WO1999021955A1 - Verfahren zur herstellung duftverstärkter wasch- oder reinigungsmittel - Google Patents

Verfahren zur herstellung duftverstärkter wasch- oder reinigungsmittel Download PDF

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Publication number
WO1999021955A1
WO1999021955A1 PCT/EP1998/006513 EP9806513W WO9921955A1 WO 1999021955 A1 WO1999021955 A1 WO 1999021955A1 EP 9806513 W EP9806513 W EP 9806513W WO 9921955 A1 WO9921955 A1 WO 9921955A1
Authority
WO
WIPO (PCT)
Prior art keywords
premix
weight
perfume
binder
fragrance
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/EP1998/006513
Other languages
German (de)
English (en)
French (fr)
Inventor
Kathleen Paatz
Wolfgang Lahn
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henkel AG and Co KGaA
Original Assignee
Henkel AG and Co KGaA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=7846357&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=WO1999021955(A1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Henkel AG and Co KGaA filed Critical Henkel AG and Co KGaA
Priority to PL98340036A priority Critical patent/PL188261B1/pl
Priority to AT98955451T priority patent/ATE246727T1/de
Priority to DE59809226T priority patent/DE59809226D1/de
Priority to EP98955451A priority patent/EP1025198B1/de
Priority to JP2000518048A priority patent/JP2001521060A/ja
Priority to US09/529,864 priority patent/US6228833B1/en
Publication of WO1999021955A1 publication Critical patent/WO1999021955A1/de
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/50Perfumes
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00Special methods for preparing compositions containing mixtures of detergents
    • C11D11/0082Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06Powder; Flakes; Free-flowing mixtures; Sheets

Definitions

  • the essentially water-free premix which is pressed agglomerated preferably has no dust-like components and in particular no particles with particle sizes below 200 ⁇ m.
  • those particle size distributions are preferred which have at least 90% by weight of particles with a diameter of at least 400 ⁇ m.
  • the washing or cleaning agents or components produced by press agglomeration consist of at least 70% by weight, advantageously at least 80% by weight and, with particular preference, up to 100% by weight spherical or almost spherical (pearl-shaped) particles with a particle size distribution which has at least 60% by weight of particles between 0.8 and 2.0 mm.
  • the premix can contain a raw material or a compound which functions as a binding and disintegration aid.
  • these binding and disintegration aids serve as lubricants and adhesives which adhere the solid components of the premix to one another and facilitate the passage of the premix through the pressure zone of the press agglomeration apparatus.
  • water-soluble binders they also facilitate the redissolution of the press agglomerates, since they act as disintegrants in aqueous liquors.
  • the particularly preferred polyethylene glycols include those with relative molecular weights between 2000 and 12000, advantageously around 4000, polyethylene glycols with relative molecular weights below 3500 and above 5000, in particular in combination with polyethylene glycols with a relative molecular weight of around 4000, and such combinations advantageously to more than 50% by weight, based on the total amount of polyethylene glycols, have polyethylene glycols with a relative molecular weight between 3500 and 5000.
  • polyethylene glycols which are in the liquid state at room temperature and a pressure of 1 bar can also be used as binders;
  • polyethylene glycol with a relative molecular mass of 200, 400 and 600 can also be used as binders;
  • these per se liquid polyethylene glycols should only be used in a mixture with at least one further binder, this mixture again having to meet the requirements according to the invention, that is to say having a melting point or softening point of at least above 45 ° C.
  • the more volatile fragrances include, in particular, the lower-boiling fragrances of natural or synthetic origin, which can be used alone or in mixtures.
  • Examples of more volatile fragrances are alkyisothiocyanates (alkyl mustards), butanedione, limonene, linalool, Linaylacetate and propionate, menthol, Menthone, methyl-n-heptenone, phellandrene, phenylacetaldehyde, terpinylacetate, citral, citronellal.
  • the group of polyhydroxy fatty acid amides also includes compounds of the formula (II)
  • Suitable organic builder substances are dextrins, for example oligomers or polymers of carbohydrates, which can be obtained by partial hydrolysis of starches.
  • the hydrolysis can be carried out by customary processes, for example acid-catalyzed or enzyme-catalyzed. They are preferably hydrolysis products with average molecular weights in the range from 400 to 500,000.
  • DE dextrose equivalent
  • polyacetals which can be obtained by reacting dialdehydes with polyolcarboxylic acids which have 5 to 7 carbon atoms and at least 3 hydroxyl groups, for example as described in European patent application EP-A-0 280 223.
  • Preferred polyacetals are obtained from dialdehydes such as glyoxal, glutaraldehyde, terephthalaldehyde and mixtures thereof and from polyol carboxylic acids such as gluconic acid and / or glucoheptonic acid.
  • the enzymes can be adsorbed on carriers and / or embedded in coating substances in order to protect them against premature decomposition.
  • the proportion of the enzymes, enzyme mixtures or enzyme granules can be, for example, about 0.1 to 5% by weight, preferably 0.1 to about 2% by weight.
  • Table 1 Composition of the spray-dried granules [% by weight]:
  • an extrudate E3 was also produced which contained part of the perfume and was also sprayed with the rest of the perfume. This agent was compared with a comparative sex trudate V3, in which the total amount of the perfume was applied by spraying.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)
  • Fats And Perfumes (AREA)
PCT/EP1998/006513 1997-10-23 1998-10-14 Verfahren zur herstellung duftverstärkter wasch- oder reinigungsmittel Ceased WO1999021955A1 (de)

Priority Applications (6)

Application Number Priority Date Filing Date Title
PL98340036A PL188261B1 (pl) 1997-10-23 1998-10-14 Sposób wytwarzania środka piorącego o wzmocnionymzapachu
AT98955451T ATE246727T1 (de) 1997-10-23 1998-10-14 Verfahren zur herstellung duftverstärkter wasch- oder reinigungsmittel
DE59809226T DE59809226D1 (de) 1997-10-23 1998-10-14 Verfahren zur herstellung duftverstärkter wasch- oder reinigungsmittel
EP98955451A EP1025198B1 (de) 1997-10-23 1998-10-14 Verfahren zur herstellung duftverstärkter wasch- oder reinigungsmittel
JP2000518048A JP2001521060A (ja) 1997-10-23 1998-10-14 芳香性増強洗剤および洗浄剤の製法
US09/529,864 US6228833B1 (en) 1997-10-23 1998-10-14 Method for producing scent intensifying washing and cleaning detergents

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19746781.4 1997-10-23
DE19746781A DE19746781A1 (de) 1997-10-23 1997-10-23 Verfahren zur Herstellung duftverstärkter Wasch- oder Reinigungsmittel

Publications (1)

Publication Number Publication Date
WO1999021955A1 true WO1999021955A1 (de) 1999-05-06

Family

ID=7846357

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP1998/006513 Ceased WO1999021955A1 (de) 1997-10-23 1998-10-14 Verfahren zur herstellung duftverstärkter wasch- oder reinigungsmittel

Country Status (9)

Country Link
US (1) US6228833B1 (https=)
EP (1) EP1025198B1 (https=)
JP (1) JP2001521060A (https=)
CN (1) CN1276829A (https=)
AT (1) ATE246727T1 (https=)
DE (2) DE19746781A1 (https=)
ES (1) ES2205570T3 (https=)
PL (1) PL188261B1 (https=)
WO (1) WO1999021955A1 (https=)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2000023556A1 (de) * 1998-10-17 2000-04-27 Henkel Kommanditgesellschaft Auf Aktien Verfahren zur herstellung extrudierter formkörper
EP1657298A1 (de) * 2004-11-12 2006-05-17 Cognis IP Management GmbH Feste Zubereitungen
WO2008025678A1 (de) * 2006-08-28 2008-03-06 Henkel Ag & Co. Kgaa Schmelzgranulate für wasch- und reinigungsmittel

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1149144A1 (en) * 1999-02-05 2001-10-31 Unilever Plc Dish washing process and compositions relating thereto
US6786223B2 (en) * 2001-10-11 2004-09-07 S. C. Johnson & Son, Inc. Hard surface cleaners which provide improved fragrance retention properties to hard surfaces
GB0130498D0 (en) * 2001-12-20 2002-02-06 Unilever Plc Process for production of detergent tablets
GB0201300D0 (en) * 2002-01-21 2002-03-06 Unilever Plc Detergent composition in tablet form
US7057008B2 (en) * 2002-05-14 2006-06-06 E.I. Du Pont De Nemours And Company Packaging and containers made of water-soluble polyamides and processes for their manufacture
US6689342B1 (en) * 2002-07-29 2004-02-10 Warner-Lambert Company Oral care compositions comprising tropolone compounds and essential oils and methods of using the same
WO2004106479A1 (en) 2003-05-28 2004-12-09 Kao Corporation Process for releasing fragrance
DE102005062008B3 (de) * 2005-12-22 2007-08-30 Henkel Kgaa Geruchsreduktion hypochlorithaltiger Mittel
BRPI0918755A2 (pt) * 2008-09-10 2015-12-08 Danisco Us Inc composição de alvejamento têxtil enzimática e métodos de uso da mesma
CN104479912A (zh) * 2014-12-13 2015-04-01 张慧娜 一种柠檬油复合清洗剂及其制备方法
CN106422978B (zh) * 2016-12-20 2019-03-05 上海试四赫维化工有限公司 水溶性引发剂的造粒方法
EP3642319B1 (en) * 2017-06-20 2020-12-30 Unilever N.V. Particulate detergent composition comprising perfume
CN108531298B (zh) * 2018-04-10 2020-06-23 上海应用技术大学 一种含有金佛手精油微胶囊的洗衣粉及其制备方法
CN111286414B (zh) * 2019-11-28 2021-04-27 纳爱斯浙江科技有限公司 一种衣物留香珠及其制备方法
WO2022104631A1 (en) * 2020-11-19 2022-05-27 The Procter & Gamble Company Method of making detergent compositions comprising perfume
CN115073287B (zh) * 2021-03-11 2024-06-25 万华化学(四川)有限公司 一种高品质乙酸芳樟酯及其制备方法
CN113712421B (zh) * 2021-09-23 2022-10-21 涟源市宝福香业有限公司 一种中药檀香的加工工艺
WO2023142099A1 (en) * 2022-01-30 2023-08-03 The Procter & Gamble Company Method of making perfume-containing particles
CN115108751B (zh) 2022-07-14 2023-03-21 武汉工程大学 一种预拌流态固化土用分散剂及其制备方法和应用
CN115923159A (zh) * 2022-11-01 2023-04-07 重庆工程学院 一种夹芯板生产用压合装置

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1991002047A1 (de) * 1989-08-09 1991-02-21 Henkel Kommanditgesellschaft Auf Aktien Herstellung verdichteter granulate für waschmittel
WO1991013678A1 (de) * 1990-03-09 1991-09-19 Henkel Kommanditgesellschaft Auf Aktien Verfahren zum herstellen von granulaten eines wasch- oder reinigungsmittels
EP0537584A1 (de) * 1991-10-12 1993-04-21 Henkel KGaA Duftstoffe enthaltende Tablette
WO1994009111A1 (de) * 1992-10-22 1994-04-28 Henkel Kommanditgesellschaft Auf Aktien Verfahren zur herstellung wasch- oder reinigungsaktiver extrudate
WO1995011291A1 (de) * 1993-10-21 1995-04-27 Henkel Kommanditgesellschaft Auf Aktien Verfahren zur herstellung wasch- oder reinigungsaktiver extrudate mit verbessertem redispergiervermögen
WO1996029389A1 (de) * 1995-03-17 1996-09-26 Henkel Kommanditgesellschaft Auf Aktien Verfahren zur herstellung eines pulverförmigen wasch- oder reinigungsmittels
WO1997020906A1 (de) * 1995-12-07 1997-06-12 Henkel Kommanditgesellschaft Auf Aktien Verfahren zur herstellung von wasch- oder reinigungsaktiven extrudaten
WO1997047720A2 (en) * 1996-06-11 1997-12-18 The Procter & Gamble Company Process for producing a particulate laundry additive for perfume delivery having improved physical properties
DE19638599A1 (de) * 1996-09-20 1998-03-26 Henkel Kgaa Verfahren zur Herstellung eines teilchenförmigen Wasch- oder Reinigungsmittels

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5198145A (en) * 1990-11-08 1993-03-30 Fmc Corporation Dry detergent compositions
US5691294A (en) * 1993-03-30 1997-11-25 The Procter & Gamble Company Flow aids for detergent powders comprising sodium aluminosilicate and hydrophobic silica

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1991002047A1 (de) * 1989-08-09 1991-02-21 Henkel Kommanditgesellschaft Auf Aktien Herstellung verdichteter granulate für waschmittel
WO1991013678A1 (de) * 1990-03-09 1991-09-19 Henkel Kommanditgesellschaft Auf Aktien Verfahren zum herstellen von granulaten eines wasch- oder reinigungsmittels
EP0537584A1 (de) * 1991-10-12 1993-04-21 Henkel KGaA Duftstoffe enthaltende Tablette
WO1994009111A1 (de) * 1992-10-22 1994-04-28 Henkel Kommanditgesellschaft Auf Aktien Verfahren zur herstellung wasch- oder reinigungsaktiver extrudate
WO1995011291A1 (de) * 1993-10-21 1995-04-27 Henkel Kommanditgesellschaft Auf Aktien Verfahren zur herstellung wasch- oder reinigungsaktiver extrudate mit verbessertem redispergiervermögen
WO1996029389A1 (de) * 1995-03-17 1996-09-26 Henkel Kommanditgesellschaft Auf Aktien Verfahren zur herstellung eines pulverförmigen wasch- oder reinigungsmittels
WO1997020906A1 (de) * 1995-12-07 1997-06-12 Henkel Kommanditgesellschaft Auf Aktien Verfahren zur herstellung von wasch- oder reinigungsaktiven extrudaten
WO1997047720A2 (en) * 1996-06-11 1997-12-18 The Procter & Gamble Company Process for producing a particulate laundry additive for perfume delivery having improved physical properties
DE19638599A1 (de) * 1996-09-20 1998-03-26 Henkel Kgaa Verfahren zur Herstellung eines teilchenförmigen Wasch- oder Reinigungsmittels
WO1998012299A1 (de) * 1996-09-20 1998-03-26 Henkel Kommanditgesellschaft Auf Aktien Verfahren zur herstellung eines teilchenförmigen wasch- oder reinigungsmittels

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2000023556A1 (de) * 1998-10-17 2000-04-27 Henkel Kommanditgesellschaft Auf Aktien Verfahren zur herstellung extrudierter formkörper
EP1657298A1 (de) * 2004-11-12 2006-05-17 Cognis IP Management GmbH Feste Zubereitungen
WO2008025678A1 (de) * 2006-08-28 2008-03-06 Henkel Ag & Co. Kgaa Schmelzgranulate für wasch- und reinigungsmittel

Also Published As

Publication number Publication date
PL188261B1 (pl) 2005-01-31
JP2001521060A (ja) 2001-11-06
ES2205570T3 (es) 2004-05-01
PL340036A1 (en) 2001-01-15
EP1025198A1 (de) 2000-08-09
US6228833B1 (en) 2001-05-08
DE19746781A1 (de) 1999-04-29
ATE246727T1 (de) 2003-08-15
DE59809226D1 (de) 2003-09-11
CN1276829A (zh) 2000-12-13
EP1025198B1 (de) 2003-08-06

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