KR20020027313A - 피메트로진의 용매화물 - Google Patents
피메트로진의 용매화물 Download PDFInfo
- Publication number
- KR20020027313A KR20020027313A KR1020017014315A KR20017014315A KR20020027313A KR 20020027313 A KR20020027313 A KR 20020027313A KR 1020017014315 A KR1020017014315 A KR 1020017014315A KR 20017014315 A KR20017014315 A KR 20017014315A KR 20020027313 A KR20020027313 A KR 20020027313A
- Authority
- KR
- South Korea
- Prior art keywords
- formula
- compounds
- pymetrozine
- water
- methyl
- Prior art date
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D401/00—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
- C07D401/02—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings
- C07D401/12—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings linked by a chain containing hetero atoms as chain links
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/64—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
- A01N43/707—1,2,3- or 1,2,4-triazines; Hydrogenated 1,2,3- or 1,2,4-triazines
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D253/00—Heterocyclic compounds containing six-membered rings having three nitrogen atoms as the only ring hetero atoms, not provided for by group C07D251/00
- C07D253/02—Heterocyclic compounds containing six-membered rings having three nitrogen atoms as the only ring hetero atoms, not provided for by group C07D251/00 not condensed with other rings
- C07D253/06—1,2,4-Triazines
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Agronomy & Crop Science (AREA)
- General Health & Medical Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Plural Heterocyclic Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
Description
d(Å) | 강도 |
12.47.16.86.36.25.825.405.144.854.684.524.314.144.083.963.833.713.583.473.443.253.213.093.032.992.902.822.762.57 | 보통약함매우 강함약함보통매우 약함보통매우 약함약함매우 약함매우 약함매우 약함약함매우 약함매우 약함매우 약함매우 약함약함매우 강함매우 강함강함약함보통약함약함약함약함약함약함 |
d(Å) | 강도 |
8.46.35.965.515.315.184.974.814.554.424.223.943.753.483.383.253.093.042.982.942.842.812.772.742.712.66 | 강함매우 약함약함매우 약함매우 약함매우 약함매우 약함매우 약함보통약함약함매우 약함매우 약함강함매우 강함약함약함약함매우 약함매우 약함매우 약함매우 약함매우 약함매우 약함매우 약함약함 |
d(Å) | 강도 |
9.78.45.875.575.144.964.864.694.404.294.233.833.733.663.493.343.283.062.952.822.652.602.532.482.302.252.202.112.072.00 | 보통매우 약함강함보통매우 약함약함보통매우 약함보통매우 약함매우 약함약함약함약함강함매우 강함보통이상약함매우 약함보통약함매우 약함매우 약함매우 약함약함매우 약함매우 약함약함약함약함 |
d(Å) | 강도 |
11.99.77.66.46.15.955.655.264.764.494.434.374.113.993.813.573.523.483.343.263.143.072.992.902.822.802.752.662.61 | 약함보통보통매우 약함보통보통보통보통약함약함매우 약함약함강함매우 강함약함약함약함강함매우 강함매우 약함강함매우 약함보통약함보통약함약함매우 약함약함 |
물 중량% | 저장하지 않는 경우의 자발성 백분율 | 실온에서 7일 동안의 개방 저장후의 자발성 백분율 | ||||
시간 | 0.5분 | 1분 | 물 중량% | 0.5분 | 1분 | |
과립 Ⅰ | 5.1 | 95 | 98 | 13.2 | 25 | 31 |
과립 Ⅱ | 10.3 | 96 | 98 | 13.7 | 93 | 98 |
Claims (9)
- 유리 형태 또는 염 형태 각각의 화학식 Ⅰ의 화합물 및 유리 형태 또는 염 형태 각각의 화학식 Ⅰ의 화합물의 호변이성체.화학식 Ⅰ상기 화학식에서,r 및 s는 각각 서로 독립적으로 0.00 내지 12.00 사이의 수치를 나타내고,L은 메탄올, 에탄올, 프로판올, 이소프로판올, 부탄올, 이소부탄올, t-부탄올, 사이클로헥산올, 테트라하이드로푸르푸릴 알콜, 에틸렌 글리콜, 글리세롤, 메틸 아세테이트, 에틸 아세테이트, 에틸 락테이트, 부티로락톤, 에틸렌 카보네이트, 프로필렌 카보네이트, 아세토니트릴, 디메틸 설폭사이드, 디메틸포름아미드, 디메틸아세트아미드, N-메틸-2-피롤리돈, N-옥틸-2-피롤리돈, N-데실-2-피롤리돈, 아세톤, 부타논, 메틸 이소부틸 케톤, 메틸프로필 케톤, 아세토페논, 사이클로헥사논, 메틸렌 클로라이드, 트리클로로메탄, 트리클로로에탄, 테트라하이드로푸란, 디에틸에테르, 1,2-디메톡시에탄, 디옥산, 메틸-3급-부틸에테르, 에탄올아민, 피리딘, 클로로벤젠, 톨루엔, 크실렌 또는 테트라메틸우레아이며, 단 이때 r 및 s는 동시에 0이 아니다.
- 제1항에 있어서, L이 메탄올인 화학식 Ⅰ의 화합물.
- 제1항에 있어서, r이 0이고 s가 2인 화학식 Ⅰ의 화합물.
- 제1항 내지 제3항 중의 어느 한 항에 따르는 화학식 Ⅰ의 화합물 및 하나 이상의 보조제를 함유하는 살충 조성물.
- 제1항에 따르는 화학식 Ⅰ의 활성 성분 또는 이러한 활성 성분을 살충 활성 양으로 함유하는 제4항에 따르는 조성물을 해충 또는 이의 서식지에 적용시킴을 포함하는, 해충의 방제방법.
- r 및 s가 0인 화학식 Ⅰ의 필수적으로 용매를 함유하지 않는 화합물을 함유하는 살충 혼합물을 용매화제와 접촉시킴을 포함하는, 제4항에 따르는 살충 조성물의 제조방법.
- 비용매화된, 살충 활성 화합물을 용매화제와 접촉시킴을 포함하는, 제1항에 따르는 화학식 Ⅰ의 화합물의 제조방법.
- 제4항에 있어서, 제6항에 따르는 방법에 의해 제조된 살충 조성물.
- 해충 방제를 위한 제4항에 따르는 조성물의 용도.
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH90599 | 1999-05-12 | ||
CH905/99 | 1999-05-12 | ||
CH1606/99 | 1999-09-03 | ||
CH160699 | 1999-09-03 |
Publications (2)
Publication Number | Publication Date |
---|---|
KR20020027313A true KR20020027313A (ko) | 2002-04-13 |
KR100736060B1 KR100736060B1 (ko) | 2007-07-06 |
Family
ID=25686072
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1020017014315A KR100736060B1 (ko) | 1999-05-12 | 2000-05-10 | 피메트로진의 용매화물 |
Country Status (26)
Country | Link |
---|---|
US (1) | US6784176B2 (ko) |
EP (1) | EP1177189B1 (ko) |
JP (1) | JP4824172B2 (ko) |
KR (1) | KR100736060B1 (ko) |
CN (1) | CN1219779C (ko) |
AR (1) | AR035908A1 (ko) |
AT (1) | ATE312832T1 (ko) |
AU (1) | AU764924B2 (ko) |
BR (1) | BR0010501B1 (ko) |
CA (1) | CA2372156C (ko) |
CO (1) | CO5210907A1 (ko) |
CY (1) | CY1105396T1 (ko) |
CZ (1) | CZ303340B6 (ko) |
DE (1) | DE60024807T2 (ko) |
DK (1) | DK1177189T3 (ko) |
DZ (1) | DZ3157A1 (ko) |
EG (1) | EG22667A (ko) |
ES (1) | ES2252021T3 (ko) |
HU (1) | HU229398B1 (ko) |
IL (1) | IL145831A0 (ko) |
NZ (1) | NZ515025A (ko) |
PL (1) | PL202065B1 (ko) |
RU (1) | RU2238941C2 (ko) |
TR (1) | TR200102931T2 (ko) |
TW (1) | TW542830B (ko) |
WO (1) | WO2000068222A2 (ko) |
Families Citing this family (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
TWI280128B (en) | 2002-05-22 | 2007-05-01 | Smithkline Beecham Corp | 3'-[(2Z)-[1-(3,4- dimethylphenyl)-1,5-dihydro-3-methyl-5-oxo-4H-pyrazol-4-ylidene]hydrazino]-2'-hydroxy-[1,1'-biphenyl]-3-carboxylic acid bis-(monoethanolamine) |
GT200500179BA (es) * | 2004-07-01 | 2008-10-29 | Mezclas sinergistas de agentes de antranilamida para el control de plagas de invertebrados | |
WO2007115967A1 (en) * | 2006-04-12 | 2007-10-18 | F. Hoffmann-La Roche Ag | Crystalline isopropanol solvate of glucokinase activator |
ECSP077628A (es) | 2007-05-03 | 2008-12-30 | Smithkline Beechman Corp | Nueva composición farmacéutica |
EP2002722A1 (en) * | 2007-06-15 | 2008-12-17 | Syngeta Participations AG | Methods of controlling insects |
GB0811300D0 (en) * | 2008-06-19 | 2008-07-30 | Syngenta Participations Ag | Methods of controlling neonicotinoid resistant insects |
CN102458120A (zh) | 2009-05-29 | 2012-05-16 | 葛兰素史密斯克莱有限责任公司 | 给药血小板生成素激动剂化合物的方法 |
CN102869259A (zh) | 2010-04-27 | 2013-01-09 | 先正达参股股份有限公司 | 控制耐新烟碱的蚜虫的方法 |
WO2013070451A1 (en) | 2011-11-07 | 2013-05-16 | 3M Innovative Properties Company | Whitening composition for selectively treating the surface of dental ceramic and related methods |
US10028809B2 (en) | 2012-10-17 | 2018-07-24 | 3M Innovative Properties Company | Multi sectional dental zirconia milling block, process of production and use thereof |
CN103098799B (zh) * | 2013-02-02 | 2016-08-03 | 广东中迅农科股份有限公司 | 吡蚜酮和氮酮悬浮乳剂及其制备方法 |
CN105828605B (zh) | 2013-12-23 | 2020-06-02 | 陶氏环球技术有限责任公司 | 吡蚜酮配制物 |
MA41827A (fr) * | 2015-03-27 | 2018-01-30 | Pharmacyclics Llc | Formes solvatées d'un inhibiteur de la tyrosine kinase de bruton |
CN107935689A (zh) * | 2017-11-29 | 2018-04-20 | 章立功 | 一种抗病梨树肥料 |
CN112538070B (zh) * | 2020-12-02 | 2023-04-07 | 天津大学 | 吡蚜酮-对羟基苯甲酸共晶及其制备方法 |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0314615B1 (de) * | 1987-10-16 | 1995-04-26 | Ciba-Geigy Ag | Schädlingsbekämpfungsmittel |
US5384403A (en) * | 1993-03-31 | 1995-01-24 | Ciba-Geigy Corporation | Process for the preparation of aminotriazine derivatives |
-
2000
- 2000-05-09 CO CO00033208A patent/CO5210907A1/es not_active Application Discontinuation
- 2000-05-10 RU RU2001132860A patent/RU2238941C2/ru active
- 2000-05-10 TW TW089108896A patent/TW542830B/zh not_active IP Right Cessation
- 2000-05-10 CN CNB008074240A patent/CN1219779C/zh not_active Expired - Lifetime
- 2000-05-10 JP JP2000617202A patent/JP4824172B2/ja not_active Expired - Lifetime
- 2000-05-10 CA CA002372156A patent/CA2372156C/en not_active Expired - Lifetime
- 2000-05-10 BR BRPI0010501-5A patent/BR0010501B1/pt active IP Right Grant
- 2000-05-10 WO PCT/EP2000/004251 patent/WO2000068222A2/en active IP Right Grant
- 2000-05-10 AU AU58082/00A patent/AU764924B2/en not_active Expired
- 2000-05-10 DZ DZ003157A patent/DZ3157A1/xx active
- 2000-05-10 PL PL351394A patent/PL202065B1/pl unknown
- 2000-05-10 KR KR1020017014315A patent/KR100736060B1/ko active IP Right Grant
- 2000-05-10 TR TR2001/02931T patent/TR200102931T2/xx unknown
- 2000-05-10 ES ES00943716T patent/ES2252021T3/es not_active Expired - Lifetime
- 2000-05-10 DE DE60024807T patent/DE60024807T2/de not_active Expired - Lifetime
- 2000-05-10 AR ARP000102242A patent/AR035908A1/es active IP Right Grant
- 2000-05-10 NZ NZ515025A patent/NZ515025A/xx not_active IP Right Cessation
- 2000-05-10 EG EG20000600A patent/EG22667A/xx active
- 2000-05-10 EP EP00943716A patent/EP1177189B1/en not_active Expired - Lifetime
- 2000-05-10 AT AT00943716T patent/ATE312832T1/de active
- 2000-05-10 IL IL14583100A patent/IL145831A0/xx not_active IP Right Cessation
- 2000-05-10 HU HU0201105A patent/HU229398B1/hu unknown
- 2000-05-10 DK DK00943716T patent/DK1177189T3/da active
- 2000-05-10 CZ CZ20014046A patent/CZ303340B6/cs not_active IP Right Cessation
-
2001
- 2001-11-09 US US10/039,706 patent/US6784176B2/en not_active Expired - Lifetime
-
2006
- 2006-03-07 CY CY20061100317T patent/CY1105396T1/el unknown
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