NL1030346A1 - Semipermeabel composietmembraan, productiewerkwijze daarvan, en element, fluïdumscheidingsinstallatie en werkwijze voor behandeling van water onder toepassing van hetzelfde. - Google Patents
Semipermeabel composietmembraan, productiewerkwijze daarvan, en element, fluïdumscheidingsinstallatie en werkwijze voor behandeling van water onder toepassing van hetzelfde.Info
- Publication number
- NL1030346A1 NL1030346A1 NL1030346A NL1030346A NL1030346A1 NL 1030346 A1 NL1030346 A1 NL 1030346A1 NL 1030346 A NL1030346 A NL 1030346A NL 1030346 A NL1030346 A NL 1030346A NL 1030346 A1 NL1030346 A1 NL 1030346A1
- Authority
- NL
- Netherlands
- Prior art keywords
- semi
- treatment
- water
- same
- composite membrane
- Prior art date
Links
- 239000002131 composite material Substances 0.000 title 1
- 239000012530 fluid Substances 0.000 title 1
- 238000004519 manufacturing process Methods 0.000 title 1
- 239000012528 membrane Substances 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- 238000000926 separation method Methods 0.000 title 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
- B01D67/0081—After-treatment of organic or inorganic membranes
- B01D67/0088—Physical treatment with compounds, e.g. swelling, coating or impregnation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D65/00—Accessories or auxiliary operations, in general, for separation processes or apparatus using semi-permeable membranes
- B01D65/10—Testing of membranes or membrane apparatus; Detecting or repairing leaks
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
- B01D67/0002—Organic membrane manufacture
- B01D67/0006—Organic membrane manufacture by chemical reactions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
- B01D67/0081—After-treatment of organic or inorganic membranes
- B01D67/0093—Chemical modification
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
- B01D67/0081—After-treatment of organic or inorganic membranes
- B01D67/0093—Chemical modification
- B01D67/00931—Chemical modification by introduction of specific groups after membrane formation, e.g. by grafting
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
- B01D69/02—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor characterised by their properties
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
- B01D69/10—Supported membranes; Membrane supports
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
- B01D69/12—Composite membranes; Ultra-thin membranes
- B01D69/1213—Laminated layers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
- B01D69/12—Composite membranes; Ultra-thin membranes
- B01D69/122—Separate manufacturing of ultra-thin membranes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
- B01D69/12—Composite membranes; Ultra-thin membranes
- B01D69/125—In situ manufacturing by polymerisation, polycondensation, cross-linking or chemical reaction
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
- B01D71/06—Organic material
- B01D71/56—Polyamides, e.g. polyester-amides
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
- C02F1/441—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by reverse osmosis
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2323/00—Details relating to membrane preparation
- B01D2323/15—Use of additives
- B01D2323/216—Surfactants
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2323/00—Details relating to membrane preparation
- B01D2323/15—Use of additives
- B01D2323/218—Additive materials
- B01D2323/2182—Organic additives
- B01D2323/21827—Salts
- B01D2323/21828—Ammonium Salts
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2323/00—Details relating to membrane preparation
- B01D2323/15—Use of additives
- B01D2323/218—Additive materials
- B01D2323/2182—Organic additives
- B01D2323/21839—Polymeric additives
- B01D2323/2185—Polyethylene glycol
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2323/00—Details relating to membrane preparation
- B01D2323/30—Cross-linking
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2325/00—Details relating to properties of membranes
- B01D2325/02—Details relating to pores or porosity of the membranes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2325/00—Details relating to properties of membranes
- B01D2325/02—Details relating to pores or porosity of the membranes
- B01D2325/0283—Pore size
- B01D2325/02834—Pore size more than 0.1 and up to 1 µm
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2325/00—Details relating to properties of membranes
- B01D2325/20—Specific permeability or cut-off range
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/10—Inorganic compounds
- C02F2101/108—Boron compounds
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
- C02F2103/08—Seawater, e.g. for desalination
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A20/00—Water conservation; Efficient water supply; Efficient water use
- Y02A20/124—Water desalination
- Y02A20/131—Reverse-osmosis
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2004330273 | 2004-11-15 | ||
JP2004330273 | 2004-11-15 |
Publications (2)
Publication Number | Publication Date |
---|---|
NL1030346A1 true NL1030346A1 (nl) | 2006-05-16 |
NL1030346C2 NL1030346C2 (nl) | 2006-09-20 |
Family
ID=35502480
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
NL1030346A NL1030346C2 (nl) | 2004-11-15 | 2005-11-03 | Semipermeabel composietmembraan, productiewerkwijze daarvan, en element, fluïdumscheidingsinstallatie en werkwijze voor behandeling van water onder toepassing van hetzelfde. |
Country Status (9)
Country | Link |
---|---|
US (1) | US7641054B2 (nl) |
EP (1) | EP1812149B1 (nl) |
JP (1) | JP5205966B2 (nl) |
KR (1) | KR101165117B1 (nl) |
CN (1) | CN101056695B (nl) |
AU (1) | AU2005303043B2 (nl) |
ES (1) | ES2423494T3 (nl) |
NL (1) | NL1030346C2 (nl) |
WO (1) | WO2006051888A1 (nl) |
Families Citing this family (37)
Publication number | Priority date | Publication date | Assignee | Title |
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JP5200535B2 (ja) * | 2005-12-16 | 2013-06-05 | 東レ株式会社 | 複合半透膜、その製造方法 |
US20070227966A1 (en) * | 2006-03-31 | 2007-10-04 | Koo Ja-Young | Composite polyamide reverse osmosis membrane showing high boron rejection and method of producing the same |
US7882963B2 (en) * | 2006-05-12 | 2011-02-08 | Dow Global Technologies Inc. | Modified membrane |
CN101605592B (zh) * | 2007-02-05 | 2011-10-12 | 陶氏环球技术公司 | 改性的聚酰胺膜 |
US20080202210A1 (en) * | 2007-02-28 | 2008-08-28 | Varian, Inc. | Test gas leak detection using a composite membrane |
EP2327469A4 (en) * | 2008-09-12 | 2015-09-16 | Toray Industries | Semi-transparent composite film and method for its production |
US7815987B2 (en) * | 2008-12-04 | 2010-10-19 | Dow Global Technologies Inc. | Polyamide membrane with coating of polyalkylene oxide and polyacrylamide compounds |
US20110049055A1 (en) | 2009-08-31 | 2011-03-03 | General Electric Company | Reverse osmosis composite membranes for boron removal |
BR112012007129B1 (pt) * | 2009-09-29 | 2019-07-02 | Kurita Water Industries Ltd | Membrana permeável, e método para melhorar sua rejeição |
WO2011078131A1 (ja) * | 2009-12-22 | 2011-06-30 | 東レ株式会社 | 半透膜およびその製造方法 |
CN102781560B (zh) * | 2010-02-23 | 2015-05-20 | 东丽株式会社 | 复合半透膜及其制造方法 |
WO2011112351A1 (en) * | 2010-03-10 | 2011-09-15 | Dow Global Technologies Llc | Polyamide membrane with a coating comprising polyalkylene oxide and acetophenone compounds |
WO2011136865A1 (en) | 2010-04-26 | 2011-11-03 | Dow Global Technologies Llc | Polyamide membrane with a coating comprising polyalkylene oxide and triazine compounds |
US8733558B2 (en) | 2010-05-24 | 2014-05-27 | Dow Global Technologies Llc | Composite membrane with coating comprising polyalkylene oxide and biguanide-type compounds |
US8757396B2 (en) | 2010-05-24 | 2014-06-24 | Dow Global Technologies Llc | Composite membrane with coating comprising polyalkylene oxide and oxy-substituted phenyl compounds |
WO2011149572A1 (en) | 2010-05-24 | 2011-12-01 | Dow Global Technologies Llc | Polyamide membrane with coating comprising polyalkylene oxide and imidazol compounds |
AR084006A1 (es) * | 2010-12-01 | 2013-04-17 | Toray Industries | Procedimiento para la separacion y recuperacion de una sal de metal alcalino purificada |
CL2011000862A1 (es) * | 2011-04-15 | 2012-01-27 | Univ De Tarapaca | Metodo para aumentar la eficiencia en el rechazo de b en sistemas de desalinizacion por osmosis inversa, el cual es modificado de modo que permita la adiccion y mezcla de un compuesto polihidroxilado soluble en agua, antes que pase por las membranas. |
JP6032011B2 (ja) * | 2011-09-29 | 2016-11-24 | 東レ株式会社 | 複合半透膜 |
WO2013108788A1 (ja) * | 2012-01-16 | 2013-07-25 | 東レ株式会社 | 複合半透膜およびその製造方法 |
WO2014003140A1 (ja) * | 2012-06-27 | 2014-01-03 | 東レ株式会社 | 複合半透膜および複合半透膜エレメント |
US9833751B2 (en) | 2013-06-07 | 2017-12-05 | Lg Chem, Ltd. | Polyamide water-treatment separation membrane having superior oxidation resistance and chlorine resistance properties, and method of manufacturing the same |
JP5733351B2 (ja) * | 2013-07-22 | 2015-06-10 | 栗田工業株式会社 | ホウ素含有水の処理方法及び装置 |
US10384167B2 (en) | 2013-11-21 | 2019-08-20 | Oasys Water LLC | Systems and methods for improving performance of osmotically driven membrane systems |
CN106257977B (zh) * | 2014-04-28 | 2019-10-29 | 陶氏环球技术有限责任公司 | 用亚硝酸后处理的复合聚酰胺膜 |
JPWO2016002819A1 (ja) * | 2014-06-30 | 2017-04-27 | 東レ株式会社 | 複合半透膜 |
CN106659986A (zh) * | 2014-06-30 | 2017-05-10 | 东丽株式会社 | 复合半透膜 |
WO2017052256A1 (ko) * | 2015-09-23 | 2017-03-30 | 주식회사 엘지화학 | 수처리 분리막 및 이의 제조방법 |
SG11201804988PA (en) | 2015-12-17 | 2018-07-30 | Univ Singapore Technology & Design | Boron removal and measurement in aqueous solutions |
WO2017104824A1 (ja) * | 2015-12-18 | 2017-06-22 | 東レ株式会社 | 複合半透膜および複合半透膜の製造方法 |
CN105771672B (zh) * | 2016-04-18 | 2018-03-02 | 天津工业大学 | 一种抗污染抗菌芳香聚酰胺反渗透复合膜及制备方法 |
KR102309602B1 (ko) * | 2017-03-22 | 2021-10-05 | 도레이첨단소재 주식회사 | 고염배제율 역삼투막 및 그 제조방법 |
KR102309603B1 (ko) * | 2017-03-22 | 2021-10-05 | 도레이첨단소재 주식회사 | 고염배제율 역삼투막 및 그 제조방법 |
WO2018194354A2 (ko) * | 2017-04-19 | 2018-10-25 | 주식회사 엘지화학 | 수처리 분리막 및 이의 제조방법 |
CN109692579A (zh) * | 2017-10-20 | 2019-04-30 | 中国石油化工股份有限公司 | 反渗透膜及其制备方法和应用 |
US10124297B1 (en) | 2018-03-06 | 2018-11-13 | Kuwait Institute For Scientific Research | Thin film nanocomposite nanofiltration membrane |
CN111437734B (zh) * | 2020-05-09 | 2022-04-19 | 中国乐凯集团有限公司 | 超疏水耐溶剂复合纳滤膜及其制备方法 |
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JPS59115704A (ja) | 1982-12-24 | 1984-07-04 | Toray Ind Inc | 半透膜の処理法 |
US4758343A (en) * | 1985-09-20 | 1988-07-19 | Toray Industries, Inc. | Interfacially synthesized reverse osmosis membrane |
JPS62110706A (ja) | 1985-11-08 | 1987-05-21 | Toray Ind Inc | 逆浸透法における膜処理法 |
US4948506A (en) * | 1986-07-07 | 1990-08-14 | Bend Research, Inc. | Physicochemically functional ultrathin films by interfacial polymerization |
US4895660A (en) * | 1986-07-14 | 1990-01-23 | The Dow Chemical Company | Water-soluble aromatic polyamides and polyureas |
US5057421A (en) * | 1987-03-16 | 1991-10-15 | Brunswick Corporation | Thin film membrane enzyme/coemzyme reactor and method of using same |
US4769148A (en) * | 1987-11-18 | 1988-09-06 | The Dow Chemical Company | Novel polyamide reverse osmosis membranes |
JPH01180208A (ja) | 1988-01-11 | 1989-07-18 | Toray Ind Inc | 複合半透膜の製造方法およびその膜 |
JP2727594B2 (ja) | 1988-10-25 | 1998-03-11 | 東レ株式会社 | 複合半透膜の製造方法 |
US4964998A (en) * | 1989-12-13 | 1990-10-23 | Filmtec Corporation | Use of treated composite polyamide membranes to separate concentrated solute |
US4960518A (en) * | 1989-12-13 | 1990-10-02 | The Filmtec Corporation | Treatment of composite polyamide membranes with compatible oxidants |
JP3031763B2 (ja) | 1990-09-14 | 2000-04-10 | 日東電工株式会社 | 複合逆浸透膜およびその製造方法 |
US5234598A (en) * | 1992-05-13 | 1993-08-10 | Allied-Signal Inc. | Thin-film composite membrane |
US5614099A (en) * | 1994-12-22 | 1997-03-25 | Nitto Denko Corporation | Highly permeable composite reverse osmosis membrane, method of producing the same, and method of using the same |
JP3023300B2 (ja) * | 1994-12-22 | 2000-03-21 | 日東電工株式会社 | 高透過性複合逆浸透膜とその製造方法及び逆浸透処理方法 |
JPH0938469A (ja) * | 1995-08-02 | 1997-02-10 | Nitto Denko Corp | 高透過性複合逆浸透膜 |
JPH1119493A (ja) | 1997-07-03 | 1999-01-26 | Nitto Denko Corp | 逆浸透膜モジュ−ル及び海水の処理方法 |
JP4284767B2 (ja) * | 1998-10-05 | 2009-06-24 | 東レ株式会社 | 複合半透膜およびそれを用いた造水方法、流体分離素子 |
DE69920419T2 (de) * | 1999-01-14 | 2006-02-23 | Toray Industries, Inc. | Semipermeable verbundmembran, verfahren zu ihrer herstellung und verfahren zur reinigung von wasser mit hilfe derselben |
EP1157734B1 (en) * | 1999-09-28 | 2009-06-10 | Toray Industries, Inc. | Process for producing composite semipermeable membrane |
JP4289757B2 (ja) * | 2000-03-23 | 2009-07-01 | 日東電工株式会社 | 複合逆浸透膜の製造方法 |
US6337018B1 (en) * | 2000-04-17 | 2002-01-08 | The Dow Chemical Company | Composite membrane and method for making the same |
JP2001327840A (ja) * | 2000-05-25 | 2001-11-27 | Toray Ind Inc | 複合半透膜およびその製造方法 |
JP2002095940A (ja) * | 2000-09-21 | 2002-04-02 | Nitto Denko Corp | 複合逆浸透膜とその製造方法及びその使用方法 |
JP2002224546A (ja) * | 2000-11-29 | 2002-08-13 | Toray Ind Inc | 下水処理用複合半透膜およびその製造方法 |
US6913694B2 (en) * | 2001-11-06 | 2005-07-05 | Saehan Industries Incorporation | Selective membrane having a high fouling resistance |
JP3885565B2 (ja) * | 2001-11-20 | 2007-02-21 | 東レ株式会社 | 複合半透膜およびその製造方法 |
JP3975933B2 (ja) * | 2003-02-13 | 2007-09-12 | 東レ株式会社 | 複合半透膜および下水処理方法 |
-
2005
- 2005-11-03 NL NL1030346A patent/NL1030346C2/nl not_active IP Right Cessation
- 2005-11-04 ES ES05803380T patent/ES2423494T3/es active Active
- 2005-11-04 WO PCT/JP2005/020670 patent/WO2006051888A1/en active Application Filing
- 2005-11-04 JP JP2007522740A patent/JP5205966B2/ja not_active Expired - Fee Related
- 2005-11-04 CN CN2005800390088A patent/CN101056695B/zh not_active Expired - Fee Related
- 2005-11-04 US US11/666,752 patent/US7641054B2/en not_active Expired - Fee Related
- 2005-11-04 KR KR1020077013569A patent/KR101165117B1/ko not_active IP Right Cessation
- 2005-11-04 AU AU2005303043A patent/AU2005303043B2/en not_active Ceased
- 2005-11-04 EP EP05803380.4A patent/EP1812149B1/en not_active Not-in-force
Also Published As
Publication number | Publication date |
---|---|
AU2005303043B2 (en) | 2010-08-05 |
KR101165117B1 (ko) | 2012-07-12 |
CN101056695A (zh) | 2007-10-17 |
JP2008519673A (ja) | 2008-06-12 |
EP1812149B1 (en) | 2013-06-12 |
US7641054B2 (en) | 2010-01-05 |
EP1812149A1 (en) | 2007-08-01 |
NL1030346C2 (nl) | 2006-09-20 |
US20080000843A1 (en) | 2008-01-03 |
KR20070086268A (ko) | 2007-08-27 |
JP5205966B2 (ja) | 2013-06-05 |
AU2005303043A1 (en) | 2006-05-18 |
CN101056695B (zh) | 2011-01-26 |
WO2006051888A1 (en) | 2006-05-18 |
ES2423494T3 (es) | 2013-09-20 |
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