WO1999021955A1 - Verfahren zur herstellung duftverstärkter wasch- oder reinigungsmittel - Google Patents
Verfahren zur herstellung duftverstärkter wasch- oder reinigungsmittel Download PDFInfo
- Publication number
- WO1999021955A1 WO1999021955A1 PCT/EP1998/006513 EP9806513W WO9921955A1 WO 1999021955 A1 WO1999021955 A1 WO 1999021955A1 EP 9806513 W EP9806513 W EP 9806513W WO 9921955 A1 WO9921955 A1 WO 9921955A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- premix
- weight
- perfume
- binder
- fragrance
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
Definitions
- the essentially water-free premix which is pressed agglomerated preferably has no dust-like components and in particular no particles with particle sizes below 200 ⁇ m.
- those particle size distributions are preferred which have at least 90% by weight of particles with a diameter of at least 400 ⁇ m.
- the washing or cleaning agents or components produced by press agglomeration consist of at least 70% by weight, advantageously at least 80% by weight and, with particular preference, up to 100% by weight spherical or almost spherical (pearl-shaped) particles with a particle size distribution which has at least 60% by weight of particles between 0.8 and 2.0 mm.
- the premix can contain a raw material or a compound which functions as a binding and disintegration aid.
- these binding and disintegration aids serve as lubricants and adhesives which adhere the solid components of the premix to one another and facilitate the passage of the premix through the pressure zone of the press agglomeration apparatus.
- water-soluble binders they also facilitate the redissolution of the press agglomerates, since they act as disintegrants in aqueous liquors.
- the particularly preferred polyethylene glycols include those with relative molecular weights between 2000 and 12000, advantageously around 4000, polyethylene glycols with relative molecular weights below 3500 and above 5000, in particular in combination with polyethylene glycols with a relative molecular weight of around 4000, and such combinations advantageously to more than 50% by weight, based on the total amount of polyethylene glycols, have polyethylene glycols with a relative molecular weight between 3500 and 5000.
- polyethylene glycols which are in the liquid state at room temperature and a pressure of 1 bar can also be used as binders;
- polyethylene glycol with a relative molecular mass of 200, 400 and 600 can also be used as binders;
- these per se liquid polyethylene glycols should only be used in a mixture with at least one further binder, this mixture again having to meet the requirements according to the invention, that is to say having a melting point or softening point of at least above 45 ° C.
- the more volatile fragrances include, in particular, the lower-boiling fragrances of natural or synthetic origin, which can be used alone or in mixtures.
- Examples of more volatile fragrances are alkyisothiocyanates (alkyl mustards), butanedione, limonene, linalool, Linaylacetate and propionate, menthol, Menthone, methyl-n-heptenone, phellandrene, phenylacetaldehyde, terpinylacetate, citral, citronellal.
- the group of polyhydroxy fatty acid amides also includes compounds of the formula (II)
- Suitable organic builder substances are dextrins, for example oligomers or polymers of carbohydrates, which can be obtained by partial hydrolysis of starches.
- the hydrolysis can be carried out by customary processes, for example acid-catalyzed or enzyme-catalyzed. They are preferably hydrolysis products with average molecular weights in the range from 400 to 500,000.
- DE dextrose equivalent
- polyacetals which can be obtained by reacting dialdehydes with polyolcarboxylic acids which have 5 to 7 carbon atoms and at least 3 hydroxyl groups, for example as described in European patent application EP-A-0 280 223.
- Preferred polyacetals are obtained from dialdehydes such as glyoxal, glutaraldehyde, terephthalaldehyde and mixtures thereof and from polyol carboxylic acids such as gluconic acid and / or glucoheptonic acid.
- the enzymes can be adsorbed on carriers and / or embedded in coating substances in order to protect them against premature decomposition.
- the proportion of the enzymes, enzyme mixtures or enzyme granules can be, for example, about 0.1 to 5% by weight, preferably 0.1 to about 2% by weight.
- Table 1 Composition of the spray-dried granules [% by weight]:
- an extrudate E3 was also produced which contained part of the perfume and was also sprayed with the rest of the perfume. This agent was compared with a comparative sex trudate V3, in which the total amount of the perfume was applied by spraying.
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
- Fats And Perfumes (AREA)
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL98340036A PL188261B1 (pl) | 1997-10-23 | 1998-10-14 | Sposób wytwarzania środka piorącego o wzmocnionymzapachu |
| AT98955451T ATE246727T1 (de) | 1997-10-23 | 1998-10-14 | Verfahren zur herstellung duftverstärkter wasch- oder reinigungsmittel |
| DE59809226T DE59809226D1 (de) | 1997-10-23 | 1998-10-14 | Verfahren zur herstellung duftverstärkter wasch- oder reinigungsmittel |
| EP98955451A EP1025198B1 (de) | 1997-10-23 | 1998-10-14 | Verfahren zur herstellung duftverstärkter wasch- oder reinigungsmittel |
| JP2000518048A JP2001521060A (ja) | 1997-10-23 | 1998-10-14 | 芳香性増強洗剤および洗浄剤の製法 |
| US09/529,864 US6228833B1 (en) | 1997-10-23 | 1998-10-14 | Method for producing scent intensifying washing and cleaning detergents |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19746781.4 | 1997-10-23 | ||
| DE19746781A DE19746781A1 (de) | 1997-10-23 | 1997-10-23 | Verfahren zur Herstellung duftverstärkter Wasch- oder Reinigungsmittel |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| WO1999021955A1 true WO1999021955A1 (de) | 1999-05-06 |
Family
ID=7846357
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PCT/EP1998/006513 Ceased WO1999021955A1 (de) | 1997-10-23 | 1998-10-14 | Verfahren zur herstellung duftverstärkter wasch- oder reinigungsmittel |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US6228833B1 (https=) |
| EP (1) | EP1025198B1 (https=) |
| JP (1) | JP2001521060A (https=) |
| CN (1) | CN1276829A (https=) |
| AT (1) | ATE246727T1 (https=) |
| DE (2) | DE19746781A1 (https=) |
| ES (1) | ES2205570T3 (https=) |
| PL (1) | PL188261B1 (https=) |
| WO (1) | WO1999021955A1 (https=) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2000023556A1 (de) * | 1998-10-17 | 2000-04-27 | Henkel Kommanditgesellschaft Auf Aktien | Verfahren zur herstellung extrudierter formkörper |
| EP1657298A1 (de) * | 2004-11-12 | 2006-05-17 | Cognis IP Management GmbH | Feste Zubereitungen |
| WO2008025678A1 (de) * | 2006-08-28 | 2008-03-06 | Henkel Ag & Co. Kgaa | Schmelzgranulate für wasch- und reinigungsmittel |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1149144A1 (en) * | 1999-02-05 | 2001-10-31 | Unilever Plc | Dish washing process and compositions relating thereto |
| US6786223B2 (en) * | 2001-10-11 | 2004-09-07 | S. C. Johnson & Son, Inc. | Hard surface cleaners which provide improved fragrance retention properties to hard surfaces |
| GB0130498D0 (en) * | 2001-12-20 | 2002-02-06 | Unilever Plc | Process for production of detergent tablets |
| GB0201300D0 (en) * | 2002-01-21 | 2002-03-06 | Unilever Plc | Detergent composition in tablet form |
| US7057008B2 (en) * | 2002-05-14 | 2006-06-06 | E.I. Du Pont De Nemours And Company | Packaging and containers made of water-soluble polyamides and processes for their manufacture |
| US6689342B1 (en) * | 2002-07-29 | 2004-02-10 | Warner-Lambert Company | Oral care compositions comprising tropolone compounds and essential oils and methods of using the same |
| WO2004106479A1 (en) | 2003-05-28 | 2004-12-09 | Kao Corporation | Process for releasing fragrance |
| DE102005062008B3 (de) * | 2005-12-22 | 2007-08-30 | Henkel Kgaa | Geruchsreduktion hypochlorithaltiger Mittel |
| BRPI0918755A2 (pt) * | 2008-09-10 | 2015-12-08 | Danisco Us Inc | composição de alvejamento têxtil enzimática e métodos de uso da mesma |
| CN104479912A (zh) * | 2014-12-13 | 2015-04-01 | 张慧娜 | 一种柠檬油复合清洗剂及其制备方法 |
| CN106422978B (zh) * | 2016-12-20 | 2019-03-05 | 上海试四赫维化工有限公司 | 水溶性引发剂的造粒方法 |
| EP3642319B1 (en) * | 2017-06-20 | 2020-12-30 | Unilever N.V. | Particulate detergent composition comprising perfume |
| CN108531298B (zh) * | 2018-04-10 | 2020-06-23 | 上海应用技术大学 | 一种含有金佛手精油微胶囊的洗衣粉及其制备方法 |
| CN111286414B (zh) * | 2019-11-28 | 2021-04-27 | 纳爱斯浙江科技有限公司 | 一种衣物留香珠及其制备方法 |
| WO2022104631A1 (en) * | 2020-11-19 | 2022-05-27 | The Procter & Gamble Company | Method of making detergent compositions comprising perfume |
| CN115073287B (zh) * | 2021-03-11 | 2024-06-25 | 万华化学(四川)有限公司 | 一种高品质乙酸芳樟酯及其制备方法 |
| CN113712421B (zh) * | 2021-09-23 | 2022-10-21 | 涟源市宝福香业有限公司 | 一种中药檀香的加工工艺 |
| WO2023142099A1 (en) * | 2022-01-30 | 2023-08-03 | The Procter & Gamble Company | Method of making perfume-containing particles |
| CN115108751B (zh) | 2022-07-14 | 2023-03-21 | 武汉工程大学 | 一种预拌流态固化土用分散剂及其制备方法和应用 |
| CN115923159A (zh) * | 2022-11-01 | 2023-04-07 | 重庆工程学院 | 一种夹芯板生产用压合装置 |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1991002047A1 (de) * | 1989-08-09 | 1991-02-21 | Henkel Kommanditgesellschaft Auf Aktien | Herstellung verdichteter granulate für waschmittel |
| WO1991013678A1 (de) * | 1990-03-09 | 1991-09-19 | Henkel Kommanditgesellschaft Auf Aktien | Verfahren zum herstellen von granulaten eines wasch- oder reinigungsmittels |
| EP0537584A1 (de) * | 1991-10-12 | 1993-04-21 | Henkel KGaA | Duftstoffe enthaltende Tablette |
| WO1994009111A1 (de) * | 1992-10-22 | 1994-04-28 | Henkel Kommanditgesellschaft Auf Aktien | Verfahren zur herstellung wasch- oder reinigungsaktiver extrudate |
| WO1995011291A1 (de) * | 1993-10-21 | 1995-04-27 | Henkel Kommanditgesellschaft Auf Aktien | Verfahren zur herstellung wasch- oder reinigungsaktiver extrudate mit verbessertem redispergiervermögen |
| WO1996029389A1 (de) * | 1995-03-17 | 1996-09-26 | Henkel Kommanditgesellschaft Auf Aktien | Verfahren zur herstellung eines pulverförmigen wasch- oder reinigungsmittels |
| WO1997020906A1 (de) * | 1995-12-07 | 1997-06-12 | Henkel Kommanditgesellschaft Auf Aktien | Verfahren zur herstellung von wasch- oder reinigungsaktiven extrudaten |
| WO1997047720A2 (en) * | 1996-06-11 | 1997-12-18 | The Procter & Gamble Company | Process for producing a particulate laundry additive for perfume delivery having improved physical properties |
| DE19638599A1 (de) * | 1996-09-20 | 1998-03-26 | Henkel Kgaa | Verfahren zur Herstellung eines teilchenförmigen Wasch- oder Reinigungsmittels |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5198145A (en) * | 1990-11-08 | 1993-03-30 | Fmc Corporation | Dry detergent compositions |
| US5691294A (en) * | 1993-03-30 | 1997-11-25 | The Procter & Gamble Company | Flow aids for detergent powders comprising sodium aluminosilicate and hydrophobic silica |
-
1997
- 1997-10-23 DE DE19746781A patent/DE19746781A1/de not_active Withdrawn
-
1998
- 1998-10-14 WO PCT/EP1998/006513 patent/WO1999021955A1/de not_active Ceased
- 1998-10-14 JP JP2000518048A patent/JP2001521060A/ja active Pending
- 1998-10-14 AT AT98955451T patent/ATE246727T1/de not_active IP Right Cessation
- 1998-10-14 DE DE59809226T patent/DE59809226D1/de not_active Revoked
- 1998-10-14 EP EP98955451A patent/EP1025198B1/de not_active Revoked
- 1998-10-14 PL PL98340036A patent/PL188261B1/pl not_active IP Right Cessation
- 1998-10-14 ES ES98955451T patent/ES2205570T3/es not_active Expired - Lifetime
- 1998-10-14 US US09/529,864 patent/US6228833B1/en not_active Expired - Fee Related
- 1998-10-14 CN CN98810454A patent/CN1276829A/zh active Pending
Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1991002047A1 (de) * | 1989-08-09 | 1991-02-21 | Henkel Kommanditgesellschaft Auf Aktien | Herstellung verdichteter granulate für waschmittel |
| WO1991013678A1 (de) * | 1990-03-09 | 1991-09-19 | Henkel Kommanditgesellschaft Auf Aktien | Verfahren zum herstellen von granulaten eines wasch- oder reinigungsmittels |
| EP0537584A1 (de) * | 1991-10-12 | 1993-04-21 | Henkel KGaA | Duftstoffe enthaltende Tablette |
| WO1994009111A1 (de) * | 1992-10-22 | 1994-04-28 | Henkel Kommanditgesellschaft Auf Aktien | Verfahren zur herstellung wasch- oder reinigungsaktiver extrudate |
| WO1995011291A1 (de) * | 1993-10-21 | 1995-04-27 | Henkel Kommanditgesellschaft Auf Aktien | Verfahren zur herstellung wasch- oder reinigungsaktiver extrudate mit verbessertem redispergiervermögen |
| WO1996029389A1 (de) * | 1995-03-17 | 1996-09-26 | Henkel Kommanditgesellschaft Auf Aktien | Verfahren zur herstellung eines pulverförmigen wasch- oder reinigungsmittels |
| WO1997020906A1 (de) * | 1995-12-07 | 1997-06-12 | Henkel Kommanditgesellschaft Auf Aktien | Verfahren zur herstellung von wasch- oder reinigungsaktiven extrudaten |
| WO1997047720A2 (en) * | 1996-06-11 | 1997-12-18 | The Procter & Gamble Company | Process for producing a particulate laundry additive for perfume delivery having improved physical properties |
| DE19638599A1 (de) * | 1996-09-20 | 1998-03-26 | Henkel Kgaa | Verfahren zur Herstellung eines teilchenförmigen Wasch- oder Reinigungsmittels |
| WO1998012299A1 (de) * | 1996-09-20 | 1998-03-26 | Henkel Kommanditgesellschaft Auf Aktien | Verfahren zur herstellung eines teilchenförmigen wasch- oder reinigungsmittels |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2000023556A1 (de) * | 1998-10-17 | 2000-04-27 | Henkel Kommanditgesellschaft Auf Aktien | Verfahren zur herstellung extrudierter formkörper |
| EP1657298A1 (de) * | 2004-11-12 | 2006-05-17 | Cognis IP Management GmbH | Feste Zubereitungen |
| WO2008025678A1 (de) * | 2006-08-28 | 2008-03-06 | Henkel Ag & Co. Kgaa | Schmelzgranulate für wasch- und reinigungsmittel |
Also Published As
| Publication number | Publication date |
|---|---|
| PL188261B1 (pl) | 2005-01-31 |
| JP2001521060A (ja) | 2001-11-06 |
| ES2205570T3 (es) | 2004-05-01 |
| PL340036A1 (en) | 2001-01-15 |
| EP1025198A1 (de) | 2000-08-09 |
| US6228833B1 (en) | 2001-05-08 |
| DE19746781A1 (de) | 1999-04-29 |
| ATE246727T1 (de) | 2003-08-15 |
| DE59809226D1 (de) | 2003-09-11 |
| CN1276829A (zh) | 2000-12-13 |
| EP1025198B1 (de) | 2003-08-06 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| EP1025198B1 (de) | Verfahren zur herstellung duftverstärkter wasch- oder reinigungsmittel | |
| EP0931137B1 (de) | Verfahren zur herstellung eines teilchenförmigen wasch- oder reinigungsmittels | |
| EP1235897B1 (de) | Waschmitteltabletten | |
| EP1025195A1 (de) | Verfahren zur herstellung von duftperlen | |
| EP0863200A2 (de) | Waschmittelformkörper | |
| DE19956803A1 (de) | Tensidgranulate mit verbesserter Auflösegeschwindigkeit | |
| EP1253193A2 (de) | Feste Tensidzusammensetzungen, deren Herstellung und Verwendung | |
| EP1081219B1 (de) | Detergentien in fester Form | |
| DE19735783A1 (de) | Hochdosierte Duftstoff-Formkörper | |
| EP1358310B1 (de) | Wasch- und reinigungsmittel umfassend feine mikropartikel mit reinigungsmittelbestandteilen | |
| EP1106678B1 (de) | Niotensidgranulate durch Prillen | |
| EP1012221B1 (de) | Verfahren zur herstellung teilchenförmiger wasch- oder reinigungsmittel | |
| DE69521791T2 (de) | Waschmittelzusammensetzung | |
| DE19940262A1 (de) | Waschmittelzusatzstoffe in fester Form | |
| WO2001016280A2 (de) | Verfahren zur herstellung von duftperlen | |
| DE19917692A1 (de) | Duftsäckchen | |
| WO2000037595A1 (de) | Kompaktat mit silicatischem builder | |
| WO2000039261A1 (de) | Niederdosierter, löslicher builder | |
| WO2000000581A1 (de) | Verfahren zur herstellung von wasch- und reinigungsmittelformkörpern | |
| DE19847569A1 (de) | Phosphonathaltige Granulate | |
| WO1998023722A1 (de) | Verfahren zum herstellen von festen, geformten waschmittelformulierungen | |
| DE10108573A1 (de) | Feste Waschmittelzusatzstoffe, deren Herstellung und Verwendung | |
| DE102004053385A1 (de) | Kugelförmige Agglomerate |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| WWE | Wipo information: entry into national phase |
Ref document number: 98810454.7 Country of ref document: CN |
|
| AK | Designated states |
Kind code of ref document: A1 Designated state(s): CN CZ HU JP PL RU SK US |
|
| AL | Designated countries for regional patents |
Kind code of ref document: A1 Designated state(s): AT BE CH CY DE DK ES FI FR GB GR IE IT LU MC NL PT SE |
|
| DFPE | Request for preliminary examination filed prior to expiration of 19th month from priority date (pct application filed before 20040101) | ||
| 121 | Ep: the epo has been informed by wipo that ep was designated in this application | ||
| WWE | Wipo information: entry into national phase |
Ref document number: 1998955451 Country of ref document: EP |
|
| WWE | Wipo information: entry into national phase |
Ref document number: 09529864 Country of ref document: US |
|
| WWP | Wipo information: published in national office |
Ref document number: 1998955451 Country of ref document: EP |
|
| WWG | Wipo information: grant in national office |
Ref document number: 1998955451 Country of ref document: EP |
|
| WWW | Wipo information: withdrawn in national office |
Ref document number: 1998955451 Country of ref document: EP |