WO2009048007A1 - 微粒子分散ポリオールの製造方法及びポリウレタン樹脂の製造方法 - Google Patents

微粒子分散ポリオールの製造方法及びポリウレタン樹脂の製造方法 Download PDF

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Publication number
WO2009048007A1
WO2009048007A1 PCT/JP2008/067807 JP2008067807W WO2009048007A1 WO 2009048007 A1 WO2009048007 A1 WO 2009048007A1 JP 2008067807 W JP2008067807 W JP 2008067807W WO 2009048007 A1 WO2009048007 A1 WO 2009048007A1
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WO
WIPO (PCT)
Prior art keywords
fine particle
dispersed polyol
producing
polyol
dispersed
Prior art date
Application number
PCT/JP2008/067807
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English (en)
French (fr)
Inventor
Shigekuni Nakada
Takayuki Tsuji
Yukiya Kobayashi
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Sanyo Chemical Industries, Ltd.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sanyo Chemical Industries, Ltd. filed Critical Sanyo Chemical Industries, Ltd.
Priority to KR1020107008127A priority Critical patent/KR101228258B1/ko
Priority to EP08837123.2A priority patent/EP2199309B1/en
Priority to CN200880105833A priority patent/CN101796078A/zh
Priority to KR1020127030251A priority patent/KR101320250B1/ko
Priority to US12/670,585 priority patent/US9062148B2/en
Publication of WO2009048007A1 publication Critical patent/WO2009048007A1/ja

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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/44—Polymerisation in the presence of compounding ingredients, e.g. plasticisers, dyestuffs, fillers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/04—Polymerisation in solution
    • C08F2/10—Aqueous solvent
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/12—Polymerisation in non-solvents
    • C08F2/16—Aqueous medium
    • C08F2/22—Emulsion polymerisation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F283/00—Macromolecular compounds obtained by polymerising monomers on to polymers provided for in subclass C08G
    • C08F283/06—Macromolecular compounds obtained by polymerising monomers on to polymers provided for in subclass C08G on to polyethers, polyoxymethylenes or polyacetals
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/4009—Two or more macromolecular compounds not provided for in one single group of groups C08G18/42 - C08G18/64
    • C08G18/4072—Mixtures of compounds of group C08G18/63 with other macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/63—Block or graft polymers obtained by polymerising compounds having carbon-to-carbon double bonds on to polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/63—Block or graft polymers obtained by polymerising compounds having carbon-to-carbon double bonds on to polymers
    • C08G18/632—Block or graft polymers obtained by polymerising compounds having carbon-to-carbon double bonds on to polymers onto polyethers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0008—Foam properties flexible
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0041—Foam properties having specified density
    • C08G2110/005—< 50kg/m3
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0083—Foam properties prepared using water as the sole blowing agent

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Graft Or Block Polymers (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Polymerisation Methods In General (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)

Abstract

　下記の工程（１）および工程（ｎ－１）を含む、微粒子分散ポリオール（Ｉ）の製造方法であって、微粒子（Ｐ１）の体積平均粒子径（Ｒ１）が０．０１～１．０μｍであり、工程（１）におけるエチレン性不飽和モノマー（ｂ）の濃度（重量％）が７～４０であることからなる微粒子分散ポリオール（Ｉ）の製造方法。 工程（１）：ポリオール（ａ）中で、（Ｐ１）及びラジカル重合開始剤（ｃ）の存在下、（ｂ）を重合させて微粒子分散ポリオール中間体（Ｂ２）を得る工程 工程（ｎ－１）：微粒子分散ポリオール中間体（Ｂ（ｎ－１））中で、（ｃ）の存在下、（ｂ）を重合させて微粒子分散ポリオール中間体（Ｂｎ）、または微粒子分散ポリオール（Ｉ）を得る工程（ｎは３～７の整数を表す。）。 　ポリオール中に分散している重合体微粒子の粒子径が小さく、ポリウレタン樹脂に用いた場合の樹脂物性に優れた微粒子分散ポリオールの製造方法を提供できる。
PCT/JP2008/067807 2007-10-10 2008-10-01 微粒子分散ポリオールの製造方法及びポリウレタン樹脂の製造方法 WO2009048007A1 (ja)

Priority Applications (5)

Application Number Priority Date Filing Date Title
KR1020107008127A KR101228258B1 (ko) 2007-10-10 2008-10-01 미립자 분산 폴리올의 제조 방법 및 폴리우레탄 수지의 제조 방법
EP08837123.2A EP2199309B1 (en) 2007-10-10 2008-10-01 Method for producing fine particle-dispersed polyol and method for producing polyurethane resin
CN200880105833A CN101796078A (zh) 2007-10-10 2008-10-01 微粒分散多元醇的制造方法以及聚氨酯树脂的制造方法
KR1020127030251A KR101320250B1 (ko) 2007-10-10 2008-10-01 미립자 분산 폴리올의 제조 방법 및 폴리우레탄 수지의 제조 방법
US12/670,585 US9062148B2 (en) 2007-10-10 2008-10-01 Method for producing fine-particle-dispersed polyol, and method for producing polyurethane resin

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007264991 2007-10-10
JP2007-264991 2007-10-10

Publications (1)

Publication Number Publication Date
WO2009048007A1 true WO2009048007A1 (ja) 2009-04-16

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PCT/JP2008/067807 WO2009048007A1 (ja) 2007-10-10 2008-10-01 微粒子分散ポリオールの製造方法及びポリウレタン樹脂の製造方法

Country Status (6)

Country Link
US (1) US9062148B2 (ja)
EP (1) EP2199309B1 (ja)
JP (2) JP4851503B2 (ja)
KR (2) KR101228258B1 (ja)
CN (2) CN101796078A (ja)
WO (1) WO2009048007A1 (ja)

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CN103068867A (zh) * 2010-08-03 2013-04-24 国际壳牌研究有限公司 用于制备聚合物多元醇的方法
CN103068866A (zh) * 2010-08-03 2013-04-24 国际壳牌研究有限公司 制备聚合物多元醇的方法
JP5846197B2 (ja) * 2011-02-25 2016-01-20 旭硝子株式会社 高濃度ポリマーポリオールおよびその製造方法

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CN102276973B (zh) 2005-07-07 2013-06-05 三洋化成工业株式会社 聚合物多元醇的制造方法及聚氨酯树脂的制造方法
EP2194097B1 (en) * 2007-09-28 2013-07-03 Sanyo Chemical Industries, Ltd. Polymer polyol, method for producing the same, and method for producing polyurethane resin
CN104039858A (zh) * 2011-08-17 2014-09-10 巴斯夫欧洲公司 制备硬质聚氨酯泡沫的方法
CN103007900B (zh) * 2012-11-27 2015-04-22 安徽皖东化工有限公司 一种硅藻土改性的吸附树脂的制备方法
CN103254367B (zh) * 2013-05-24 2015-07-15 淄博德信联邦化学工业有限公司 聚合物多元醇的制备方法
WO2014196607A1 (ja) * 2013-06-07 2014-12-11 株式会社カネカ 硬化性樹脂組成物、それを用いてなる構造接着剤、コーティング材又は繊維強化複合材料、それを発泡してなる発泡体、それを硬化してなる積層体、及びそれらの硬化物
KR101638794B1 (ko) * 2014-02-24 2016-07-12 주식회사 노루홀딩스 천연물질 유도체를 함유한 바이오매스 폴리우레탄 수지 및 이의 제조방법
US9505881B1 (en) * 2015-06-10 2016-11-29 Covestro Llc Polymer polyol compositions, a process for preparing these novel polymer polyol compositions, flexible foams prepared from these novel polymer polyols and a process for the preparation of these flexible foams
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JP6936810B2 (ja) * 2016-03-31 2021-09-22 ダウ グローバル テクノロジーズ エルエルシー 単分散分散ポリマー粒子を有するポリマーポリオールを作製するプロセス
KR101903857B1 (ko) * 2016-11-18 2018-11-22 전정희 주형 ppdi계 폴리우레탄 나노클레이 탄성체 제조방법 및 이에 의해 제조된 주형 ppdi계 폴리우레탄 나노클레이 탄성체
KR101998849B1 (ko) * 2018-03-02 2019-07-11 금호석유화학 주식회사 저점도를 갖는 고고형분 폴리머 폴리올의 제조방법
TWI792463B (zh) * 2020-10-16 2023-02-11 得裕盛業股份有限公司 減震材料之製造方法及含有該減震材料之高分子加工方法
CN113388083B (zh) * 2021-05-24 2022-07-12 丽水学院 一种共价连接的聚氨酯/氧化铈复合材料及其制备方法

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