KR102218052B1 - 세라믹 리튬-이온 고체 전해질의 반응성 소결 - Google Patents

세라믹 리튬-이온 고체 전해질의 반응성 소결 Download PDF

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KR102218052B1
KR102218052B1 KR1020147017973A KR20147017973A KR102218052B1 KR 102218052 B1 KR102218052 B1 KR 102218052B1 KR 1020147017973 A KR1020147017973 A KR 1020147017973A KR 20147017973 A KR20147017973 A KR 20147017973A KR 102218052 B1 KR102218052 B1 KR 102218052B1
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lithium
solid
electrolyte membrane
less
forming
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KR20140106632A (ko
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브루스 가디너 아이트켄
마이클 에드워드 배딩
조지 핼시 비올
커티스 로버트 페키티
란리크 웨인 케스터
로버트 미카엘 모레나
전 송
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코닝 인코포레이티드
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    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/056—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
    • H01M10/0561—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of inorganic materials only
    • H01M10/0562—Solid materials
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B19/00—Other methods of shaping glass
    • C03B19/06—Other methods of shaping glass by sintering, e.g. by cold isostatic pressing of powders and subsequent sintering, by hot pressing of powders, by sintering slurries or dispersions not undergoing a liquid phase reaction
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C3/00—Glass compositions
    • C03C3/12—Silica-free oxide glass compositions
    • C03C3/16—Silica-free oxide glass compositions containing phosphorus
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C3/00—Glass compositions
    • C03C3/12—Silica-free oxide glass compositions
    • C03C3/253—Silica-free oxide glass compositions containing germanium
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
    • C03C8/20—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions containing titanium compounds; containing zirconium compounds
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    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/447—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on phosphates, e.g. hydroxyapatite
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    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M50/00—Constructional details or processes of manufacture of the non-active parts of electrochemical cells other than fuel cells, e.g. hybrid cells
    • H01M50/40—Separators; Membranes; Diaphragms; Spacing elements inside cells
    • H01M50/409—Separators, membranes or diaphragms characterised by the material
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3201—Alkali metal oxides or oxide-forming salts thereof
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
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    • C04B2235/3203—Lithium oxide or oxide-forming salts thereof
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3217—Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina
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    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3231—Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
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    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3231—Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
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    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3287—Germanium oxides, germanates or oxide forming salts thereof, e.g. copper germanate
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    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
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    • C04B2235/5418—Particle size related information expressed by the size of the particles or aggregates thereof
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    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
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    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
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  • Chemical & Material Sciences (AREA)
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  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Electrochemistry (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Nanotechnology (AREA)
  • Ceramic Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Structural Engineering (AREA)
  • Composite Materials (AREA)
  • Conductive Materials (AREA)
  • Secondary Cells (AREA)
  • Glass Compositions (AREA)
KR1020147017973A 2011-11-29 2012-11-29 세라믹 리튬-이온 고체 전해질의 반응성 소결 Expired - Fee Related KR102218052B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US13/306,011 2011-11-29
US13/306,011 US10411288B2 (en) 2011-11-29 2011-11-29 Reactive sintering of ceramic lithium-ion solid electrolytes
PCT/US2012/066968 WO2013082231A1 (en) 2011-11-29 2012-11-29 Reactive sintering of ceramic lithium-ion solid electrolytes

Publications (2)

Publication Number Publication Date
KR20140106632A KR20140106632A (ko) 2014-09-03
KR102218052B1 true KR102218052B1 (ko) 2021-02-22

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US (5) US10411288B2 (enExample)
EP (1) EP2786440B1 (enExample)
JP (2) JP2015506063A (enExample)
KR (1) KR102218052B1 (enExample)
CN (2) CN104221183A (enExample)
TW (1) TWI559599B (enExample)
WO (1) WO2013082231A1 (enExample)

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* Cited by examiner, † Cited by third party
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US9308511B2 (en) 2009-10-14 2016-04-12 Arizona Board Of Regents, A Body Corporate Of The State Of Arizona Acting For And On Behalf Of Arizona State University Fabricating porous materials using thixotropic gels
US9242900B2 (en) 2009-12-01 2016-01-26 Arizona Board Of Regents, A Body Corporate Of The State Of Arizona Acting For And On Behalf Of Arizona State University Porous geopolymer materials
CN103946181A (zh) 2011-09-21 2014-07-23 亚利桑那州立大学董事会(代理及代表亚利桑那州立大学的法人团体) 地聚合物树脂材料、地聚合物材料及由其制备的材料
WO2013109622A1 (en) * 2012-01-16 2013-07-25 Ceramatec, Inc Lithium-ion-conducting materials
JP5969799B2 (ja) * 2012-04-11 2016-08-17 株式会社コベルコ科研 Ｌｉ含有燐酸化合物焼結体およびスパッタリングターゲット、並びにその製造方法
US8821771B2 (en) 2012-09-26 2014-09-02 Corning Incorporated Flame spray pyrolysis method for forming nanoscale lithium metal phosphate powders
US9876247B2 (en) 2012-11-15 2018-01-23 Corning Incorporated Solid ceramic electrolytes
WO2015006010A2 (en) * 2013-06-21 2015-01-15 Dong-Kyun Seo Metal oxides from acidic solutions
KR101683949B1 (ko) * 2013-11-14 2016-12-07 주식회사 엘지화학 화염분무열분해법을 이용한 리튬 이차전지용 고체 전해질 나노 입자의 제조 방법
WO2015191962A1 (en) 2014-06-12 2015-12-17 Arizona Board Of Regents On Behalf Of Arizona State University Carbon dioxide adsorbents
US9673483B2 (en) 2015-01-19 2017-06-06 Corning Incorporated Reactive sintering of ceramic lithium ion electrolyte membranes
CN105304938B (zh) * 2015-09-29 2017-10-17 山东玉皇新能源科技有限公司 固体电解质磷酸钛铝锂的电化学制备方法
KR101945363B1 (ko) * 2016-05-10 2019-02-07 가부시키가이샤 스미타코가쿠가라스 Ltp 또는 latp 결정입자 제조 방법
WO2018136695A1 (en) 2017-01-20 2018-07-26 Seo Dong Kyun Aluminosilicate nanorods
DE102018102387B3 (de) 2018-02-02 2019-06-27 Schott Ag Glaskeramik mit ionenleitender Restglasphase und Verfahren zu ihrer Herstellung
CN108383517B (zh) * 2018-03-30 2020-12-22 华南理工大学 一种低温烧结Li-Mg-P-O固体电解质陶瓷及其制备方法
JP7054658B2 (ja) * 2018-07-31 2022-04-14 太平洋セメント株式会社 二次電池の固体電解質用ｌａｔｐ結晶粒子の製造方法
CN108987799B (zh) * 2018-08-09 2021-07-20 河南科技学院 一种全固态电池固态电解质及其制备方法和应用
US11819806B1 (en) * 2018-10-15 2023-11-21 Ampcera Inc. Methods for manufacturing a solid state ionic conductive membrane on a macro porous support scaffold
CN110137564B (zh) * 2019-04-09 2021-08-10 中国科学院合肥物质科学研究院 一种用于锂离子电池的多孔型固态电解质制备方法
WO2020206552A1 (fr) * 2019-04-11 2020-10-15 HYDRO-QUéBEC Électrolytes céramiques, leurs procédés de préparation et les cellules électrochimiques les comprenant
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