TWI717628B - 金屬污染評價方法 - Google Patents

金屬污染評價方法 Download PDF

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Publication number
TWI717628B
TWI717628B TW107128807A TW107128807A TWI717628B TW I717628 B TWI717628 B TW I717628B TW 107128807 A TW107128807 A TW 107128807A TW 107128807 A TW107128807 A TW 107128807A TW I717628 B TWI717628 B TW I717628B
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Taiwan
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silicon wafer
silicon
metal contamination
concentration
evaluation method
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TW107128807A
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English (en)
Chinese (zh)
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TW201929111A (zh
Inventor
荒木延惠
小野塚健
石原知幸
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日商環球晶圓日本股份有限公司
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    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10PGENERIC PROCESSES OR APPARATUS FOR THE MANUFACTURE OR TREATMENT OF DEVICES COVERED BY CLASS H10
    • H10P74/00Testing or measuring during manufacture or treatment of wafers, substrates or devices
    • H10P74/20Testing or measuring during manufacture or treatment of wafers, substrates or devices characterised by the properties tested or measured, e.g. structural or electrical properties
    • H10P74/203Structural properties, e.g. testing or measuring thicknesses, line widths, warpage, bond strengths or physical defects
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B15/00Single-crystal growth by pulling from a melt, e.g. Czochralski method
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B15/00Single-crystal growth by pulling from a melt, e.g. Czochralski method
    • C30B15/14Heating of the melt or the crystallised materials
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B15/00Single-crystal growth by pulling from a melt, e.g. Czochralski method
    • C30B15/20Controlling or regulating
    • C30B15/203Controlling or regulating the relationship of pull rate (v) to axial thermal gradient (G)
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/02Elements
    • C30B29/06Silicon
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/62Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
    • G01N21/63Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
    • G01N21/64Fluorescence; Phosphorescence
    • G01N21/6408Fluorescence; Phosphorescence with measurement of decay time, time resolved fluorescence
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/62Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
    • G01N21/63Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
    • G01N21/64Fluorescence; Phosphorescence
    • G01N21/6489Photoluminescence of semiconductors
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/32Gas-filled discharge tubes
    • H01J37/32009Arrangements for generation of plasma specially adapted for examination or treatment of objects, e.g. plasma sources
    • H01J37/32073Corona discharge
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10PGENERIC PROCESSES OR APPARATUS FOR THE MANUFACTURE OR TREATMENT OF DEVICES COVERED BY CLASS H10
    • H10P14/00Formation of materials, e.g. in the shape of layers or pillars
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10PGENERIC PROCESSES OR APPARATUS FOR THE MANUFACTURE OR TREATMENT OF DEVICES COVERED BY CLASS H10
    • H10P34/00Irradiation with electromagnetic or particle radiation of wafers, substrates or parts of devices
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10PGENERIC PROCESSES OR APPARATUS FOR THE MANUFACTURE OR TREATMENT OF DEVICES COVERED BY CLASS H10
    • H10P36/00Gettering within semiconductor bodies
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10PGENERIC PROCESSES OR APPARATUS FOR THE MANUFACTURE OR TREATMENT OF DEVICES COVERED BY CLASS H10
    • H10P74/00Testing or measuring during manufacture or treatment of wafers, substrates or devices
    • H10P74/23Testing or measuring during manufacture or treatment of wafers, substrates or devices characterised by multiple measurements, corrections, marking or sorting processes
    • H10P74/232Testing or measuring during manufacture or treatment of wafers, substrates or devices characterised by multiple measurements, corrections, marking or sorting processes comprising connection or disconnection of parts of a device in response to a measurement
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J2237/00Discharge tubes exposing object to beam, e.g. for analysis treatment, etching, imaging
    • H01J2237/245Detection characterised by the variable being measured
    • H01J2237/24592Inspection and quality control of devices
    • HELECTRICITY
    • H10SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10PGENERIC PROCESSES OR APPARATUS FOR THE MANUFACTURE OR TREATMENT OF DEVICES COVERED BY CLASS H10
    • H10P74/00Testing or measuring during manufacture or treatment of wafers, substrates or devices
    • H10P74/23Testing or measuring during manufacture or treatment of wafers, substrates or devices characterised by multiple measurements, corrections, marking or sorting processes

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Organic Chemistry (AREA)
  • Metallurgy (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • General Physics & Mathematics (AREA)
  • General Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Plasma & Fusion (AREA)
  • Testing Or Measuring Of Semiconductors Or The Like (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
  • High Energy & Nuclear Physics (AREA)
  • Toxicology (AREA)
TW107128807A 2017-12-22 2018-08-17 金屬污染評價方法 TWI717628B (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2017246190A JP7057122B2 (ja) 2017-12-22 2017-12-22 金属汚染評価方法
JP2017-246190 2017-12-22

Publications (2)

Publication Number Publication Date
TW201929111A TW201929111A (zh) 2019-07-16
TWI717628B true TWI717628B (zh) 2021-02-01

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TW107128807A TWI717628B (zh) 2017-12-22 2018-08-17 金屬污染評價方法

Country Status (7)

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US (1) US11538721B2 (https=)
EP (1) EP3731263A4 (https=)
JP (1) JP7057122B2 (https=)
KR (1) KR102463966B1 (https=)
CN (1) CN111480219A (https=)
TW (1) TWI717628B (https=)
WO (1) WO2019123706A1 (https=)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7561498B2 (ja) 2020-02-14 2024-10-04 グローバルウェーハズ・ジャパン株式会社 シリコン単結晶の製造方法
CN112366146A (zh) * 2020-11-05 2021-02-12 天津中环领先材料技术有限公司 一种晶圆片的寿命测试方法
CN112908876A (zh) * 2021-01-18 2021-06-04 上海新昇半导体科技有限公司 硅片金属污染测试方法及装置
JP7249395B1 (ja) * 2021-11-10 2023-03-30 株式会社Sumco 半導体試料の評価方法、半導体試料の評価装置および半導体ウェーハの製造方法

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TW201239144A (en) * 2011-01-19 2012-10-01 Sumco Corp Inspection method and fabricating method for silicon single crystal
US20140191370A1 (en) * 2013-01-08 2014-07-10 Woo Young Sim Silicon single crystal wafer, manufacturing method thereof and method of detecting defects
TW201445013A (zh) * 2012-08-08 2014-12-01 世創電子材料公司 單晶矽半導體晶圓及其製造方法
US20150020728A1 (en) * 2012-03-16 2015-01-22 Shin-Etsu Handotai Co., Ltd. Method for manufacturing silicon single crystal wafer
TW201639036A (zh) * 2015-02-19 2016-11-01 信越半導體股份有限公司 矽晶圓的製造方法
TW201720972A (zh) * 2015-12-11 2017-06-16 世創電子材料公司 由單晶矽製成的半導體晶圓及其製備方法

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB0216184D0 (en) 2002-07-12 2002-08-21 Aoti Operating Co Inc Detection method and apparatus
JP4200845B2 (ja) 2002-10-18 2008-12-24 株式会社Sumco シリコン単結晶インゴットの点欠陥分布を測定する方法
TWI231357B (en) 2002-10-18 2005-04-21 Sumitomo Mitsubishi Silicon Method for measuring defect-distribution in silicon monocrystal ingot
KR100500712B1 (ko) * 2002-12-16 2005-07-11 주식회사 실트론 실리콘웨이퍼의 금속 불순물 농도 측정 방법
JP2009266835A (ja) * 2008-04-21 2009-11-12 Sumco Corp シリコン単結晶の金属汚染評価方法
JP5439752B2 (ja) 2008-06-13 2014-03-12 信越半導体株式会社 汚染検出用モニターウェーハ、汚染検出方法及びエピタキシャルウェーハの製造方法
JP5410769B2 (ja) 2009-01-30 2014-02-05 グローバルウェーハズ・ジャパン株式会社 シリコンウェーハの熱処理方法
US8252700B2 (en) 2009-01-30 2012-08-28 Covalent Materials Corporation Method of heat treating silicon wafer
WO2010119614A1 (ja) 2009-04-13 2010-10-21 信越半導体株式会社 アニールウエーハおよびアニールウエーハの製造方法ならびにデバイスの製造方法
JP5467923B2 (ja) * 2010-05-06 2014-04-09 信越半導体株式会社 金属汚染評価用シリコンウエーハの製造方法
JP5590002B2 (ja) 2011-10-12 2014-09-17 信越半導体株式会社 金属汚染評価方法及びエピタキシャルウェーハの製造方法
JP2013105914A (ja) 2011-11-14 2013-05-30 Shin Etsu Handotai Co Ltd 気相成長装置の清浄度評価方法
JP5742742B2 (ja) * 2012-02-08 2015-07-01 信越半導体株式会社 金属汚染評価方法
JP2014058414A (ja) 2012-09-14 2014-04-03 Jnc Corp 評価用シリコン単結晶の製造方法
EP2779220B1 (en) * 2013-03-12 2017-10-25 GLobalWafers Japan Co., Ltd. Saturation voltage estimation method and silicon epitaxial wafer manufaturing method
JP5885305B2 (ja) * 2013-08-07 2016-03-15 グローバルウェーハズ・ジャパン株式会社 シリコンウェーハ及びその製造方法
JP6555103B2 (ja) 2015-11-30 2019-08-07 株式会社Sumco シリコンウェーハの評価方法およびその利用

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TW201239144A (en) * 2011-01-19 2012-10-01 Sumco Corp Inspection method and fabricating method for silicon single crystal
US20150020728A1 (en) * 2012-03-16 2015-01-22 Shin-Etsu Handotai Co., Ltd. Method for manufacturing silicon single crystal wafer
TW201445013A (zh) * 2012-08-08 2014-12-01 世創電子材料公司 單晶矽半導體晶圓及其製造方法
US20140191370A1 (en) * 2013-01-08 2014-07-10 Woo Young Sim Silicon single crystal wafer, manufacturing method thereof and method of detecting defects
TW201639036A (zh) * 2015-02-19 2016-11-01 信越半導體股份有限公司 矽晶圓的製造方法
TW201720972A (zh) * 2015-12-11 2017-06-16 世創電子材料公司 由單晶矽製成的半導體晶圓及其製備方法

Also Published As

Publication number Publication date
EP3731263A1 (en) 2020-10-28
KR20200100783A (ko) 2020-08-26
WO2019123706A1 (ja) 2019-06-27
JP7057122B2 (ja) 2022-04-19
EP3731263A4 (en) 2021-09-08
US11538721B2 (en) 2022-12-27
US20210082774A1 (en) 2021-03-18
KR102463966B1 (ko) 2022-11-04
CN111480219A (zh) 2020-07-31
TW201929111A (zh) 2019-07-16
JP2019114633A (ja) 2019-07-11

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