NO321276B1 - Fremgangsmate for fremstilling av triklorsilan og silisium for bruk ved fremstilling av triklorsilan - Google Patents
Fremgangsmate for fremstilling av triklorsilan og silisium for bruk ved fremstilling av triklorsilan Download PDFInfo
- Publication number
- NO321276B1 NO321276B1 NO20033093A NO20033093A NO321276B1 NO 321276 B1 NO321276 B1 NO 321276B1 NO 20033093 A NO20033093 A NO 20033093A NO 20033093 A NO20033093 A NO 20033093A NO 321276 B1 NO321276 B1 NO 321276B1
- Authority
- NO
- Norway
- Prior art keywords
- silicon
- chromium
- reactor
- trichlorosilane
- ppm
- Prior art date
Links
- 229910052710 silicon Inorganic materials 0.000 title claims abstract description 91
- 239000010703 silicon Substances 0.000 title claims abstract description 91
- ZDHXKXAHOVTTAH-UHFFFAOYSA-N trichlorosilane Chemical compound Cl[SiH](Cl)Cl ZDHXKXAHOVTTAH-UHFFFAOYSA-N 0.000 title claims abstract description 52
- 239000005052 trichlorosilane Substances 0.000 title claims abstract description 52
- 238000000034 method Methods 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title description 3
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims abstract description 90
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims abstract description 49
- 229910052804 chromium Inorganic materials 0.000 claims abstract description 46
- 239000011651 chromium Substances 0.000 claims abstract description 46
- 238000006243 chemical reaction Methods 0.000 claims abstract description 23
- 238000004519 manufacturing process Methods 0.000 claims abstract description 17
- 239000012535 impurity Substances 0.000 claims abstract description 5
- 239000000203 mixture Substances 0.000 claims description 10
- 229910052799 carbon Inorganic materials 0.000 claims description 6
- 239000007787 solid Substances 0.000 abstract description 2
- 238000002474 experimental method Methods 0.000 description 12
- 229910052698 phosphorus Inorganic materials 0.000 description 12
- 239000011574 phosphorus Substances 0.000 description 10
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 9
- 239000007789 gas Substances 0.000 description 9
- 239000002245 particle Substances 0.000 description 9
- 230000009257 reactivity Effects 0.000 description 9
- 150000004756 silanes Chemical class 0.000 description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 8
- 229910052782 aluminium Inorganic materials 0.000 description 5
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 4
- 238000011109 contamination Methods 0.000 description 4
- 238000010586 diagram Methods 0.000 description 4
- 239000010453 quartz Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- VXEGSRKPIUDPQT-UHFFFAOYSA-N 4-[4-(4-methoxyphenyl)piperazin-1-yl]aniline Chemical compound C1=CC(OC)=CC=C1N1CCN(C=2C=CC(N)=CC=2)CC1 VXEGSRKPIUDPQT-UHFFFAOYSA-N 0.000 description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 3
- 239000005049 silicon tetrachloride Substances 0.000 description 3
- 229910052786 argon Inorganic materials 0.000 description 2
- 229910052796 boron Inorganic materials 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 229910001510 metal chloride Inorganic materials 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 229910052719 titanium Inorganic materials 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 229910021420 polycrystalline silicon Inorganic materials 0.000 description 1
- 229920005591 polysilicon Polymers 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000011856 silicon-based particle Substances 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/08—Compounds containing halogen
- C01B33/107—Halogenated silanes
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/08—Compounds containing halogen
- C01B33/107—Halogenated silanes
- C01B33/1071—Tetrachloride, trichlorosilane or silicochloroform, dichlorosilane, monochlorosilane or mixtures thereof
- C01B33/10742—Tetrachloride, trichlorosilane or silicochloroform, dichlorosilane, monochlorosilane or mixtures thereof prepared by hydrochlorination of silicon or of a silicon-containing material
- C01B33/10757—Tetrachloride, trichlorosilane or silicochloroform, dichlorosilane, monochlorosilane or mixtures thereof prepared by hydrochlorination of silicon or of a silicon-containing material with the preferential formation of trichlorosilane
- C01B33/10763—Tetrachloride, trichlorosilane or silicochloroform, dichlorosilane, monochlorosilane or mixtures thereof prepared by hydrochlorination of silicon or of a silicon-containing material with the preferential formation of trichlorosilane from silicon
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/08—Compounds containing halogen
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Silicon Compounds (AREA)
- Catalysts (AREA)
Priority Applications (12)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NO20033093A NO321276B1 (no) | 2003-07-07 | 2003-07-07 | Fremgangsmate for fremstilling av triklorsilan og silisium for bruk ved fremstilling av triklorsilan |
| DE04748762T DE04748762T1 (de) | 2003-07-07 | 2004-06-24 | Verfahren zur herstellung von trichlorsilan und silicium zur verwendung bei der herstellung von trichlorsilan |
| JP2006518566A JP4778896B2 (ja) | 2003-07-07 | 2004-06-24 | トリクロルシランの製造法及びトリクロルシランの製造に使用する珪素 |
| AT04748762T ATE409678T1 (de) | 2003-07-07 | 2004-06-24 | Verfahren zur herstellung von trichlorsilan |
| CNB2004800196948A CN100349797C (zh) | 2003-07-07 | 2004-06-24 | 生产三氯硅烷的方法和用于生产三氯硅烷的硅 |
| ES04748762T ES2310741T3 (es) | 2003-07-07 | 2004-06-24 | Metodo para la produccion de triclorosilano. |
| KR1020067000260A KR100752810B1 (ko) | 2003-07-07 | 2004-06-24 | 트리클로로실란을 제조하는 방법 및 트리클로로실란의제조에서 사용되는 실리콘 |
| PCT/NO2004/000186 WO2005003030A1 (en) | 2003-07-07 | 2004-06-24 | Method for production of trichlorosilane and silicon for use in the production of trichlorosilane |
| EP04748762A EP1680357B1 (en) | 2003-07-07 | 2004-06-24 | Method for production of trichlorosilane |
| US10/563,781 US7462341B2 (en) | 2003-07-07 | 2004-06-24 | Method for production of trichlorosilane and silicon for use in the production of trichlorosilane |
| DE602004016876T DE602004016876D1 (de) | 2003-07-07 | 2004-06-24 | Verfahren zur herstellung von trichlorsilan |
| EA200600192A EA009060B1 (ru) | 2003-07-07 | 2004-06-24 | Способ получения трихлорсилана и кремния, используемого для получения трихлорсилана |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NO20033093A NO321276B1 (no) | 2003-07-07 | 2003-07-07 | Fremgangsmate for fremstilling av triklorsilan og silisium for bruk ved fremstilling av triklorsilan |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| NO20033093D0 NO20033093D0 (no) | 2003-07-07 |
| NO20033093L NO20033093L (no) | 2005-01-10 |
| NO321276B1 true NO321276B1 (no) | 2006-04-18 |
Family
ID=27800779
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO20033093A NO321276B1 (no) | 2003-07-07 | 2003-07-07 | Fremgangsmate for fremstilling av triklorsilan og silisium for bruk ved fremstilling av triklorsilan |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US7462341B2 (ru) |
| EP (1) | EP1680357B1 (ru) |
| JP (1) | JP4778896B2 (ru) |
| KR (1) | KR100752810B1 (ru) |
| CN (1) | CN100349797C (ru) |
| AT (1) | ATE409678T1 (ru) |
| DE (2) | DE602004016876D1 (ru) |
| EA (1) | EA009060B1 (ru) |
| ES (1) | ES2310741T3 (ru) |
| NO (1) | NO321276B1 (ru) |
| WO (1) | WO2005003030A1 (ru) |
Families Citing this family (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NO20043828L (no) * | 2004-09-13 | 2006-03-14 | Elkem As | Fremgangsmate for fremstilling av triklorsilan, fremgangsmate for fremstilling av silisium og silisium for bruk ved fremstilling av triklorsilan |
| NO20054402L (no) * | 2005-09-22 | 2007-03-23 | Elkem As | Method for production of trichlorosilane and silicon for use in the production of trichlorosilane |
| EP2371382B1 (en) | 2005-12-29 | 2016-03-02 | Boehringer Ingelheim Vetmedica, Inc. | Use of a PCV2 immunogenic composition for lessening clinical symptoms in pigs |
| KR101573933B1 (ko) * | 2008-02-29 | 2015-12-02 | 미쓰비시 마테리알 가부시키가이샤 | 트리클로로실란의 제조 방법 및 제조 장치 |
| US20100264362A1 (en) * | 2008-07-01 | 2010-10-21 | Yongchae Chee | Method of producing trichlorosilane (TCS) rich Chlorosilane product stably from a fluidized gas phase reactor (FBR) and the structure of the reactor |
| DE102008041974A1 (de) | 2008-09-10 | 2010-03-11 | Evonik Degussa Gmbh | Vorrichtung, deren Verwendung und ein Verfahren zur energieautarken Hydrierung von Chlorsilanen |
| WO2010074673A1 (en) * | 2008-12-23 | 2010-07-01 | Arise Technologies Corporation | Method and apparatus for the production of chlorosilanes |
| KR101687833B1 (ko) * | 2009-01-20 | 2016-12-19 | 미쓰비시 마테리알 가부시키가이샤 | 트리클로로실란 제조 장치 및 트리클로로실란 제조 방법 |
| US8168123B2 (en) * | 2009-02-26 | 2012-05-01 | Siliken Chemicals, S.L. | Fluidized bed reactor for production of high purity silicon |
| WO2010123869A1 (en) * | 2009-04-20 | 2010-10-28 | Ae Polysilicon Corporation | Methods and system for cooling a reaction effluent gas |
| JP2012523963A (ja) | 2009-04-20 | 2012-10-11 | エーイー ポリシリコン コーポレーション | ケイ化物がコーティングされた金属表面を有する反応器 |
| NO20100358A1 (no) * | 2010-03-12 | 2011-09-13 | Elkem As | Fremgangsmate for fremstilling av triklorsilan fra silisium, hydrogen og silisiumtetraklorid |
| NO334216B1 (no) * | 2010-08-13 | 2014-01-13 | Elkem As | Fremgangsmåte for fremstilling av triklorsilan og silisium for bruk ved fremstilling av triklorsilan |
| EP2825506A4 (en) * | 2012-03-14 | 2015-12-02 | Sitec Gmbh | PRODUCTION OF TRICHLOROSILANE |
| US8875728B2 (en) | 2012-07-12 | 2014-11-04 | Siliken Chemicals, S.L. | Cooled gas distribution plate, thermal bridge breaking system, and related methods |
| EP2969948A1 (en) * | 2013-03-13 | 2016-01-20 | SiTec GmbH | Temperature management in chlorination processes and systems related thereto |
| DE102013215011A1 (de) | 2013-07-31 | 2015-02-05 | Wacker Chemie Ag | Verfahren zur Herstellung von Trichlorsilan |
| KR101580171B1 (ko) | 2014-01-23 | 2015-12-24 | 한국화학연구원 | 금속 실리사이드 표면개질 방법, 표면개질된 금속 실리사이드를 이용한 삼염화실란의 제조방법 및 제조장치 |
| US10040689B2 (en) * | 2014-12-19 | 2018-08-07 | Dow Silicones Corporation | Process for preparing monohydrogentrihalosilanes |
| JP2022534930A (ja) * | 2019-05-29 | 2022-08-04 | ワッカー ケミー アクチエンゲゼルシャフト | 構造最適化シリコン粒子を有するトリクロロシランを生成するための方法 |
| JP7278888B2 (ja) * | 2019-06-28 | 2023-05-22 | 高純度シリコン株式会社 | トリクロロシランの製造方法 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2380995A (en) * | 1941-09-26 | 1945-08-07 | Gen Electric | Preparation of organosilicon halides |
| US4247528A (en) * | 1979-04-11 | 1981-01-27 | Dow Corning Corporation | Method for producing solar-cell-grade silicon |
| US4585643A (en) * | 1985-05-31 | 1986-04-29 | Union Carbide Corporation | Process for preparing chlorosilanes from silicon and hydrogen chloride using an oxygen promoter |
| DE3809784C1 (ru) * | 1988-03-23 | 1989-07-13 | Huels Ag, 4370 Marl, De | |
| KR950002860B1 (ko) * | 1992-06-13 | 1995-03-27 | 한국과학기술연구원 | 클로로알켄닐실란들과그제조방법 |
| US5871705A (en) * | 1996-09-19 | 1999-02-16 | Tokuyama Corporation | Process for producing trichlorosilane |
| DE19645359A1 (de) * | 1996-11-04 | 1998-05-07 | Bayer Ag | Verfahren zur Herstellung von Alkylhalogensilanen |
| DE10063863A1 (de) | 2000-12-21 | 2003-07-10 | Solarworld Ag | Wirbelbettreaktor für die Trichlorsilansynthese |
| JP3812642B2 (ja) * | 2001-02-14 | 2006-08-23 | 信越化学工業株式会社 | オルガノハロシランの製造方法 |
| DE10118483C1 (de) * | 2001-04-12 | 2002-04-18 | Wacker Chemie Gmbh | Staubrückführung bei der Direktsynthese von Chlor- und Methylchlorsilanen in Wirbelschicht |
| NO314138B1 (no) * | 2001-08-27 | 2003-02-03 | Elkem Materials | Fremgangsmåte for fjerning av forurensinger fra silisiuminneholdende residuer |
| US7780938B2 (en) * | 2006-04-13 | 2010-08-24 | Cabot Corporation | Production of silicon through a closed-loop process |
-
2003
- 2003-07-07 NO NO20033093A patent/NO321276B1/no not_active IP Right Cessation
-
2004
- 2004-06-24 EP EP04748762A patent/EP1680357B1/en not_active Revoked
- 2004-06-24 CN CNB2004800196948A patent/CN100349797C/zh not_active Expired - Fee Related
- 2004-06-24 JP JP2006518566A patent/JP4778896B2/ja not_active Expired - Fee Related
- 2004-06-24 ES ES04748762T patent/ES2310741T3/es active Active
- 2004-06-24 DE DE602004016876T patent/DE602004016876D1/de active Active
- 2004-06-24 DE DE04748762T patent/DE04748762T1/de active Pending
- 2004-06-24 KR KR1020067000260A patent/KR100752810B1/ko not_active IP Right Cessation
- 2004-06-24 US US10/563,781 patent/US7462341B2/en not_active Expired - Fee Related
- 2004-06-24 WO PCT/NO2004/000186 patent/WO2005003030A1/en active Application Filing
- 2004-06-24 EA EA200600192A patent/EA009060B1/ru not_active IP Right Cessation
- 2004-06-24 AT AT04748762T patent/ATE409678T1/de active
Also Published As
| Publication number | Publication date |
|---|---|
| EA200600192A1 (ru) | 2006-06-30 |
| CN1819971A (zh) | 2006-08-16 |
| KR100752810B1 (ko) | 2007-08-29 |
| EA009060B1 (ru) | 2007-10-26 |
| ES2310741T3 (es) | 2009-01-16 |
| NO20033093L (no) | 2005-01-10 |
| DE602004016876D1 (de) | 2008-11-13 |
| DE04748762T1 (de) | 2007-06-06 |
| WO2005003030A1 (en) | 2005-01-13 |
| ATE409678T1 (de) | 2008-10-15 |
| EP1680357A1 (en) | 2006-07-19 |
| CN100349797C (zh) | 2007-11-21 |
| JP2007527352A (ja) | 2007-09-27 |
| JP4778896B2 (ja) | 2011-09-21 |
| US20070086936A1 (en) | 2007-04-19 |
| NO20033093D0 (no) | 2003-07-07 |
| KR20060056306A (ko) | 2006-05-24 |
| US7462341B2 (en) | 2008-12-09 |
| EP1680357B1 (en) | 2008-10-01 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM1K | Lapsed by not paying the annual fees |