WO1999021955A1 - Verfahren zur herstellung duftverstärkter wasch- oder reinigungsmittel - Google Patents
Verfahren zur herstellung duftverstärkter wasch- oder reinigungsmittel Download PDFInfo
- Publication number
- WO1999021955A1 WO1999021955A1 PCT/EP1998/006513 EP9806513W WO9921955A1 WO 1999021955 A1 WO1999021955 A1 WO 1999021955A1 EP 9806513 W EP9806513 W EP 9806513W WO 9921955 A1 WO9921955 A1 WO 9921955A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- premix
- weight
- perfume
- binder
- fragrance
- Prior art date
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- 125000001046 glycoluril group Chemical group [H]C12N(*)C(=O)N(*)C1([H])N(*)C(=O)N2* 0.000 description 1
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- 229910000271 hectorite Inorganic materials 0.000 description 1
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- 150000003951 lactams Chemical class 0.000 description 1
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- 238000000691 measurement method Methods 0.000 description 1
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- 229930007503 menthone Natural products 0.000 description 1
- UZKWTJUDCOPSNM-UHFFFAOYSA-N methoxybenzene Substances CCCCOC=C UZKWTJUDCOPSNM-UHFFFAOYSA-N 0.000 description 1
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- OSWPMRLSEDHDFF-UHFFFAOYSA-N methyl salicylate Chemical compound COC(=O)C1=CC=CC=C1O OSWPMRLSEDHDFF-UHFFFAOYSA-N 0.000 description 1
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- JPTOCTSNXXKSSN-UHFFFAOYSA-N methylheptenone Chemical compound CCCC=CC(=O)CC JPTOCTSNXXKSSN-UHFFFAOYSA-N 0.000 description 1
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- 239000004200 microcrystalline wax Substances 0.000 description 1
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- 150000005673 monoalkenes Chemical class 0.000 description 1
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- 239000001186 myroxylon pereirae klotzsch oil Substances 0.000 description 1
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- 239000007800 oxidant agent Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- VGTPKLINSHNZRD-UHFFFAOYSA-N oxoborinic acid Chemical class OB=O VGTPKLINSHNZRD-UHFFFAOYSA-N 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 125000000913 palmityl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- FJKROLUGYXJWQN-UHFFFAOYSA-N papa-hydroxy-benzoic acid Natural products OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 description 1
- QNGNSVIICDLXHT-UHFFFAOYSA-N para-ethylbenzaldehyde Natural products CCC1=CC=C(C=O)C=C1 QNGNSVIICDLXHT-UHFFFAOYSA-N 0.000 description 1
- 235000011837 pasties Nutrition 0.000 description 1
- LVECZGHBXXYWBO-UHFFFAOYSA-N pentadecanolide Natural products CC1CCCCCCCCCCCCC(=O)O1 LVECZGHBXXYWBO-UHFFFAOYSA-N 0.000 description 1
- 235000019477 peppermint oil Nutrition 0.000 description 1
- 150000004965 peroxy acids Chemical class 0.000 description 1
- 150000007875 phellandrene derivatives Chemical class 0.000 description 1
- PATMLLNMTPIUSY-UHFFFAOYSA-N phenoxysulfonyl 7-methyloctanoate Chemical compound CC(C)CCCCCC(=O)OS(=O)(=O)OC1=CC=CC=C1 PATMLLNMTPIUSY-UHFFFAOYSA-N 0.000 description 1
- WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 description 1
- 229940067107 phenylethyl alcohol Drugs 0.000 description 1
- 150000003022 phthalic acids Chemical class 0.000 description 1
- 229910052615 phyllosilicate Inorganic materials 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000001622 pimenta officinalis fruit oil Substances 0.000 description 1
- 239000010665 pine oil Substances 0.000 description 1
- SATCULPHIDQDRE-UHFFFAOYSA-N piperonal Chemical compound O=CC1=CC=C2OCOC2=C1 SATCULPHIDQDRE-UHFFFAOYSA-N 0.000 description 1
- 239000001738 pogostemon cablin oil Substances 0.000 description 1
- 239000004584 polyacrylic acid Substances 0.000 description 1
- 229920001521 polyalkylene glycol ether Polymers 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 229920005862 polyol Polymers 0.000 description 1
- 235000020777 polyunsaturated fatty acids Nutrition 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 235000019353 potassium silicate Nutrition 0.000 description 1
- WSHYKIAQCMIPTB-UHFFFAOYSA-M potassium;2-oxo-3-(3-oxo-1-phenylbutyl)chromen-4-olate Chemical compound [K+].[O-]C=1C2=CC=CC=C2OC(=O)C=1C(CC(=O)C)C1=CC=CC=C1 WSHYKIAQCMIPTB-UHFFFAOYSA-M 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 230000002028 premature Effects 0.000 description 1
- 150000003138 primary alcohols Chemical class 0.000 description 1
- 238000004886 process control Methods 0.000 description 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 238000006268 reductive amination reaction Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 239000010666 rose oil Substances 0.000 description 1
- 235000019719 rose oil Nutrition 0.000 description 1
- 239000010668 rosemary oil Substances 0.000 description 1
- 229940058206 rosemary oil Drugs 0.000 description 1
- 239000010670 sage oil Substances 0.000 description 1
- 229960004889 salicylic acid Drugs 0.000 description 1
- 229910000275 saponite Inorganic materials 0.000 description 1
- 150000004671 saturated fatty acids Chemical class 0.000 description 1
- 150000003333 secondary alcohols Chemical class 0.000 description 1
- ZFRKQXVRDFCRJG-UHFFFAOYSA-N skatole Chemical compound C1=CC=C2C(C)=CNC2=C1 ZFRKQXVRDFCRJG-UHFFFAOYSA-N 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- HLBBKKJFGFRGMU-UHFFFAOYSA-M sodium formate Chemical compound [Na+].[O-]C=O HLBBKKJFGFRGMU-UHFFFAOYSA-M 0.000 description 1
- 235000019254 sodium formate Nutrition 0.000 description 1
- 239000012418 sodium perborate tetrahydrate Substances 0.000 description 1
- 229940045872 sodium percarbonate Drugs 0.000 description 1
- 239000004328 sodium tetraborate Substances 0.000 description 1
- 235000010339 sodium tetraborate Nutrition 0.000 description 1
- RPACBEVZENYWOL-XFULWGLBSA-M sodium;(2r)-2-[6-(4-chlorophenoxy)hexyl]oxirane-2-carboxylate Chemical compound [Na+].C=1C=C(Cl)C=CC=1OCCCCCC[C@]1(C(=O)[O-])CO1 RPACBEVZENYWOL-XFULWGLBSA-M 0.000 description 1
- IBDSNZLUHYKHQP-UHFFFAOYSA-N sodium;3-oxidodioxaborirane;tetrahydrate Chemical compound O.O.O.O.[Na+].[O-]B1OO1 IBDSNZLUHYKHQP-UHFFFAOYSA-N 0.000 description 1
- 239000000600 sorbitol Substances 0.000 description 1
- 235000019721 spearmint oil Nutrition 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000010675 spruce oil Substances 0.000 description 1
- 239000010676 star anise oil Substances 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- 229940012831 stearyl alcohol Drugs 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 150000008163 sugars Chemical class 0.000 description 1
- 125000000020 sulfo group Chemical group O=S(=O)([*])O[H] 0.000 description 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
- 150000003871 sulfonates Chemical class 0.000 description 1
- 150000003470 sulfuric acid monoesters Chemical class 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 235000020357 syrup Nutrition 0.000 description 1
- 239000006188 syrup Substances 0.000 description 1
- KUCOHFSKRZZVRO-UHFFFAOYSA-N terephthalaldehyde Chemical compound O=CC1=CC=C(C=O)C=C1 KUCOHFSKRZZVRO-UHFFFAOYSA-N 0.000 description 1
- 150000003505 terpenes Chemical class 0.000 description 1
- 235000007586 terpenes Nutrition 0.000 description 1
- 229940116411 terpineol Drugs 0.000 description 1
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical class CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 1
- 229960000790 thymol Drugs 0.000 description 1
- CRDAMVZIKSXKFV-UHFFFAOYSA-N trans-Farnesol Natural products CC(C)=CCCC(C)=CCCC(C)=CCO CRDAMVZIKSXKFV-UHFFFAOYSA-N 0.000 description 1
- BJIOGJUNALELMI-UHFFFAOYSA-N trans-isoeugenol Natural products COC1=CC(C=CC)=CC=C1O BJIOGJUNALELMI-UHFFFAOYSA-N 0.000 description 1
- XMLSXPIVAXONDL-UHFFFAOYSA-N trans-jasmone Natural products CCC=CCC1=C(C)CCC1=O XMLSXPIVAXONDL-UHFFFAOYSA-N 0.000 description 1
- 238000005809 transesterification reaction Methods 0.000 description 1
- 150000003626 triacylglycerols Chemical class 0.000 description 1
- 150000003918 triazines Chemical class 0.000 description 1
- 150000005691 triesters Chemical class 0.000 description 1
- 239000013638 trimer Substances 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- MWOOGOJBHIARFG-UHFFFAOYSA-N vanillin Chemical compound COC1=CC(C=O)=CC=C1O MWOOGOJBHIARFG-UHFFFAOYSA-N 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- WJUFSDZVCOTFON-UHFFFAOYSA-N veratraldehyde Chemical compound COC1=CC=C(C=O)C=C1OC WJUFSDZVCOTFON-UHFFFAOYSA-N 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
- 239000009637 wintergreen oil Substances 0.000 description 1
- ZFNVDHOSLNRHNN-UHFFFAOYSA-N xi-3-(4-Isopropylphenyl)-2-methylpropanal Chemical compound O=CC(C)CC1=CC=C(C(C)C)C=C1 ZFNVDHOSLNRHNN-UHFFFAOYSA-N 0.000 description 1
- 239000002888 zwitterionic surfactant Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
Definitions
- the essentially water-free premix which is pressed agglomerated preferably has no dust-like components and in particular no particles with particle sizes below 200 ⁇ m.
- those particle size distributions are preferred which have at least 90% by weight of particles with a diameter of at least 400 ⁇ m.
- the washing or cleaning agents or components produced by press agglomeration consist of at least 70% by weight, advantageously at least 80% by weight and, with particular preference, up to 100% by weight spherical or almost spherical (pearl-shaped) particles with a particle size distribution which has at least 60% by weight of particles between 0.8 and 2.0 mm.
- the premix can contain a raw material or a compound which functions as a binding and disintegration aid.
- these binding and disintegration aids serve as lubricants and adhesives which adhere the solid components of the premix to one another and facilitate the passage of the premix through the pressure zone of the press agglomeration apparatus.
- water-soluble binders they also facilitate the redissolution of the press agglomerates, since they act as disintegrants in aqueous liquors.
- the particularly preferred polyethylene glycols include those with relative molecular weights between 2000 and 12000, advantageously around 4000, polyethylene glycols with relative molecular weights below 3500 and above 5000, in particular in combination with polyethylene glycols with a relative molecular weight of around 4000, and such combinations advantageously to more than 50% by weight, based on the total amount of polyethylene glycols, have polyethylene glycols with a relative molecular weight between 3500 and 5000.
- polyethylene glycols which are in the liquid state at room temperature and a pressure of 1 bar can also be used as binders;
- polyethylene glycol with a relative molecular mass of 200, 400 and 600 can also be used as binders;
- these per se liquid polyethylene glycols should only be used in a mixture with at least one further binder, this mixture again having to meet the requirements according to the invention, that is to say having a melting point or softening point of at least above 45 ° C.
- the more volatile fragrances include, in particular, the lower-boiling fragrances of natural or synthetic origin, which can be used alone or in mixtures.
- Examples of more volatile fragrances are alkyisothiocyanates (alkyl mustards), butanedione, limonene, linalool, Linaylacetate and propionate, menthol, Menthone, methyl-n-heptenone, phellandrene, phenylacetaldehyde, terpinylacetate, citral, citronellal.
- the group of polyhydroxy fatty acid amides also includes compounds of the formula (II)
- Suitable organic builder substances are dextrins, for example oligomers or polymers of carbohydrates, which can be obtained by partial hydrolysis of starches.
- the hydrolysis can be carried out by customary processes, for example acid-catalyzed or enzyme-catalyzed. They are preferably hydrolysis products with average molecular weights in the range from 400 to 500,000.
- DE dextrose equivalent
- polyacetals which can be obtained by reacting dialdehydes with polyolcarboxylic acids which have 5 to 7 carbon atoms and at least 3 hydroxyl groups, for example as described in European patent application EP-A-0 280 223.
- Preferred polyacetals are obtained from dialdehydes such as glyoxal, glutaraldehyde, terephthalaldehyde and mixtures thereof and from polyol carboxylic acids such as gluconic acid and / or glucoheptonic acid.
- the enzymes can be adsorbed on carriers and / or embedded in coating substances in order to protect them against premature decomposition.
- the proportion of the enzymes, enzyme mixtures or enzyme granules can be, for example, about 0.1 to 5% by weight, preferably 0.1 to about 2% by weight.
- Table 1 Composition of the spray-dried granules [% by weight]:
- an extrudate E3 was also produced which contained part of the perfume and was also sprayed with the rest of the perfume. This agent was compared with a comparative sex trudate V3, in which the total amount of the perfume was applied by spraying.
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
- Fats And Perfumes (AREA)
Abstract
Description
Claims
Priority Applications (6)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US09/529,864 US6228833B1 (en) | 1997-10-23 | 1998-10-14 | Method for producing scent intensifying washing and cleaning detergents |
PL98340036A PL188261B1 (pl) | 1997-10-23 | 1998-10-14 | Sposób wytwarzania środka piorącego o wzmocnionymzapachu |
AT98955451T ATE246727T1 (de) | 1997-10-23 | 1998-10-14 | Verfahren zur herstellung duftverstärkter wasch- oder reinigungsmittel |
EP98955451A EP1025198B1 (de) | 1997-10-23 | 1998-10-14 | Verfahren zur herstellung duftverstärkter wasch- oder reinigungsmittel |
DE59809226T DE59809226D1 (de) | 1997-10-23 | 1998-10-14 | Verfahren zur herstellung duftverstärkter wasch- oder reinigungsmittel |
JP2000518048A JP2001521060A (ja) | 1997-10-23 | 1998-10-14 | 芳香性増強洗剤および洗浄剤の製法 |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19746781.4 | 1997-10-23 | ||
DE19746781A DE19746781A1 (de) | 1997-10-23 | 1997-10-23 | Verfahren zur Herstellung duftverstärkter Wasch- oder Reinigungsmittel |
Publications (1)
Publication Number | Publication Date |
---|---|
WO1999021955A1 true WO1999021955A1 (de) | 1999-05-06 |
Family
ID=7846357
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/EP1998/006513 WO1999021955A1 (de) | 1997-10-23 | 1998-10-14 | Verfahren zur herstellung duftverstärkter wasch- oder reinigungsmittel |
Country Status (9)
Country | Link |
---|---|
US (1) | US6228833B1 (de) |
EP (1) | EP1025198B1 (de) |
JP (1) | JP2001521060A (de) |
CN (1) | CN1276829A (de) |
AT (1) | ATE246727T1 (de) |
DE (2) | DE19746781A1 (de) |
ES (1) | ES2205570T3 (de) |
PL (1) | PL188261B1 (de) |
WO (1) | WO1999021955A1 (de) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
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WO2000023556A1 (de) * | 1998-10-17 | 2000-04-27 | Henkel Kommanditgesellschaft Auf Aktien | Verfahren zur herstellung extrudierter formkörper |
EP1657298A1 (de) * | 2004-11-12 | 2006-05-17 | Cognis IP Management GmbH | Feste Zubereitungen |
WO2008025678A1 (de) * | 2006-08-28 | 2008-03-06 | Henkel Ag & Co. Kgaa | Schmelzgranulate für wasch- und reinigungsmittel |
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WO2000046329A1 (en) * | 1999-02-05 | 2000-08-10 | Unilever Plc | Dish washing process and compositions relating thereto |
US6786223B2 (en) * | 2001-10-11 | 2004-09-07 | S. C. Johnson & Son, Inc. | Hard surface cleaners which provide improved fragrance retention properties to hard surfaces |
GB0130498D0 (en) * | 2001-12-20 | 2002-02-06 | Unilever Plc | Process for production of detergent tablets |
GB0201300D0 (en) * | 2002-01-21 | 2002-03-06 | Unilever Plc | Detergent composition in tablet form |
AU2003234550A1 (en) * | 2002-05-14 | 2003-12-02 | E.I. Du Pont De Nemours And Company | Packaging and containers made of water-soluble polyamides and processes for their manufacture |
US6689342B1 (en) * | 2002-07-29 | 2004-02-10 | Warner-Lambert Company | Oral care compositions comprising tropolone compounds and essential oils and methods of using the same |
CN100532525C (zh) | 2003-05-28 | 2009-08-26 | 花王株式会社 | 释放香味的方法 |
DE102005062008B3 (de) * | 2005-12-22 | 2007-08-30 | Henkel Kgaa | Geruchsreduktion hypochlorithaltiger Mittel |
WO2010030769A1 (en) * | 2008-09-10 | 2010-03-18 | Danisco Us Inc. | Enzymatic textile bleaching compositions and methods of use thereof |
CN104479912A (zh) * | 2014-12-13 | 2015-04-01 | 张慧娜 | 一种柠檬油复合清洗剂及其制备方法 |
CN106422978B (zh) * | 2016-12-20 | 2019-03-05 | 上海试四赫维化工有限公司 | 水溶性引发剂的造粒方法 |
EP3642319B1 (de) * | 2017-06-20 | 2020-12-30 | Unilever N.V. | Partikelförmige waschmittelzusammensetzungen mit parfüm |
CN108531298B (zh) * | 2018-04-10 | 2020-06-23 | 上海应用技术大学 | 一种含有金佛手精油微胶囊的洗衣粉及其制备方法 |
CN111286414B (zh) * | 2019-11-28 | 2021-04-27 | 纳爱斯浙江科技有限公司 | 一种衣物留香珠及其制备方法 |
EP4247930A1 (de) * | 2020-11-19 | 2023-09-27 | The Procter & Gamble Company | Verfahren zum herstellen von waschmittelzusammensetzungen mit parfüm |
CN115073287B (zh) * | 2021-03-11 | 2024-06-25 | 万华化学(四川)有限公司 | 一种高品质乙酸芳樟酯及其制备方法 |
CN113712421B (zh) * | 2021-09-23 | 2022-10-21 | 涟源市宝福香业有限公司 | 一种中药檀香的加工工艺 |
CN115108751B (zh) | 2022-07-14 | 2023-03-21 | 武汉工程大学 | 一种预拌流态固化土用分散剂及其制备方法和应用 |
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US5198145A (en) * | 1990-11-08 | 1993-03-30 | Fmc Corporation | Dry detergent compositions |
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1997
- 1997-10-23 DE DE19746781A patent/DE19746781A1/de not_active Withdrawn
-
1998
- 1998-10-14 PL PL98340036A patent/PL188261B1/pl not_active IP Right Cessation
- 1998-10-14 CN CN98810454A patent/CN1276829A/zh active Pending
- 1998-10-14 DE DE59809226T patent/DE59809226D1/de not_active Revoked
- 1998-10-14 ES ES98955451T patent/ES2205570T3/es not_active Expired - Lifetime
- 1998-10-14 US US09/529,864 patent/US6228833B1/en not_active Expired - Fee Related
- 1998-10-14 AT AT98955451T patent/ATE246727T1/de not_active IP Right Cessation
- 1998-10-14 EP EP98955451A patent/EP1025198B1/de not_active Revoked
- 1998-10-14 WO PCT/EP1998/006513 patent/WO1999021955A1/de not_active Application Discontinuation
- 1998-10-14 JP JP2000518048A patent/JP2001521060A/ja active Pending
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WO1991002047A1 (de) * | 1989-08-09 | 1991-02-21 | Henkel Kommanditgesellschaft Auf Aktien | Herstellung verdichteter granulate für waschmittel |
WO1991013678A1 (de) * | 1990-03-09 | 1991-09-19 | Henkel Kommanditgesellschaft Auf Aktien | Verfahren zum herstellen von granulaten eines wasch- oder reinigungsmittels |
EP0537584A1 (de) * | 1991-10-12 | 1993-04-21 | Henkel KGaA | Duftstoffe enthaltende Tablette |
WO1994009111A1 (de) * | 1992-10-22 | 1994-04-28 | Henkel Kommanditgesellschaft Auf Aktien | Verfahren zur herstellung wasch- oder reinigungsaktiver extrudate |
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WO1996029389A1 (de) * | 1995-03-17 | 1996-09-26 | Henkel Kommanditgesellschaft Auf Aktien | Verfahren zur herstellung eines pulverförmigen wasch- oder reinigungsmittels |
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WO1997047720A2 (en) * | 1996-06-11 | 1997-12-18 | The Procter & Gamble Company | Process for producing a particulate laundry additive for perfume delivery having improved physical properties |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
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WO2000023556A1 (de) * | 1998-10-17 | 2000-04-27 | Henkel Kommanditgesellschaft Auf Aktien | Verfahren zur herstellung extrudierter formkörper |
EP1657298A1 (de) * | 2004-11-12 | 2006-05-17 | Cognis IP Management GmbH | Feste Zubereitungen |
WO2008025678A1 (de) * | 2006-08-28 | 2008-03-06 | Henkel Ag & Co. Kgaa | Schmelzgranulate für wasch- und reinigungsmittel |
Also Published As
Publication number | Publication date |
---|---|
EP1025198B1 (de) | 2003-08-06 |
PL340036A1 (en) | 2001-01-15 |
US6228833B1 (en) | 2001-05-08 |
DE59809226D1 (de) | 2003-09-11 |
JP2001521060A (ja) | 2001-11-06 |
PL188261B1 (pl) | 2005-01-31 |
DE19746781A1 (de) | 1999-04-29 |
EP1025198A1 (de) | 2000-08-09 |
ATE246727T1 (de) | 2003-08-15 |
ES2205570T3 (es) | 2004-05-01 |
CN1276829A (zh) | 2000-12-13 |
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