KR102246137B1 - 대전방지성 액체 결정질 중합체 조성물 - Google Patents
대전방지성 액체 결정질 중합체 조성물 Download PDFInfo
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- KR102246137B1 KR102246137B1 KR1020157009445A KR20157009445A KR102246137B1 KR 102246137 B1 KR102246137 B1 KR 102246137B1 KR 1020157009445 A KR1020157009445 A KR 1020157009445A KR 20157009445 A KR20157009445 A KR 20157009445A KR 102246137 B1 KR102246137 B1 KR 102246137B1
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- 239000000203 mixture Substances 0.000 title claims abstract description 92
- 229920000106 Liquid crystal polymer Polymers 0.000 title claims abstract description 48
- 239000002608 ionic liquid Substances 0.000 claims abstract description 28
- 239000011159 matrix material Substances 0.000 claims abstract description 12
- 229920000642 polymer Polymers 0.000 claims description 91
- -1 antimonate Chemical class 0.000 claims description 50
- 238000012360 testing method Methods 0.000 claims description 32
- 125000003118 aryl group Chemical group 0.000 claims description 29
- 239000000835 fiber Substances 0.000 claims description 27
- 238000002844 melting Methods 0.000 claims description 19
- 230000008018 melting Effects 0.000 claims description 19
- 238000000034 method Methods 0.000 claims description 17
- 150000001875 compounds Chemical class 0.000 claims description 15
- 150000003839 salts Chemical class 0.000 claims description 14
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 9
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- 229930195729 fatty acid Natural products 0.000 claims description 9
- 125000002091 cationic group Chemical group 0.000 claims description 8
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- 229910002804 graphite Inorganic materials 0.000 claims description 5
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- 150000002367 halogens Chemical class 0.000 claims description 5
- ZXMGHDIOOHOAAE-UHFFFAOYSA-N 1,1,1-trifluoro-n-(trifluoromethylsulfonyl)methanesulfonamide Chemical compound FC(F)(F)S(=O)(=O)NS(=O)(=O)C(F)(F)F ZXMGHDIOOHOAAE-UHFFFAOYSA-N 0.000 claims description 4
- 150000001408 amides Chemical class 0.000 claims description 4
- 150000008430 aromatic amides Chemical group 0.000 claims description 4
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- 239000010456 wollastonite Substances 0.000 claims description 4
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- ZGLLUEAYLAHJKB-UHFFFAOYSA-N 1,1,1-trifluoro-n-(trifluoromethyl)methanamine Chemical compound FC(F)(F)NC(F)(F)F ZGLLUEAYLAHJKB-UHFFFAOYSA-N 0.000 claims description 3
- DOYSIZKQWJYULQ-UHFFFAOYSA-N 1,1,2,2,2-pentafluoro-n-(1,1,2,2,2-pentafluoroethylsulfonyl)ethanesulfonamide Chemical group FC(F)(F)C(F)(F)S(=O)(=O)NS(=O)(=O)C(F)(F)C(F)(F)F DOYSIZKQWJYULQ-UHFFFAOYSA-N 0.000 claims description 3
- BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical compound [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 claims description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 3
- 150000003868 ammonium compounds Chemical class 0.000 claims description 3
- 150000001491 aromatic compounds Chemical class 0.000 claims description 3
- 229910052739 hydrogen Inorganic materials 0.000 claims description 3
- 239000001257 hydrogen Substances 0.000 claims description 3
- ACVYVLVWPXVTIT-UHFFFAOYSA-M phosphinate Chemical compound [O-][PH2]=O ACVYVLVWPXVTIT-UHFFFAOYSA-M 0.000 claims description 3
- 125000004178 (C1-C4) alkyl group Chemical group 0.000 claims description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims description 2
- 229910019142 PO4 Inorganic materials 0.000 claims description 2
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 2
- ULUAUXLGCMPNKK-UHFFFAOYSA-N Sulfobutanedioic acid Chemical compound OC(=O)CC(C(O)=O)S(O)(=O)=O ULUAUXLGCMPNKK-UHFFFAOYSA-N 0.000 claims description 2
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- 229910052736 halogen Inorganic materials 0.000 claims description 2
- 239000010452 phosphate Substances 0.000 claims description 2
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- HJHUXWBTVVFLQI-UHFFFAOYSA-N tributyl(methyl)azanium Chemical compound CCCC[N+](C)(CCCC)CCCC HJHUXWBTVVFLQI-UHFFFAOYSA-N 0.000 claims description 2
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 claims 1
- 230000003068 static effect Effects 0.000 abstract description 6
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- 238000010128 melt processing Methods 0.000 abstract description 4
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- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 43
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 description 18
- 238000006116 polymerization reaction Methods 0.000 description 16
- 239000000523 sample Substances 0.000 description 14
- FJKROLUGYXJWQN-UHFFFAOYSA-N 4-hydroxybenzoic acid Chemical compound OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 description 12
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- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 10
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 10
- QQVIHTHCMHWDBS-UHFFFAOYSA-N isophthalic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=C1 QQVIHTHCMHWDBS-UHFFFAOYSA-N 0.000 description 10
- 239000000178 monomer Substances 0.000 description 10
- RZVAJINKPMORJF-UHFFFAOYSA-N Acetaminophen Chemical compound CC(=O)NC1=CC=C(O)C=C1 RZVAJINKPMORJF-UHFFFAOYSA-N 0.000 description 9
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 9
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- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- 239000002585 base Substances 0.000 description 8
- 239000000314 lubricant Substances 0.000 description 8
- 125000003545 alkoxy group Chemical group 0.000 description 7
- 125000000217 alkyl group Chemical group 0.000 description 7
- 230000000052 comparative effect Effects 0.000 description 7
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- 239000003365 glass fiber Substances 0.000 description 7
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- 239000000463 material Substances 0.000 description 7
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- ALKYHXVLJMQRLQ-UHFFFAOYSA-N 3-Hydroxy-2-naphthoate Chemical compound C1=CC=C2C=C(O)C(C(=O)O)=CC2=C1 ALKYHXVLJMQRLQ-UHFFFAOYSA-N 0.000 description 6
- 229940090248 4-hydroxybenzoic acid Drugs 0.000 description 6
- KAUQJMHLAFIZDU-UHFFFAOYSA-N 6-Hydroxy-2-naphthoic acid Chemical compound C1=C(O)C=CC2=CC(C(=O)O)=CC=C21 KAUQJMHLAFIZDU-UHFFFAOYSA-N 0.000 description 6
- 239000000654 additive Substances 0.000 description 6
- VCCBEIPGXKNHFW-UHFFFAOYSA-N biphenyl-4,4'-diol Chemical compound C1=CC(O)=CC=C1C1=CC=C(O)C=C1 VCCBEIPGXKNHFW-UHFFFAOYSA-N 0.000 description 6
- 229910052799 carbon Inorganic materials 0.000 description 6
- 239000010445 mica Substances 0.000 description 6
- 229910052618 mica group Inorganic materials 0.000 description 6
- 238000002156 mixing Methods 0.000 description 6
- RXOHFPCZGPKIRD-UHFFFAOYSA-N naphthalene-2,6-dicarboxylic acid Chemical compound C1=C(C(O)=O)C=CC2=CC(C(=O)O)=CC=C21 RXOHFPCZGPKIRD-UHFFFAOYSA-N 0.000 description 6
- 238000012545 processing Methods 0.000 description 6
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 description 6
- 239000000758 substrate Substances 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 125000004423 acyloxy group Chemical group 0.000 description 5
- 208000029618 autoimmune pulmonary alveolar proteinosis Diseases 0.000 description 5
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 5
- 239000003054 catalyst Substances 0.000 description 5
- 125000000753 cycloalkyl group Chemical group 0.000 description 5
- 238000000113 differential scanning calorimetry Methods 0.000 description 5
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 5
- 229910052757 nitrogen Inorganic materials 0.000 description 5
- 239000002245 particle Substances 0.000 description 5
- 238000006068 polycondensation reaction Methods 0.000 description 5
- 239000004594 Masterbatch (MB) Substances 0.000 description 4
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 4
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- 125000004442 acylamino group Chemical group 0.000 description 4
- 125000003342 alkenyl group Chemical group 0.000 description 4
- 230000001143 conditioned effect Effects 0.000 description 4
- 150000001991 dicarboxylic acids Chemical class 0.000 description 4
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- 125000001188 haloalkyl group Chemical group 0.000 description 4
- 125000005843 halogen group Chemical group 0.000 description 4
- 125000001072 heteroaryl group Chemical group 0.000 description 4
- 125000000623 heterocyclic group Chemical group 0.000 description 4
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 4
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 4
- 238000010992 reflux Methods 0.000 description 4
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- JTGCXYYDAVPSFD-UHFFFAOYSA-N 4-(4-hydroxyphenyl)benzoic acid Chemical compound C1=CC(C(=O)O)=CC=C1C1=CC=C(O)C=C1 JTGCXYYDAVPSFD-UHFFFAOYSA-N 0.000 description 3
- JCJUKCIXTRWAQY-UHFFFAOYSA-N 6-hydroxynaphthalene-1-carboxylic acid Chemical compound OC1=CC=C2C(C(=O)O)=CC=CC2=C1 JCJUKCIXTRWAQY-UHFFFAOYSA-N 0.000 description 3
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 3
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- 230000000996 additive effect Effects 0.000 description 3
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- 125000004104 aryloxy group Chemical group 0.000 description 3
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 3
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- 125000000000 cycloalkoxy group Chemical group 0.000 description 3
- 238000013461 design Methods 0.000 description 3
- HBGGXOJOCNVPFY-UHFFFAOYSA-N diisononyl phthalate Chemical group CC(C)CCCCCCOC(=O)C1=CC=CC=C1C(=O)OCCCCCCC(C)C HBGGXOJOCNVPFY-UHFFFAOYSA-N 0.000 description 3
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 3
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- CJZGTCYPCWQAJB-UHFFFAOYSA-L calcium stearate Chemical compound [Ca+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O CJZGTCYPCWQAJB-UHFFFAOYSA-L 0.000 description 2
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- 125000000027 (C1-C10) alkoxy group Chemical group 0.000 description 1
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- HCNHNBLSNVSJTJ-UHFFFAOYSA-N 1,1-Bis(4-hydroxyphenyl)ethane Chemical compound C=1C=C(O)C=CC=1C(C)C1=CC=C(O)C=C1 HCNHNBLSNVSJTJ-UHFFFAOYSA-N 0.000 description 1
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- 125000001989 1,3-phenylene group Chemical group [H]C1=C([H])C([*:1])=C([H])C([*:2])=C1[H] 0.000 description 1
- WZCQRUWWHSTZEM-UHFFFAOYSA-N 1,3-phenylenediamine Chemical compound NC1=CC=CC(N)=C1 WZCQRUWWHSTZEM-UHFFFAOYSA-N 0.000 description 1
- 125000001140 1,4-phenylene group Chemical group [H]C1=C([H])C([*:2])=C([H])C([H])=C1[*:1] 0.000 description 1
- CBCKQZAAMUWICA-UHFFFAOYSA-N 1,4-phenylenediamine Chemical compound NC1=CC=C(N)C=C1 CBCKQZAAMUWICA-UHFFFAOYSA-N 0.000 description 1
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- 238000010998 test method Methods 0.000 description 1
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 1
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- 229910052723 transition metal Inorganic materials 0.000 description 1
- 150000003624 transition metals Chemical class 0.000 description 1
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- DXJLCRNXYNRGRA-UHFFFAOYSA-M tributyl(methyl)azanium;iodide Chemical compound [I-].CCCC[N+](C)(CCCC)CCCC DXJLCRNXYNRGRA-UHFFFAOYSA-M 0.000 description 1
- ITMCEJHCFYSIIV-UHFFFAOYSA-M triflate Chemical compound [O-]S(=O)(=O)C(F)(F)F ITMCEJHCFYSIIV-UHFFFAOYSA-M 0.000 description 1
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- 229910052724 xenon Inorganic materials 0.000 description 1
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- C08K5/36—Sulfur-, selenium-, or tellurium-containing compounds
- C08K5/43—Compounds containing sulfur bound to nitrogen
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- C09K19/38—Polymers
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- C08K5/19—Quaternary ammonium compounds
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- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
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- C08L67/02—Polyesters derived from dicarboxylic acids and dihydroxy compounds
- C08L67/03—Polyesters derived from dicarboxylic acids and dihydroxy compounds the dicarboxylic acids and dihydroxy compounds having the carboxyl- and the hydroxy groups directly linked to aromatic rings
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- C09K19/04—Liquid crystal materials characterised by the chemical structure of the liquid crystal components, e.g. by a specific unit
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- G02B27/0006—Optical systems or apparatus not provided for by any of the groups G02B1/00 - G02B26/00, G02B30/00 with means to keep optical surfaces clean, e.g. by preventing or removing dirt, stains, contamination, condensation
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- G03B17/00—Details of cameras or camera bodies; Accessories therefor
- G03B17/02—Bodies
- G03B17/12—Bodies with means for supporting objectives, supplementary lenses, filters, masks, or turrets
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- H04N23/00—Cameras or camera modules comprising electronic image sensors; Control thereof
- H04N23/50—Constructional details
- H04N23/55—Optical parts specially adapted for electronic image sensors; Mounting thereof
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- C09K19/00—Liquid crystal materials
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- C09K2019/521—Inorganic solid particles
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- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K19/00—Liquid crystal materials
- C09K19/52—Liquid crystal materials characterised by components which are not liquid crystals, e.g. additives with special physical aspect: solvents, solid particles
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| CN111732821A (zh) | 2013-03-13 | 2020-10-02 | 提克纳有限责任公司 | 抗静电液晶聚合物组合物 |
| CN106164172B (zh) | 2014-04-09 | 2019-07-26 | 提克纳有限责任公司 | 摄像模组 |
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| DE112016000328T5 (de) * | 2015-01-13 | 2017-10-19 | Ube Exsymo Co., Ltd. | Flexible Verbundplatte und mehrschichtige Leiterplatte |
| US9862809B2 (en) | 2015-07-31 | 2018-01-09 | Ticona Llc | Camera module |
| US10407605B2 (en) | 2015-07-31 | 2019-09-10 | Ticona Llc | Thermally conductive polymer composition |
| TWI708806B (zh) * | 2015-08-17 | 2020-11-01 | 美商堤康那責任有限公司 | 用於相機模組之液晶聚合物組合物 |
| CN107924039B (zh) * | 2015-09-01 | 2020-10-16 | 宝理塑料株式会社 | 照相机模块用液晶性树脂组合物及使用其的照相机模块 |
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| WO2019109595A1 (en) * | 2017-12-05 | 2019-06-13 | Ticona Llc | Liquid crystalline polymer composition |
| KR102627886B1 (ko) | 2017-12-05 | 2024-01-19 | 티코나 엘엘씨 | 카메라 모듈에 사용하기 위한 방향족 중합체 조성물 |
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| EP3755515A4 (en) | 2018-02-20 | 2021-11-10 | Ticona LLC | THERMAL CONDUCTIVE POLYMER COMPOSITION |
| KR20210088555A (ko) * | 2018-11-09 | 2021-07-14 | 스미또모 가가꾸 가부시끼가이샤 | 액정 폴리에스테르 수지 조성물 및 성형품 |
| US11722759B2 (en) | 2019-03-20 | 2023-08-08 | Ticona Llc | Actuator assembly for a camera module |
| KR20210148198A (ko) | 2019-03-20 | 2021-12-07 | 티코나 엘엘씨 | 카메라 모듈에서 사용하기 위한 중합체 조성물 |
| CN110746754B (zh) * | 2019-09-25 | 2021-06-29 | 广东格瑞新材料股份有限公司 | 一种激光雕刻液晶高分子组合物及其制备方法 |
| CN115151403A (zh) | 2019-12-17 | 2022-10-04 | 提克纳有限责任公司 | 采用热致液晶聚合物的三维打印系统 |
| JP2023515975A (ja) * | 2020-02-26 | 2023-04-17 | ティコナ・エルエルシー | 電子デバイス |
| EP4110610A4 (en) * | 2020-02-26 | 2024-03-27 | Ticona LLC | POLYMER COMPOSITION FOR ELECTRONIC DEVICE |
| JP7737387B2 (ja) | 2020-02-26 | 2025-09-10 | ティコナ・エルエルシー | 回路構造体 |
| KR20220146567A (ko) * | 2020-02-26 | 2022-11-01 | 티코나 엘엘씨 | 전자 디바이스 |
| JP7744146B2 (ja) * | 2020-03-30 | 2025-09-25 | 日東電工株式会社 | 粘着剤組成物、粘着シート、及び接合体 |
| US11728065B2 (en) | 2020-07-28 | 2023-08-15 | Ticona Llc | Molded interconnect device |
| CN112126243B (zh) * | 2020-09-09 | 2022-06-07 | 金发科技股份有限公司 | 一种液晶聚合物组合物 |
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| EP4263632A4 (en) | 2020-12-17 | 2024-11-20 | Ticona LLC | FIBER-REINFORCED PROPYLENE POLYMER COMPOSITION |
| US11728559B2 (en) | 2021-02-18 | 2023-08-15 | Ticona Llc | Polymer composition for use in an antenna system |
| US12209163B2 (en) | 2021-05-06 | 2025-01-28 | Ticona Llc | Polymer composition for use in a camera module |
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| CN118613966A (zh) | 2021-12-01 | 2024-09-06 | 提克纳有限责任公司 | 天线模块 |
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| TW201431932A (zh) | 2014-08-16 |
| WO2014062536A1 (en) | 2014-04-24 |
| US9988519B2 (en) | 2018-06-05 |
| TWI646135B (zh) | 2019-01-01 |
| JP2015532353A (ja) | 2015-11-09 |
| US20160185940A1 (en) | 2016-06-30 |
| KR20150073171A (ko) | 2015-06-30 |
| US20140105590A1 (en) | 2014-04-17 |
| JP6462576B2 (ja) | 2019-01-30 |
| CN104736672A (zh) | 2015-06-24 |
| CN104736672B (zh) | 2017-10-24 |
| US9284435B2 (en) | 2016-03-15 |
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