AR240789A2 - Procedimiento para recristalizar los altos explosivos hmx y rdx. - Google Patents
Procedimiento para recristalizar los altos explosivos hmx y rdx.Info
- Publication number
- AR240789A2 AR240789A2 AR29992885A AR29992885A AR240789A2 AR 240789 A2 AR240789 A2 AR 240789A2 AR 29992885 A AR29992885 A AR 29992885A AR 29992885 A AR29992885 A AR 29992885A AR 240789 A2 AR240789 A2 AR 240789A2
- Authority
- AR
- Argentina
- Prior art keywords
- hmx
- recrystallization
- rdx
- gamma
- temperature
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D257/00—Heterocyclic compounds containing rings having four nitrogen atoms as the only ring hetero atoms
- C07D257/02—Heterocyclic compounds containing rings having four nitrogen atoms as the only ring hetero atoms not condensed with other rings
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B25/00—Compositions containing a nitrated organic compound
- C06B25/34—Compositions containing a nitrated organic compound the compound being a nitrated acyclic, alicyclic or heterocyclic amine
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/40—Nitrogen atoms
- C07D251/54—Three nitrogen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Saccharide Compounds (AREA)
- Peptides Or Proteins (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Liquid Crystal Substances (AREA)
Abstract
UN PROCEDIMIENTO PARA RECRISTALIZAR LOS ALTOS EXPLOSIVOS HMX Y RDX, EN DONDE SE DISUELVEN A UNA TEMPERATURA DE POR LO MENOS 50 C LOS CRISTALES DE PARTIDA DE DICHOS EXPLOSIVOS HMX Y RDX EN LACTONA DE BAJO PESO MOLECULAR, LIQUIDA A LA TEMPERATURA AMBIENTE, Y CON MAS DE 3 ATOMOS DE CARBONO EN EL ANILLO, SELECCIONADA ENTRE GAMMA-BUTIROLACTONA, GAMMA-VALEROLACTONA, DELTA-VARELOLACTONA Y EPSILON-CAPROLACTONA, ENFRIAR PROGRESIVAMENTE HASTA ALCANZAR EL GRADO DE SATURACION DE LA SOLUCION OBTENIDA Y DEJAR FORMAR LOS NUEVOS CRISTALES DE LOS EXPLOSIVOS.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
SE8401857A SE451718B (sv) | 1984-04-04 | 1984-04-04 | Sett att omkristallisera sprengemnena oktogen och hexogen |
Publications (2)
Publication Number | Publication Date |
---|---|
AR240789A2 true AR240789A2 (es) | 1991-02-28 |
AR240789A1 AR240789A1 (es) | 1991-02-28 |
Family
ID=20355439
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AR299928A AR240789A1 (es) | 1984-04-04 | 1985-03-29 | Procedimiento para recristalizar los altos explosivos hmx y rdx. |
Country Status (16)
Country | Link |
---|---|
US (1) | US4638065A (es) |
JP (1) | JPS60226500A (es) |
AR (1) | AR240789A1 (es) |
AU (1) | AU567609B2 (es) |
BR (1) | BR8501575A (es) |
CA (1) | CA1243672A (es) |
DE (1) | DE3510761C2 (es) |
ES (1) | ES8608325A1 (es) |
FR (1) | FR2562538B1 (es) |
GB (1) | GB2156805B (es) |
IN (1) | IN163711B (es) |
IT (1) | IT1181872B (es) |
NO (1) | NO160775B (es) |
RO (1) | RO93878B (es) |
SE (1) | SE451718B (es) |
YU (1) | YU45244B (es) |
Families Citing this family (34)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3527200A1 (de) * | 1985-07-30 | 1987-03-19 | Horst Dipl Ing Hommel | Verfahren zum herstellen von sphaerolitischem kristallisat hoher schuett- und packungsdichte, insbesondere von kugelig kristallisiertem nitroguanidin |
DE3605634A1 (de) * | 1986-02-21 | 1987-08-27 | Messerschmitt Boelkow Blohm | Verfahren zur behandlung kristalliner sprengstoffe fuer hochleistungssprengladungen |
DE3617408C1 (de) * | 1986-05-23 | 1987-06-11 | Dynamit Nobel Ag | Verfahren zur Herstellung von feinkoernigem beta-Oktogen |
ES2053705T3 (es) * | 1987-04-22 | 1994-08-01 | Nobel Kemi Ab | Metodo para la fabricacion de explosivos cristalinos. |
DE4237580C1 (de) * | 1992-11-06 | 1994-03-17 | Wasagchemie Sythen Gmbh | Aufbereitung wachshaltiger Explosivstoffe |
SE504054C2 (sv) * | 1995-01-27 | 1996-10-28 | Bofors Explosives Ab | Flödesschema över återvinning av sprängämne |
WO1998027072A1 (en) * | 1996-12-17 | 1998-06-25 | Cordant Technologies, Inc. | Salting-out process of crystallizing 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.0?5,903,11¿]-dodecane |
US6214988B1 (en) | 1999-01-03 | 2001-04-10 | Schlumberger Technology Corporation | Process for making an HMX product |
US6428724B1 (en) | 1999-05-26 | 2002-08-06 | Schlumberger Technology Corporation | Granulation process |
US6201117B1 (en) | 1999-05-26 | 2001-03-13 | Schlumberger Technology Corporation | Process for making a 1,3,5,7-tetraalkanoyl-1,3,5,7-tetraazacyclooctane |
US6194571B1 (en) | 1999-05-26 | 2001-02-27 | Schlumberger Technology Corporation | HMX compositions and processes for their preparation |
US6265573B1 (en) | 1999-05-26 | 2001-07-24 | Schlumberger Technology Corporation | Purification process |
JP4530528B2 (ja) * | 2000-12-11 | 2010-08-25 | 旭化成ケミカルズ株式会社 | 粉状火薬組成物の製法 |
NO318866B1 (no) * | 2003-10-06 | 2005-05-18 | Dyno Nobel Asa | Pressbar plastisk bundet sprengstoffkomposisjon |
FR2886641A1 (fr) * | 2005-06-02 | 2006-12-08 | Saint Louis Inst | Particules d'explosif peu sensibles aux chocs et procede de traitement associe |
FR2887544B1 (fr) * | 2005-06-02 | 2008-07-18 | Saint Louis Inst | Particules d'explosif peu sensibles aux chocs et procede de traitement associe |
GB2426755B (en) * | 2005-06-02 | 2009-07-22 | Saint Louis Inst | Crystalline explosive form and preparation process thereof |
US20060272756A1 (en) * | 2005-06-06 | 2006-12-07 | Schlumberger Technology Corporation | RDX Composition and Process for Its Manufacture |
JP2008189515A (ja) * | 2007-02-05 | 2008-08-21 | Nippon Koki Co Ltd | 鈍感化爆薬組成物およびその製造方法 |
JP5253762B2 (ja) * | 2007-06-07 | 2013-07-31 | 日本工機株式会社 | Rdxの球状化方法 |
JP2009051692A (ja) * | 2007-08-27 | 2009-03-12 | Nippon Koki Co Ltd | 多面体化したrdx、rdxの多面体化方法、球状化rdxの製造方法 |
US8002917B2 (en) | 2009-02-09 | 2011-08-23 | The United States Of America As Represented By The Secretary Of The Army | Adjusting yield of a manufacturing process for energetic compounds through solubility modification |
CN101955469A (zh) * | 2010-09-17 | 2011-01-26 | 北京理工大学 | 一种奥克托今与黑索今混合物分离方法 |
CN101973947B (zh) * | 2010-09-25 | 2015-12-09 | 北京理工大学 | 一种用结晶控制技术制备球形化黑索今的方法 |
JP5993241B2 (ja) * | 2012-08-02 | 2016-09-14 | 中国化薬株式会社 | Rdxの製造方法 |
CN102887865A (zh) * | 2012-09-22 | 2013-01-23 | 山西北化关铝化工有限公司 | 特质黑索今的制备方法 |
CN102887870B (zh) * | 2012-09-22 | 2015-07-15 | 山西北化关铝化工有限公司 | 导爆管用奥克托今 |
CN102887866B (zh) * | 2012-09-22 | 2015-08-12 | 山西北化关铝化工有限公司 | 改性黑索今的生产方法 |
CN103044173B (zh) * | 2012-12-06 | 2015-03-04 | 中国工程物理研究院化工材料研究所 | 一种有序多孔含能晶体材料的制备方法 |
CN103936534B (zh) * | 2014-05-09 | 2016-07-06 | 北京理工大学 | 一种特质细化hmx晶体及制备方法 |
CN104294366B (zh) * | 2014-10-11 | 2017-01-18 | 中北大学 | 一种厘米级奥克托今单晶的培养方法 |
RU2670231C1 (ru) * | 2017-11-15 | 2018-10-19 | Акционерное общество "Федеральный научно-производственный центр "Алтай" | Способ перекристаллизации октогена |
KR101999744B1 (ko) * | 2017-12-29 | 2019-07-12 | 주식회사 한화 | 사이클로 트리메틸렌 트리나이트라민의 제조 방법 |
CN114230534B (zh) * | 2021-11-23 | 2023-11-24 | 中北大学 | 一种声共振辅助溶剂侵蚀技术制备黑索今球晶方法 |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2434230A (en) * | 1948-01-06 | Method of preparing i | ||
US2656355A (en) * | 1953-10-20 | Purification of cyclonite | ||
CA816157A (en) * | 1969-06-24 | D. Evans Albert | Crystallization of fine hmx | |
DE681848C (de) * | 1937-04-11 | 1939-09-15 | Edmund Von Herz | Verfahren zur Gewinnung von reinem Cyclotrimethylentrinitramin |
US2959587A (en) * | 1943-07-16 | 1960-11-08 | John R Johnson | Sensitivity control during purification of crude cyclonite |
US3133054A (en) * | 1962-03-07 | 1964-05-12 | Eastman Kodak Co | Processing of hmx |
US3297681A (en) * | 1964-02-26 | 1967-01-10 | Eastman Kodak Co | Crystallization of fine hmx |
AU6718365A (en) * | 1965-11-29 | 1967-06-01 | Eastman Kodakcompany | Crystallization of fine hmx |
JPS4714112Y1 (es) * | 1969-07-08 | 1972-05-22 | ||
US4092383A (en) * | 1977-08-15 | 1978-05-30 | The United States Of America As Represented By The Secretary Of The Navy | Modification of ballistic properties of HMX by spray drying |
-
1984
- 1984-04-04 SE SE8401857A patent/SE451718B/sv not_active Application Discontinuation
-
1985
- 1985-03-13 GB GB08506432A patent/GB2156805B/en not_active Expired
- 1985-03-15 IN IN216/DEL/85A patent/IN163711B/en unknown
- 1985-03-18 YU YU423/85A patent/YU45244B/xx unknown
- 1985-03-25 DE DE3510761A patent/DE3510761C2/de not_active Expired - Lifetime
- 1985-03-26 US US06/716,066 patent/US4638065A/en not_active Expired - Lifetime
- 1985-03-28 NO NO851270A patent/NO160775B/no unknown
- 1985-03-29 AR AR299928A patent/AR240789A1/es active
- 1985-04-02 JP JP60069862A patent/JPS60226500A/ja active Granted
- 1985-04-02 IT IT47908/85A patent/IT1181872B/it active
- 1985-04-02 ES ES541846A patent/ES8608325A1/es not_active Expired
- 1985-04-02 CA CA000478130A patent/CA1243672A/en not_active Expired
- 1985-04-02 RO RO118238A patent/RO93878B/ro unknown
- 1985-04-03 FR FR8505087A patent/FR2562538B1/fr not_active Expired
- 1985-04-03 AU AU40806/85A patent/AU567609B2/en not_active Ceased
- 1985-04-03 BR BR8501575A patent/BR8501575A/pt not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
CA1243672A (en) | 1988-10-25 |
SE451718B (sv) | 1987-10-26 |
NO160775B (no) | 1989-02-20 |
JPH0471039B2 (es) | 1992-11-12 |
GB2156805B (en) | 1987-10-07 |
DE3510761C2 (de) | 1997-03-06 |
ES541846A0 (es) | 1986-07-16 |
BR8501575A (pt) | 1985-12-03 |
IT1181872B (it) | 1987-09-30 |
JPS60226500A (ja) | 1985-11-11 |
RO93878B (ro) | 1988-03-01 |
SE8401857L (sv) | 1985-10-05 |
US4638065A (en) | 1987-01-20 |
IT8547908A0 (it) | 1985-04-02 |
GB2156805A (en) | 1985-10-16 |
IN163711B (es) | 1988-10-29 |
SE8401857D0 (sv) | 1984-04-04 |
GB8506432D0 (en) | 1985-04-17 |
ES8608325A1 (es) | 1986-07-16 |
YU42385A (en) | 1988-10-31 |
AR240789A1 (es) | 1991-02-28 |
FR2562538B1 (fr) | 1987-04-30 |
RO93878A (ro) | 1988-02-29 |
FR2562538A1 (fr) | 1985-10-11 |
YU45244B (en) | 1992-05-28 |
DE3510761A1 (de) | 1985-10-17 |
AU4080685A (en) | 1985-10-10 |
NO851270L (no) | 1985-10-07 |
AU567609B2 (en) | 1987-11-26 |
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