-11-29 | E. I. Du Pont De Nemours And Company | Expression of caleosin in recombinant oleaginous microorganisms to increase oil content therein |
JP2014529607A (ja) * | 2011-08-26 | 2014-11-13 | ピーティーティー グローバル ケミカル パブリック カンパニー リミテッド | 天然物質からルテイン/キサントフィルを抽出する方法、並びにこの方法により得られる高度精製ルテイン/キサントフィル |
CN103160138A (zh) * | 2011-12-08 | 2013-06-19 | 上海蓝普生物科技有限公司 | 一种枸杞花花色素的提取方法 |
CN104125987B (zh) * | 2012-02-27 | 2016-11-23 | 帝斯曼知识产权资产管理有限公司 | 制造高度富含玉米黄质和/或其酯的萃取物的方法 |
CN102850820A (zh) * | 2012-09-17 | 2013-01-02 | 塔里木大学 | 锐孔法制备黑果枸杞色素微胶囊的方法 |
RU2516637C1 (ru) * | 2012-10-22 | 2014-05-20 | Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Воронежский государственный университет инженерных технологий" (ФГБОУ ВПО "ВГУИТ") | Способ получения натурального смесевого каротиноидно-антоцианового красителя |
CN102886153B (zh) * | 2012-10-24 | 2015-12-02 | 周学义 | 枸杞及其渣粕中明目功能成分的提取方法 |
CN103305028A (zh) * | 2013-06-20 | 2013-09-18 | 邯郸市中进天然色素有限公司 | 提高辣椒红色素色价的方法 |
JP6388201B2 (ja) * | 2014-08-01 | 2018-09-12 | 二村 芳弘 | サイトケラチン増加作用を呈するカロチノイド誘導体 |
JP6380840B2 (ja) * | 2014-09-05 | 2018-08-29 | 二村 芳弘 | 脂肪前駆細胞増殖抑制作用を呈するカロチノイド誘導体 |
JP6817951B2 (ja) * | 2014-11-25 | 2021-01-20 | ライコード・リミテツド | 少量のリコペンを有する生物活性トマト組成物 |
JP6606635B2 (ja) * | 2015-05-18 | 2019-11-20 | 株式会社 A&C Beaute | サイトケラチン増加作用を呈するカロチノイド誘導体 |
CN104984710B (zh) * | 2015-07-06 | 2017-01-04 | 中国天辰工程有限公司 | 一种用于制备分子筛催化剂的卧式反应装置及制备方法 |
CN107098839A (zh) * | 2017-04-11 | 2017-08-29 | 邱绚波 | 枸杞玉米黄质的提取方法 |
CN107827797A (zh) * | 2017-10-07 | 2018-03-23 | 山东多元户户食品有限公司 | 从辣椒红色素中提取β胡萝卜素的工艺 |
WO2019122444A1 (en) | 2017-12-21 | 2019-06-27 | Dsm Ip Assets B.V. | Process for the manufacture of an extract containing lycopene |
US20220259128A1 (en) * | 2019-07-26 | 2022-08-18 | Universita' Degli Studi Di Cagliari | Isolation of chromoplastid carotenoids from fruits |
CN111603797A (zh) * | 2020-05-27 | 2020-09-01 | 云南博浩生物科技集团股份有限公司 | 一种万寿菊鲜花压榨水中沉淀物的回用方法 |
CN113509746B (zh) * | 2021-03-29 | 2022-08-09 | 艾斯普瑞(广州)食品有限公司 | 一种类胡萝卜素芝麻油扯动式浸料系统及其浸料方法 |
CN118510402A (zh) | 2021-12-20 | 2024-08-16 | 雀巢产品有限公司 | 制备浆果组合物的方法 |
Family Cites Families (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
BR8604172A (pt) * | 1986-09-01 | 1988-05-03 | Univ Estadual Paulista Julio D | Processo microbiologico para obtencao de oleos e gorduras a partir de materiais acucarados |
WO1990002493A1 (en) * | 1988-09-12 | 1990-03-22 | Counter Current Technology Pty. Limited | Tomato processing method and products |
US5837311A (en) | 1993-12-13 | 1998-11-17 | Makhteshim Chemical Works Ltd. | Industrial processing of tomatoes and product thereof |
HUT75371A (en) * | 1995-10-09 | 1997-05-28 | Motiv Magyar Nemet Kereskedelm | Natural carotene-concentrate of vegetable material and process for producing of that |
US5648564A (en) * | 1995-12-21 | 1997-07-15 | Kemin Industries, Inc. | Process for the formation, isolation and purification of comestible xanthophyll crystals from plants |
US5951875A (en) * | 1996-12-20 | 1999-09-14 | Eastman Chemical Company | Adsorptive bubble separation methods and systems for dewatering suspensions of microalgae and extracting components therefrom |
JP3606702B2 (ja) * | 1997-04-08 | 2005-01-05 | カゴメ株式会社 | 低粘度で高リコピン含量の食品材料の製造方法 |
US5869749A (en) * | 1997-04-30 | 1999-02-09 | Honeywell Inc. | Micromachined integrated opto-flow gas/liquid sensor |
US5876782A (en) | 1997-05-14 | 1999-03-02 | Kemin Industries, Inc. | Method for the conversion of xanthophylls in plant material |
US6221417B1 (en) * | 1997-05-14 | 2001-04-24 | Kemin Industries, Inc. | Conversion of xanthophylls in plant material for use as a food colorant |
JPH10324816A (ja) * | 1997-05-26 | 1998-12-08 | Nippon Derumonte Kk | トマト色素およびその製造方法 |
US5871574A (en) * | 1997-07-01 | 1999-02-16 | Nippon Del Monte Corporation | Method for collecting tomato pigment and its application |
JPH11169134A (ja) * | 1997-12-17 | 1999-06-29 | Nippon Del Monte Corp | タンパク質含有飲食品の着色方法 |
US6191293B1 (en) * | 1998-04-20 | 2001-02-20 | Inexa, Industria Extractora C.A. | Trans-xanthophyll ester concentrates of enhanced purity and methods of making same |
KR100343781B1 (ko) * | 1999-12-13 | 2002-07-25 | 주식회사 제은 | 가오리류로부터 콘드로이틴황산의 추출 및 정제방법 |
CN1137639C (zh) * | 2000-07-27 | 2004-02-11 | 北京顺鑫牵手有限责任公司 | 以胡萝卜为主要原料的系列果蔬汁及其制造方法 |
JP2002193850A (ja) * | 2000-12-25 | 2002-07-10 | Nippon Del Monte Corp | 高純度リコペンの製造方法及び用途 |
-
2001
- 2001-09-04 US US09/944,105 patent/US6797303B2/en not_active Expired - Lifetime
-
2002
- 2002-09-04 EP EP02765314A patent/EP1423020B1/en not_active Expired - Lifetime
- 2002-09-04 BR BR0212639-7A patent/BR0212639A/pt not_active IP Right Cessation
- 2002-09-04 IL IL16053502A patent/IL160535A0/xx unknown
- 2002-09-04 JP JP2003524375A patent/JP2005501541A/ja active Pending
- 2002-09-04 AT AT02765314T patent/ATE448698T1/de not_active IP Right Cessation
- 2002-09-04 ES ES02765314T patent/ES2334648T3/es not_active Expired - Lifetime
- 2002-09-04 NZ NZ531299A patent/NZ531299A/en unknown
- 2002-09-04 RU RU2004106151/13A patent/RU2304163C2/ru not_active IP Right Cessation
- 2002-09-04 CA CA002458789A patent/CA2458789A1/en not_active Abandoned
- 2002-09-04 AU AU2002329028A patent/AU2002329028B2/en not_active Ceased
- 2002-09-04 KR KR10-2004-7003108A patent/KR20040040449A/ko active IP Right Grant
- 2002-09-04 PL PL367871A patent/PL204551B1/pl not_active IP Right Cessation
- 2002-09-04 CN CNB028217934A patent/CN100358605C/zh not_active Expired - Fee Related
- 2002-09-04 DE DE60234455T patent/DE60234455D1/de not_active Expired - Lifetime
- 2002-09-04 WO PCT/IL2002/000728 patent/WO2003020053A1/en active IP Right Grant
- 2002-09-04 MX MXPA04002083A patent/MXPA04002083A/es not_active Application Discontinuation
-
2004
- 2004-02-24 ZA ZA200401476A patent/ZA200401476B/en unknown
- 2004-03-02 MA MA27556A patent/MA26285A1/fr unknown
-
2009
- 2009-08-28 JP JP2009197650A patent/JP5537869B2/ja not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
EP1423020B1 (en) | 2009-11-18 |
PL367871A1 (en) | 2005-03-07 |
JP2005501541A (ja) | 2005-01-20 |
RU2004106151A (ru) | 2005-07-10 |
DE60234455D1 (de) | 2009-12-31 |
EP1423020A1 (en) | 2004-06-02 |
WO2003020053A9 (en) | 2004-04-15 |
PL204551B1 (pl) | 2010-01-29 |
IL160535A0 (en) | 2004-07-25 |
AU2002329028B2 (en) | 2007-07-26 |
CA2458789A1 (en) | 2003-03-13 |
ES2334648T3 (es) | 2010-03-15 |
NZ531299A (en) | 2004-08-27 |
US6797303B2 (en) | 2004-09-28 |
WO2003020053A1 (en) | 2003-03-13 |
CN1578628A (zh) | 2005-02-09 |
MXPA04002083A (es) | 2004-06-07 |
JP5537869B2 (ja) | 2014-07-02 |
RU2304163C2 (ru) | 2007-08-10 |
MA26285A1 (fr) | 2004-09-01 |
US20030044499A1 (en) | 2003-03-06 |
JP2010013457A (ja) | 2010-01-21 |
ATE448698T1 (de) | 2009-12-15 |
CN100358605C (zh) | 2008-01-02 |
BR0212639A (pt) | 2004-08-24 |
KR20040040449A (ko) | 2004-05-12 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
US6797303B2 (en) | Carotenoid extraction process | |
AU2002329028A1 (en) | Carotenoid extraction process | |
DK1534673T3 (en) | Improved method of making xanthophyll crystals | |
US6504067B1 (en) | Process to obtain xanthophyll concentrates of high purity | |
US7622599B2 (en) | Isolation and purification of carotenoids from marigold flowers | |
JP5795572B2 (ja) | 種々の植物からカロテノイド結晶を分離する方法 | |
US6737552B1 (en) | Method for extracting lutein from green plant materials | |
EP1201762B1 (en) | Process for producing lycopen | |
US8481769B2 (en) | Isolation and purification of cartenoids from marigold flowers | |
US7875751B2 (en) | Method for the purification of carotenoids from plant extracts and the products so obtained | |
IL160535A (en) | Carotonoid extraction from plant material | |
EP2196207B1 (en) | Method for the purification of carotenoids from plant extracts and the products so obtained |