RO93878B - Procedeu de recristalizare - Google Patents

Procedeu de recristalizare

Info

Publication number
RO93878B
RO93878B RO118238A RO11823885A RO93878B RO 93878 B RO93878 B RO 93878B RO 118238 A RO118238 A RO 118238A RO 11823885 A RO11823885 A RO 11823885A RO 93878 B RO93878 B RO 93878B
Authority
RO
Romania
Prior art keywords
microns
rdx
crystals
hmx
recrystallization process
Prior art date
Application number
RO118238A
Other languages
English (en)
Other versions
RO93878A (ro
Inventor
Svensson Leif
Westling Lars
Nyqvist Jan-Olof
Original Assignee
Ab Bofors
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ab Bofors filed Critical Ab Bofors
Publication of RO93878A publication Critical patent/RO93878A/ro
Publication of RO93878B publication Critical patent/RO93878B/ro

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D257/00—Heterocyclic compounds containing rings having four nitrogen atoms as the only ring hetero atoms
    • C07D257/02—Heterocyclic compounds containing rings having four nitrogen atoms as the only ring hetero atoms not condensed with other rings
    • C—CHEMISTRY; METALLURGY
    • C06—EXPLOSIVES; MATCHES
    • C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
    • C06B25/00—Compositions containing a nitrated organic compound
    • C06B25/34—Compositions containing a nitrated organic compound the compound being a nitrated acyclic, alicyclic or heterocyclic amine
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
    • C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
    • C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
    • C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
    • C07D251/40—Nitrogen atoms
    • C07D251/54—Three nitrogen atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
  • Saccharide Compounds (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Peptides Or Proteins (AREA)
  • Liquid Crystal Substances (AREA)

Abstract

Inventia de fata se refera la un procedeu pentru recristalizarea explozibililor puternici HMX si RDX. în conformitate cu inventia, explozibilul este dizolvat într-o lactona cu greutate moleculara mica, lichida (la temperatura camerei), dupa care gradul de saturatie al solutiei obtinute este modificat, fie prin reducerea temperaturii, fie prin diluare cu apa. Prin aceasta metoda se obtine, în functie de metoda de cristalizare aleasa, cristale de -HMX sau cristale de RDX cu diametrul mediu al particulelor fie de 50...1500 miu m, fie de 5...50 miu m.
RO118238A 1984-04-04 1985-04-02 Procedeu de recristalizare RO93878B (ro)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SE8401857A SE451718B (sv) 1984-04-04 1984-04-04 Sett att omkristallisera sprengemnena oktogen och hexogen

Publications (2)

Publication Number Publication Date
RO93878A RO93878A (ro) 1988-02-29
RO93878B true RO93878B (ro) 1988-03-01

Family

ID=20355439

Family Applications (1)

Application Number Title Priority Date Filing Date
RO118238A RO93878B (ro) 1984-04-04 1985-04-02 Procedeu de recristalizare

Country Status (16)

Country Link
US (1) US4638065A (ro)
JP (1) JPS60226500A (ro)
AR (1) AR240789A1 (ro)
AU (1) AU567609B2 (ro)
BR (1) BR8501575A (ro)
CA (1) CA1243672A (ro)
DE (1) DE3510761C2 (ro)
ES (1) ES8608325A1 (ro)
FR (1) FR2562538B1 (ro)
GB (1) GB2156805B (ro)
IN (1) IN163711B (ro)
IT (1) IT1181872B (ro)
NO (1) NO160775B (ro)
RO (1) RO93878B (ro)
SE (1) SE451718B (ro)
YU (1) YU45244B (ro)

Families Citing this family (35)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3527200A1 (de) * 1985-07-30 1987-03-19 Horst Dipl Ing Hommel Verfahren zum herstellen von sphaerolitischem kristallisat hoher schuett- und packungsdichte, insbesondere von kugelig kristallisiertem nitroguanidin
DE3605634A1 (de) * 1986-02-21 1987-08-27 Messerschmitt Boelkow Blohm Verfahren zur behandlung kristalliner sprengstoffe fuer hochleistungssprengladungen
DE3617408C1 (de) * 1986-05-23 1987-06-11 Dynamit Nobel Ag Verfahren zur Herstellung von feinkoernigem beta-Oktogen
EP0288122B1 (en) * 1987-04-22 1993-02-24 Nobel Kemi AB A method in the production of crystalline explosives
DE4237580C1 (de) * 1992-11-06 1994-03-17 Wasagchemie Sythen Gmbh Aufbereitung wachshaltiger Explosivstoffe
SE504054C2 (sv) * 1995-01-27 1996-10-28 Bofors Explosives Ab Flödesschema över återvinning av sprängämne
DE69727963T2 (de) * 1996-12-17 2004-07-22 Alliant Techsystems Inc., Edina Verfahren zur kristallisation von 2,4,6,8,10,12,-hexanitro-2,4,6,8,10,12,-hexaazatetrazyklo- [5.5.0.05,9 0 3,11]-dodecan durch ausfällen
US6214988B1 (en) 1999-01-03 2001-04-10 Schlumberger Technology Corporation Process for making an HMX product
US6201117B1 (en) 1999-05-26 2001-03-13 Schlumberger Technology Corporation Process for making a 1,3,5,7-tetraalkanoyl-1,3,5,7-tetraazacyclooctane
US6194571B1 (en) 1999-05-26 2001-02-27 Schlumberger Technology Corporation HMX compositions and processes for their preparation
US6265573B1 (en) 1999-05-26 2001-07-24 Schlumberger Technology Corporation Purification process
US6428724B1 (en) 1999-05-26 2002-08-06 Schlumberger Technology Corporation Granulation process
JP4530528B2 (ja) * 2000-12-11 2010-08-25 旭化成ケミカルズ株式会社 粉状火薬組成物の製法
NO318866B1 (no) * 2003-10-06 2005-05-18 Dyno Nobel Asa Pressbar plastisk bundet sprengstoffkomposisjon
GB2426755B (en) * 2005-06-02 2009-07-22 Saint Louis Inst Crystalline explosive form and preparation process thereof
FR2887544B1 (fr) * 2005-06-02 2008-07-18 Saint Louis Inst Particules d'explosif peu sensibles aux chocs et procede de traitement associe
FR2886641A1 (fr) * 2005-06-02 2006-12-08 Saint Louis Inst Particules d'explosif peu sensibles aux chocs et procede de traitement associe
US20060272756A1 (en) * 2005-06-06 2006-12-07 Schlumberger Technology Corporation RDX Composition and Process for Its Manufacture
JP2008189515A (ja) * 2007-02-05 2008-08-21 Nippon Koki Co Ltd 鈍感化爆薬組成物およびその製造方法
JP5253762B2 (ja) * 2007-06-07 2013-07-31 日本工機株式会社 Ｒｄｘの球状化方法
JP2009051692A (ja) * 2007-08-27 2009-03-12 Nippon Koki Co Ltd 多面体化したｒｄｘ、ｒｄｘの多面体化方法、球状化ｒｄｘの製造方法
RU2362758C1 (ru) * 2008-03-24 2009-07-27 Федеральное Казенное Предприятие "Бийский Олеумный Завод" Способ перекристаллизации октогена
US8002917B2 (en) 2009-02-09 2011-08-23 The United States Of America As Represented By The Secretary Of The Army Adjusting yield of a manufacturing process for energetic compounds through solubility modification
CN101955469A (zh) * 2010-09-17 2011-01-26 北京理工大学 一种奥克托今与黑索今混合物分离方法
CN101973947B (zh) * 2010-09-25 2015-12-09 北京理工大学 一种用结晶控制技术制备球形化黑索今的方法
JP5993241B2 (ja) * 2012-08-02 2016-09-14 中国化薬株式会社 Ｒｄｘの製造方法
CN102887870B (zh) * 2012-09-22 2015-07-15 山西北化关铝化工有限公司 导爆管用奥克托今
CN102887865A (zh) * 2012-09-22 2013-01-23 山西北化关铝化工有限公司 特质黑索今的制备方法
CN102887866B (zh) * 2012-09-22 2015-08-12 山西北化关铝化工有限公司 改性黑索今的生产方法
CN103044173B (zh) * 2012-12-06 2015-03-04 中国工程物理研究院化工材料研究所 一种有序多孔含能晶体材料的制备方法
CN103936534B (zh) * 2014-05-09 2016-07-06 北京理工大学 一种特质细化hmx晶体及制备方法
CN104294366B (zh) * 2014-10-11 2017-01-18 中北大学 一种厘米级奥克托今单晶的培养方法
RU2670231C1 (ru) * 2017-11-15 2018-10-19 Акционерное общество "Федеральный научно-производственный центр "Алтай" Способ перекристаллизации октогена
KR101999744B1 (ko) * 2017-12-29 2019-07-12 주식회사 한화 사이클로 트리메틸렌 트리나이트라민의 제조 방법
CN114230534B (zh) * 2021-11-23 2023-11-24 中北大学 一种声共振辅助溶剂侵蚀技术制备黑索今球晶方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2434230A (en) * 1948-01-06 Method of preparing i
CA816157A (en) * 1969-06-24 D. Evans Albert Crystallization of fine hmx
US2656355A (en) * 1953-10-20 Purification of cyclonite
DE681848C (de) * 1937-04-11 1939-09-15 Edmund Von Herz Verfahren zur Gewinnung von reinem Cyclotrimethylentrinitramin
US2959587A (en) * 1943-07-16 1960-11-08 John R Johnson Sensitivity control during purification of crude cyclonite
US3133054A (en) * 1962-03-07 1964-05-12 Eastman Kodak Co Processing of hmx
US3297681A (en) * 1964-02-26 1967-01-10 Eastman Kodak Co Crystallization of fine hmx
AU6718365A (en) * 1965-11-29 1967-06-01 Eastman Kodakcompany Crystallization of fine hmx
JPS4714112Y1 (ro) * 1969-07-08 1972-05-22
US4092383A (en) * 1977-08-15 1978-05-30 The United States Of America As Represented By The Secretary Of The Navy Modification of ballistic properties of HMX by spray drying

Also Published As

Publication number Publication date
NO851270L (no) 1985-10-07
JPS60226500A (ja) 1985-11-11
BR8501575A (pt) 1985-12-03
GB8506432D0 (en) 1985-04-17
AU567609B2 (en) 1987-11-26
IT1181872B (it) 1987-09-30
ES8608325A1 (es) 1986-07-16
SE8401857D0 (sv) 1984-04-04
AR240789A2 (es) 1991-02-28
GB2156805B (en) 1987-10-07
US4638065A (en) 1987-01-20
CA1243672A (en) 1988-10-25
AU4080685A (en) 1985-10-10
SE451718B (sv) 1987-10-26
SE8401857L (sv) 1985-10-05
IT8547908A0 (it) 1985-04-02
DE3510761A1 (de) 1985-10-17
GB2156805A (en) 1985-10-16
NO160775B (no) 1989-02-20
YU42385A (en) 1988-10-31
IN163711B (ro) 1988-10-29
YU45244B (en) 1992-05-28
AR240789A1 (es) 1991-02-28
RO93878A (ro) 1988-02-29
DE3510761C2 (de) 1997-03-06
JPH0471039B2 (ro) 1992-11-12
FR2562538A1 (fr) 1985-10-11
ES541846A0 (es) 1986-07-16
FR2562538B1 (fr) 1987-04-30

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