KR20240134323A - Caf2-기초 불소화 시약, 이의 제조 방법 및 용도 - Google Patents

Caf2-기초 불소화 시약, 이의 제조 방법 및 용도 Download PDF

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Publication number
KR20240134323A
KR20240134323A KR1020247024338A KR20247024338A KR20240134323A KR 20240134323 A KR20240134323 A KR 20240134323A KR 1020247024338 A KR1020247024338 A KR 1020247024338A KR 20247024338 A KR20247024338 A KR 20247024338A KR 20240134323 A KR20240134323 A KR 20240134323A
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salt
reagent
fluorination
activated
fluorine
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Korean (ko)
Inventor
베로니크 거버뉴어
가브리엘레 푸포
제이미 레이치
던컨 브라운
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옥스포드 유니버시티 이노베이션 리미티드
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Publication of KR20240134323A publication Critical patent/KR20240134323A/ko
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    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01FCOMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F11/00Compounds of calcium, strontium, or barium
    • C01F11/18Carbonates
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00Phosphorus; Compounds thereof
    • C01B25/16Oxyacids of phosphorus; Salts thereof
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B9/00General methods of preparing halides
    • C01B9/08Fluorides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01FCOMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F11/00Compounds of calcium, strontium, or barium
    • C01F11/46Sulfates
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/093Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/20Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
    • C07C17/202Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
    • C07C17/208Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being MX
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/70Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/80Compositional purity

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Disintegrating Or Milling (AREA)
  • Crushing And Grinding (AREA)
KR1020247024338A 2021-12-22 2022-12-21 Caf2-기초 불소화 시약, 이의 제조 방법 및 용도 Pending KR20240134323A (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
GB2118767.9 2021-12-22
GB202118767 2021-12-22
PCT/GB2022/053347 WO2023118867A1 (en) 2021-12-22 2022-12-21 Caf2-based fluorination reagents, methods of preparation and uses thereof

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Publication Number Publication Date
KR20240134323A true KR20240134323A (ko) 2024-09-09

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KR1020247024338A Pending KR20240134323A (ko) 2021-12-22 2022-12-21 Caf2-기초 불소화 시약, 이의 제조 방법 및 용도

Country Status (11)

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US (3) US20240017996A1 (https=)
EP (1) EP4452857A1 (https=)
JP (1) JP2025506603A (https=)
KR (1) KR20240134323A (https=)
CN (1) CN118742517A (https=)
AU (1) AU2022421021A1 (https=)
CA (1) CA3241969A1 (https=)
IL (1) IL313534A (https=)
MX (1) MX2024007743A (https=)
TW (1) TW202426416A (https=)
WO (1) WO2023118867A1 (https=)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN118742517A (zh) 2021-12-22 2024-10-01 牛津大学科技创新有限公司 Caf2基氟化试剂、其制备方法和用途
KR20260025832A (ko) * 2023-06-15 2026-02-24 플루로크 리미티드 전해질 및 전해질 성분, 첨가제, 이의 전구체, 및 제조 방법
KR20260025838A (ko) * 2023-06-15 2026-02-24 플루로크 리미티드 전해질 및 전해질 성분, 첨가제, 이의 전구체, 및 제조 방법

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CN112707418B (zh) 2021-01-12 2022-12-30 苏州华一新能源科技股份有限公司 一种六氟磷酸锂的制备方法
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CN216236064U (zh) 2021-10-17 2022-04-08 会昌宏氟高新材料有限责任公司 一种六氟磷酸锂合成生产线
CN113772695B (zh) 2021-10-21 2022-08-26 福建省龙德新能源有限公司 六氟磷酸锂高效合成方法
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CN114057170A (zh) 2021-12-20 2022-02-18 瓮福(集团)有限责任公司 一种固相法合成五氟化磷及制备六氟磷酸锂的方法
CN118742517A (zh) 2021-12-22 2024-10-01 牛津大学科技创新有限公司 Caf2基氟化试剂、其制备方法和用途
CN114014283B (zh) 2022-01-06 2022-04-08 深圳市研一新材料有限责任公司 一种六氟磷酸盐、五氟化磷及其制备方法与应用
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CN115207307B (zh) 2022-06-09 2025-06-13 中国科学院化学研究所 一种锂/硅/碳复合负极及包含其的锂离子电池
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CN115849409B (zh) 2022-12-01 2024-04-09 胜华新能源科技(东营)有限公司 一种液态六氟磷酸锂的合成工艺
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CN115974107B (zh) 2022-12-15 2024-07-19 福建省龙德新能源有限公司 六氟磷酸钠的制备方法
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CN115959687B (zh) 2022-12-30 2024-04-12 四川大学 低成本生产六氟磷酸盐的工艺
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CN116282084A (zh) 2023-03-22 2023-06-23 哈工大机器人集团(杭州湾)国际创新研究院 一种在全卤有机化合物中制备六氟磷酸钠的方法
CN116462167A (zh) 2023-05-23 2023-07-21 多氟多新材料股份有限公司 一种制备五氟化磷和六氟磷酸盐的方法
KR102687640B1 (ko) 2023-07-06 2024-07-23 (주)후성 육불화인산알칼리금속염 제조방법, 육불화인산알칼리금속염 함유 전해농축액 제조방법, 및 이차전지 제조방법
CN116768243B (zh) 2023-08-23 2023-12-15 深圳新宙邦科技股份有限公司 六氟磷酸锂的制备方法和锂离子电池
CN117447501A (zh) 2023-10-27 2024-01-26 安阳工学院 一种二氟草酸硼酸锂联产六氟磷酸锂的方法
CN117486239A (zh) 2023-11-07 2024-02-02 哈工大机器人集团(杭州湾)国际创新研究院 一种制备六氟磷酸钠的方法
CN117534693A (zh) 2023-11-09 2024-02-09 安阳工学院 一种双草酸硼酸锂联产六氟磷酸锂及其制备方法和应用
CN117430139A (zh) 2023-11-09 2024-01-23 江苏新泰材料科技有限公司 一种六氟磷酸钠液体产品及其制备方法与应用
CN117401697B (zh) 2023-11-09 2025-10-17 九江天赐高新材料有限公司 一种六氟磷酸锂及其制备工艺
CN117504763B (zh) 2023-11-09 2024-07-30 多氟多海纳新材料有限责任公司 一种基于微通道反应器的六氟磷酸锂生产系统
CN117599747B (zh) 2023-11-27 2025-12-30 万华化学集团股份有限公司 一种Li+-NH2/介孔碳吸附剂及液体六氟磷酸锂的制备方法
CN117673456A (zh) 2023-12-04 2024-03-08 万华化学集团股份有限公司 一种六氟磷酸锂溶液及其制备方法和电解液
CN117800367A (zh) 2023-12-19 2024-04-02 万华化学集团股份有限公司 一种六氟磷酸锂的制备方法
CN118108238A (zh) 2024-02-04 2024-05-31 多氟多新材料股份有限公司 一种液态六氟磷酸盐的除酸方法
CN118164503A (zh) 2024-03-14 2024-06-11 多氟多新材料股份有限公司 一种二氟草酸硼酸锂联产六氟磷酸锂的方法
CN118165022A (zh) 2024-03-14 2024-06-11 多氟多新材料股份有限公司 一种双草酸硼酸锂和六氟磷酸锂的联合制备方法
CN118529750A (zh) 2024-07-26 2024-08-23 杭州万锂达新能源科技有限公司 一种同时制备六氟磷酸盐与二氟磷酸盐的方法

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AU2022421021A1 (en) 2024-08-01
JP2025506603A (ja) 2025-03-13
CN118742517A (zh) 2024-10-01
WO2023118867A1 (en) 2023-06-29
US12466776B2 (en) 2025-11-11
EP4452857A1 (en) 2024-10-30
TW202426416A (zh) 2024-07-01
US12071390B2 (en) 2024-08-27
MX2024007743A (es) 2024-07-01
IL313534A (en) 2024-08-01
US20250002431A1 (en) 2025-01-02
US20240017996A1 (en) 2024-01-18
CA3241969A1 (en) 2023-06-29
US20230339829A1 (en) 2023-10-26

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