MX354153B - Proceso para la preparacion de metionina. - Google Patents
Proceso para la preparacion de metionina.Info
- Publication number
- MX354153B MX354153B MX2014011130A MX2014011130A MX354153B MX 354153 B MX354153 B MX 354153B MX 2014011130 A MX2014011130 A MX 2014011130A MX 2014011130 A MX2014011130 A MX 2014011130A MX 354153 B MX354153 B MX 354153B
- Authority
- MX
- Mexico
- Prior art keywords
- methionine
- solution
- recrystallization
- takes place
- separated
- Prior art date
Links
- FFEARJCKVFRZRR-BYPYZUCNSA-N L-methionine Chemical compound CSCC[C@H](N)C(O)=O FFEARJCKVFRZRR-BYPYZUCNSA-N 0.000 title abstract 6
- 229930182817 methionine Natural products 0.000 title abstract 6
- 238000000034 method Methods 0.000 title abstract 2
- 238000002360 preparation method Methods 0.000 title abstract 2
- 229960004452 methionine Drugs 0.000 abstract 5
- 239000000243 solution Substances 0.000 abstract 4
- 238000001953 recrystallisation Methods 0.000 abstract 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 abstract 2
- 239000000654 additive Substances 0.000 abstract 2
- 230000000996 additive effect Effects 0.000 abstract 2
- 239000003945 anionic surfactant Substances 0.000 abstract 2
- 238000002425 crystallisation Methods 0.000 abstract 2
- 230000008025 crystallization Effects 0.000 abstract 2
- 239000002736 nonionic surfactant Substances 0.000 abstract 2
- 239000000725 suspension Substances 0.000 abstract 2
- SBKRXUMXMKBCLD-UHFFFAOYSA-N 5-(2-methylsulfanylethyl)imidazolidine-2,4-dione Chemical compound CSCCC1NC(=O)NC1=O SBKRXUMXMKBCLD-UHFFFAOYSA-N 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 229910002092 carbon dioxide Inorganic materials 0.000 abstract 1
- 239000001569 carbon dioxide Substances 0.000 abstract 1
- 230000007062 hydrolysis Effects 0.000 abstract 1
- 238000006460 hydrolysis reaction Methods 0.000 abstract 1
- FFEARJCKVFRZRR-UHFFFAOYSA-N methionine Chemical compound CSCCC(N)C(O)=O FFEARJCKVFRZRR-UHFFFAOYSA-N 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 229910001414 potassium ion Inorganic materials 0.000 abstract 1
- CDWZRHFHYAOGGK-WCCKRBBISA-M potassium;(2s)-2-amino-4-methylsulfanylbutanoate Chemical compound [K+].CSCC[C@H](N)C([O-])=O CDWZRHFHYAOGGK-WCCKRBBISA-M 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
- C07C319/26—Separation; Purification; Stabilisation; Use of additives
- C07C319/28—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
- C07C319/02—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols
- C07C319/12—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols by reactions not involving the formation of mercapto groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
- C07C319/14—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides
- C07C319/20—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of sulfides by reactions not involving the formation of sulfide groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
- C07C319/26—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
- C07C323/50—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton
- C07C323/51—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton
- C07C323/52—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being acyclic and saturated
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/141—Feedstock
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Degasification And Air Bubble Elimination (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP12160257.7A EP2641898A1 (de) | 2012-03-20 | 2012-03-20 | Verfahren zur Herstellung von Methionin |
| PCT/EP2013/053795 WO2013139562A1 (en) | 2012-03-20 | 2013-02-26 | Process for the preparation of methionine |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MX2014011130A MX2014011130A (es) | 2014-12-10 |
| MX354153B true MX354153B (es) | 2018-02-15 |
Family
ID=47749849
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2014011130A MX354153B (es) | 2012-03-20 | 2013-02-26 | Proceso para la preparacion de metionina. |
Country Status (12)
| Country | Link |
|---|---|
| US (2) | US9156782B2 (de) |
| EP (3) | EP2641898A1 (de) |
| JP (1) | JP6143840B2 (de) |
| KR (1) | KR101988692B1 (de) |
| CN (2) | CN104203912B (de) |
| BR (1) | BR112014023279B1 (de) |
| ES (1) | ES2662937T3 (de) |
| MX (1) | MX354153B (de) |
| MY (1) | MY167899A (de) |
| RU (1) | RU2640656C2 (de) |
| SG (1) | SG11201405870SA (de) |
| WO (1) | WO2013139562A1 (de) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2678312B1 (de) | 2011-02-23 | 2017-10-11 | Evonik Degussa GmbH | Verfahren zur herstellung von 2-hydroxy-4-(methylthio)buttersäurenitril aus 3-(methylthio)propanal und cyanwasserstoff |
| US9822051B2 (en) | 2013-06-03 | 2017-11-21 | Evonik Degussa Gmbh | Method for producing acrolein |
| EP2848607A1 (de) * | 2013-09-17 | 2015-03-18 | Evonik Industries AG | Verfahren zur Gewinnung von Methionin |
| CN104744326B (zh) | 2015-02-12 | 2016-08-10 | 山东新和成氨基酸有限公司 | 一种连续制备高堆积密度甲硫氨酸结晶的方法 |
| CN106008297B (zh) * | 2016-06-03 | 2018-11-30 | 宁夏紫光天化蛋氨酸有限责任公司 | 一种蛋氨酸新晶型ⅱ及其制备方法 |
| CN106083675B (zh) * | 2016-06-03 | 2018-07-27 | 宁夏紫光天化蛋氨酸有限责任公司 | 一种蛋氨酸新晶型i及其制备方法 |
| KR20180078621A (ko) | 2016-12-30 | 2018-07-10 | 씨제이제일제당 (주) | 결정화 기술을 이용한 l-메티오닌 결정의 제조방법 |
| US10829447B2 (en) | 2017-04-27 | 2020-11-10 | Sumitomo Chemical Company, Limited | Methionine production method and production equipment |
| US10919848B2 (en) * | 2017-05-15 | 2021-02-16 | Evonik Operations Gmbh | Process for preparing methionine |
| CN109384696A (zh) * | 2017-08-03 | 2019-02-26 | 宁夏紫光天化蛋氨酸有限责任公司 | 一种获得高纯度高堆积密度蛋氨酸的方法 |
| US12195422B2 (en) * | 2019-06-18 | 2025-01-14 | Evonik Operations Gmbh | Process for the preparation of D,L-methionine |
| CN111100051B (zh) | 2019-12-31 | 2022-01-28 | 山东新和成氨基酸有限公司 | 在甲硫氨酸制备过程中使用的添加剂及甲硫氨酸的制备方法 |
| US20230391720A1 (en) | 2020-10-13 | 2023-12-07 | Evonik Operations Gmbh | D,l-methionine with an optimized particle size distribution |
| CN112679397B (zh) * | 2020-12-21 | 2023-08-01 | 宁夏紫光天化蛋氨酸有限责任公司 | 一种dl-蛋氨酸的制备方法 |
| EP4023637A1 (de) * | 2020-12-30 | 2022-07-06 | Evonik Operations GmbH | Verfahren zur diastereomerenreinen herstellung von dl/ld-methionyl-methionin |
| CN114920675B (zh) * | 2022-04-20 | 2024-02-06 | 天津大学 | 一种蛋氨酸晶体及其制备方法和应用 |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4619610B1 (de) * | 1966-08-25 | 1971-06-01 | ||
| JPS4619610Y1 (de) | 1968-09-16 | 1971-07-08 | ||
| JPS5921732A (ja) * | 1982-07-28 | 1984-02-03 | ユニチカ株式会社 | 強撚糸調特殊複合糸の製造方法 |
| JPH0619610A (ja) | 1992-07-03 | 1994-01-28 | Fuji Elelctrochem Co Ltd | 故障診断装置付き座標入力装置 |
| FR2708267B1 (fr) * | 1993-07-28 | 1995-09-01 | Rhone Poulenc Nutrition Animal | Méthode de cristallisation de la méthionine. |
| DE19547236A1 (de) | 1995-12-18 | 1997-07-03 | Degussa | Verfahren zur Herstellung von D,L-Methionin oder dessen Salz |
| JP3947269B2 (ja) | 1997-05-06 | 2007-07-18 | 日本曹達株式会社 | 粒状ｄｌ−メチオニン結晶およびその製造方法 |
| JP3292119B2 (ja) | 1997-11-26 | 2002-06-17 | 住友化学工業株式会社 | メチオニンの製造方法 |
| CN1178909C (zh) * | 1999-05-21 | 2004-12-08 | 住友化学工业株式会社 | 蛋氨酸的制备方法 |
| JP2001340098A (ja) * | 2000-03-30 | 2001-12-11 | Nippon Shokubai Co Ltd | Ｌ−アスパラギン酸の製造方法 |
| EP1457486A4 (de) * | 2001-11-29 | 2006-04-05 | Nippon Soda Co | Verfahren zur herstellung von methionin |
| DE10160358A1 (de) * | 2001-12-08 | 2003-06-18 | Degussa | Verfahren zur Herstellung von Methionin |
| JP2004292324A (ja) | 2003-03-26 | 2004-10-21 | Nippon Soda Co Ltd | メチオニンの精製方法 |
| JP6368488B2 (ja) * | 2010-12-29 | 2018-08-01 | シージェイ チェイルジェダン コーポレーション | Ｌ−メチオニン及び関連産物の生産方法 |
-
2012
- 2012-03-20 EP EP12160257.7A patent/EP2641898A1/de not_active Withdrawn
-
2013
- 2013-02-26 EP EP17156859.5A patent/EP3187489B1/de active Active
- 2013-02-26 MY MYPI2014002674A patent/MY167899A/en unknown
- 2013-02-26 CN CN201380015209.9A patent/CN104203912B/zh active Active
- 2013-02-26 WO PCT/EP2013/053795 patent/WO2013139562A1/en not_active Ceased
- 2013-02-26 SG SG11201405870SA patent/SG11201405870SA/en unknown
- 2013-02-26 RU RU2014141935A patent/RU2640656C2/ru active
- 2013-02-26 US US14/386,165 patent/US9156782B2/en active Active
- 2013-02-26 KR KR1020147028874A patent/KR101988692B1/ko active Active
- 2013-02-26 CN CN201610151118.3A patent/CN105646304B/zh active Active
- 2013-02-26 MX MX2014011130A patent/MX354153B/es active IP Right Grant
- 2013-02-26 EP EP13706017.4A patent/EP2828239B1/de active Active
- 2013-02-26 BR BR112014023279-2A patent/BR112014023279B1/pt active IP Right Grant
- 2013-02-26 ES ES13706017.4T patent/ES2662937T3/es active Active
- 2013-02-26 JP JP2015500817A patent/JP6143840B2/ja active Active
-
2015
- 2015-09-10 US US14/850,207 patent/US9464045B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| MX2014011130A (es) | 2014-12-10 |
| RU2014141935A (ru) | 2016-05-20 |
| CN105646304A (zh) | 2016-06-08 |
| US20150051421A1 (en) | 2015-02-19 |
| US9464045B2 (en) | 2016-10-11 |
| EP3187489B1 (de) | 2020-11-25 |
| WO2013139562A1 (en) | 2013-09-26 |
| SG11201405870SA (en) | 2014-10-30 |
| ES2662937T3 (es) | 2018-04-10 |
| BR112014023279B1 (pt) | 2021-06-01 |
| KR101988692B1 (ko) | 2019-06-12 |
| US9156782B2 (en) | 2015-10-13 |
| EP2828239A1 (de) | 2015-01-28 |
| EP3187489A1 (de) | 2017-07-05 |
| CN104203912B (zh) | 2016-08-17 |
| CN105646304B (zh) | 2018-09-28 |
| MY167899A (en) | 2018-09-26 |
| JP6143840B2 (ja) | 2017-06-07 |
| EP2828239B1 (de) | 2018-01-31 |
| EP2641898A1 (de) | 2013-09-25 |
| CN104203912A (zh) | 2014-12-10 |
| RU2640656C2 (ru) | 2018-01-11 |
| US20160068480A1 (en) | 2016-03-10 |
| JP2015515458A (ja) | 2015-05-28 |
| KR20140138946A (ko) | 2014-12-04 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GB | Transfer or rights |
Owner name: EVONIK DEGUSSA GMBH.* |
|
| FG | Grant or registration |