KR101885503B1 - 폴리사이클릭 구아니딘 화합물의 합성방법 - Google Patents
폴리사이클릭 구아니딘 화합물의 합성방법 Download PDFInfo
- Publication number
- KR101885503B1 KR101885503B1 KR1020127019400A KR20127019400A KR101885503B1 KR 101885503 B1 KR101885503 B1 KR 101885503B1 KR 1020127019400 A KR1020127019400 A KR 1020127019400A KR 20127019400 A KR20127019400 A KR 20127019400A KR 101885503 B1 KR101885503 B1 KR 101885503B1
- Authority
- KR
- South Korea
- Prior art keywords
- delete delete
- compound
- formula
- guanidine
- triamine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- OTBHHUPVCYLGQO-UHFFFAOYSA-N NCCCNCCCN Chemical compound NCCCNCCCN OTBHHUPVCYLGQO-UHFFFAOYSA-N 0.000 description 1
- DTSDBGVDESRKKD-UHFFFAOYSA-N NCCCNCCN Chemical compound NCCCNCCN DTSDBGVDESRKKD-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D487/00—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00
- C07D487/02—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00 in which the condensed system contains two hetero rings
- C07D487/04—Ortho-condensed systems
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US29008709P | 2009-12-24 | 2009-12-24 | |
| US61/290,087 | 2009-12-24 | ||
| US29904710P | 2010-01-28 | 2010-01-28 | |
| US61/299,047 | 2010-01-28 | ||
| US42249210P | 2010-12-13 | 2010-12-13 | |
| US61/422,492 | 2010-12-13 | ||
| PCT/US2010/060985 WO2011079041A1 (en) | 2009-12-24 | 2010-12-17 | Methods for the synthesis of polycyclic guanidine compounds |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR20120124419A KR20120124419A (ko) | 2012-11-13 |
| KR101885503B1 true KR101885503B1 (ko) | 2018-08-07 |
Family
ID=44196108
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020127019400A Active KR101885503B1 (ko) | 2009-12-24 | 2010-12-17 | 폴리사이클릭 구아니딘 화합물의 합성방법 |
Country Status (7)
| Country | Link |
|---|---|
| US (2) | US8642771B2 (https=) |
| EP (1) | EP2515648B1 (https=) |
| JP (1) | JP5766716B2 (https=) |
| KR (1) | KR101885503B1 (https=) |
| CN (1) | CN102665406B (https=) |
| NO (1) | NO2515648T3 (https=) |
| WO (1) | WO2011079041A1 (https=) |
Families Citing this family (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8334380B2 (en) | 2008-05-09 | 2012-12-18 | Ppg Industries Ohio, Inc. | Method for producing bicyclic guanidines by use of a cyclic urea and a dehydrating agent |
| CN102665406B (zh) | 2009-12-24 | 2016-03-09 | 诺沃梅尔公司 | 合成多环胍化合物的方法 |
| US8148490B2 (en) | 2010-03-10 | 2012-04-03 | Ppg Industries Ohio, Inc. | Method of making a cyclic guanidine from a guanidinium salt and a weak acid and coating compositions containing the same |
| US8288504B2 (en) | 2010-03-10 | 2012-10-16 | Ppg Industries Ohio, Inc. | Method of making a cyclic guanidine from dicyandiamide and coating compositions containing same |
| US8563560B2 (en) | 2011-02-25 | 2013-10-22 | Ppg Industries Ohio, Inc. | Preparation of bicyclic guanidine salts in an aqueous media |
| KR102024510B1 (ko) | 2011-07-18 | 2019-11-14 | 사우디 아람코 테크놀로지스 컴퍼니 | 금속 착체 |
| WO2013055747A1 (en) * | 2011-10-10 | 2013-04-18 | Novomer, Inc. | Methods to produce alkylated polycyclic guanidine compounds |
| EP2838954B1 (en) | 2012-04-16 | 2024-09-18 | Saudi Aramco Technologies Company | Adhesive compositions and methods |
| US20130289273A1 (en) * | 2012-04-25 | 2013-10-31 | Ppg Industries Ohio, Inc. | Methods for producing 1,5,7-triazabicyclo[4.4.0]dec-5-ene by reaction of a disubstituted carbodiimide and dipropylene triamine |
| US9108968B2 (en) | 2012-04-25 | 2015-08-18 | Ppg Industries Ohio, Inc. | Methods for producing 1,5,7-triazabicyclo[4.4.0]dec-5-ene by reaction of a disubstituted carbodiimide and dipropylene triamine |
| EP2888271B1 (en) | 2012-08-24 | 2019-11-06 | Saudi Aramco Technologies Company | Metal complexes |
| EP2951154B1 (de) * | 2013-01-30 | 2017-04-19 | Basf Se | 2,6-bis-(aminomethyl)piperidin- (2,6-bamp-), 2,6-bis-(isocyanomethyl)piperidin- (diisocyanat-) und 2,6-dicyanopiperidin-derivate (2,6-dcp-derivate) und ihre verwendung in der herstellung von epoxyharzen, polyurethanen, polyetherolen und polyamiden |
| US9068089B2 (en) | 2013-03-15 | 2015-06-30 | Ppg Industries Ohio, Inc. | Phenolic admix for electrodepositable coating composition containing a cyclic guanidine |
| CN103172639B (zh) * | 2013-03-18 | 2015-08-12 | 惠州市莱佛士制药技术有限公司 | 一种基于盐酸胍的六元二环胍的制备方法 |
| US9688874B2 (en) | 2013-10-25 | 2017-06-27 | Ppg Industries Ohio, Inc. | Method of making a bicyclic guanidine-cured acrylic coating |
| CN103539798A (zh) * | 2013-11-12 | 2014-01-29 | 南京大学 | 一种双环胍(1,5,7-三氮杂双环[5.5.0]癸-5-烯)的合成方法 |
| CN103755598A (zh) * | 2014-01-23 | 2014-04-30 | 上海旭新化工科技有限公司 | 胍丁胺硫酸盐的合成方法 |
| CN104844608B (zh) * | 2015-04-13 | 2017-09-19 | 南京大学 | 相转移催化法合成双环胍tbd的工艺方法 |
| CN110121548A (zh) * | 2017-01-03 | 2019-08-13 | 陈煌兴 | 支化聚合双胍化合物及其用途 |
| CN107325102B (zh) * | 2017-08-11 | 2019-11-12 | 南京大学 | 自催化双亲混合溶剂中合成1,5,7-三氮杂双环[4.4.0]癸-5-烯的工艺方法 |
| FI129024B (en) | 2017-11-08 | 2021-05-14 | Helsingin Yliopisto | Process for the preparation of bicyclic guanidine and its derivatives |
| WO2019126221A1 (en) | 2017-12-22 | 2019-06-27 | Saudi Aramco Technologies Company | Catalysts for polycarbonate production |
| US12145937B2 (en) | 2018-09-06 | 2024-11-19 | Wacker Chemie Ag | Process for preparing bicyclic guanidines |
| EP4048673B1 (en) * | 2019-10-22 | 2023-12-06 | Basf Se | Process for the production of cyclic guanidine derivates |
| CN112094273A (zh) * | 2020-08-07 | 2020-12-18 | 天津全和诚科技有限责任公司 | 一种的双环胍的合成方法 |
| CN112961343B (zh) * | 2021-02-19 | 2023-08-29 | 上海凯赛生物技术股份有限公司 | 一种戊二胺磷酸胍盐齐聚物、其制备方法及由其制得的抗菌聚合物 |
| WO2025045680A1 (en) | 2023-08-25 | 2025-03-06 | Evonik Operations Gmbh | Method to make bicyclic guanidines |
Family Cites Families (38)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2473111A (en) * | 1949-06-14 | Process for production of z-amino | ||
| US3873266A (en) * | 1971-03-19 | 1975-03-25 | Sandoz Ag | Solutions of polyalkylene polyamine-cyanamide condensation products |
| JPS585904B2 (ja) | 1977-04-05 | 1983-02-02 | 三井東圧化学株式会社 | グアニジン及びその塩類の製造方法 |
| GB2070006B (en) | 1980-02-22 | 1984-05-02 | Sandoz Ltd | Amine condencates useful in textile treatment |
| FR2509724B1 (fr) | 1981-07-15 | 1985-10-25 | Centre Nat Rech Scient | Nouvelles guanidines a fort encombrement sterique et procedes pour leur preparation |
| GB8509531D0 (en) * | 1985-04-13 | 1985-05-15 | Bp Chem Int Ltd | Preparation of guanidines |
| US5101041A (en) | 1989-04-26 | 1992-03-31 | The Curators Of The University Of Missouri | Triamines and their derivatives as bifunctional chelating agents |
| US5637739A (en) | 1990-03-21 | 1997-06-10 | Research Corporation Technologies, Inc. | Chiral catalysts and catalytic epoxidation catalyzed thereby |
| WO1995014461A1 (en) * | 1993-11-23 | 1995-06-01 | Cambridge Neuroscience, Inc. | Therapeutic substituted guanidines |
| US5659011A (en) * | 1994-09-23 | 1997-08-19 | Waldmann; John J. | Agents having high nitrogen content and high cationic charge based on dicyanimide dicyandiamide or guanidine and inorganic ammonium salts |
| US5665890A (en) | 1995-03-14 | 1997-09-09 | President And Fellows Of Harvard College | Stereoselective ring opening reactions |
| WO1998004538A1 (en) | 1996-07-26 | 1998-02-05 | Princeton University | Catalytic oxygenation of hydrocarbons by metalloporphyrin and metallosalen complexes |
| TWI246520B (en) | 1997-04-25 | 2006-01-01 | Mitsui Chemicals Inc | Processes for olefin polymerization |
| US6130340A (en) | 1998-01-13 | 2000-10-10 | President And Fellows Of Harvard College | Asymmetric cycloaddition reactions |
| US6521561B1 (en) | 1998-05-01 | 2003-02-18 | President And Fellows Of Harvard College | Main-group metal based asymmetric catalysts and applications thereof |
| KR100342659B1 (en) | 2000-12-15 | 2002-07-04 | Rstech Co Ltd | Chiral polymer salene catalyst and process for preparing chiral compounds from racemic epoxide using the same |
| US6884750B2 (en) | 2001-06-27 | 2005-04-26 | Rs Tech Corp. | Chiral salen catalyst and methods for the preparation of chiral compounds from racemic epoxides by using new catalyst |
| US6639087B2 (en) | 2001-08-22 | 2003-10-28 | Rhodia Pharma Solutions Inc. | Kinetic resolution method |
| DE10235316A1 (de) | 2002-08-01 | 2004-02-12 | Basf Ag | Katalysator und Verfahren zur Carbonylierung von Oxiranen |
| AU2004270304A1 (en) * | 2003-09-05 | 2005-03-17 | Actelion Pharmaceuticals Ltd. | Guanidine derivatives |
| KR100724550B1 (ko) | 2004-12-16 | 2007-06-04 | 주식회사 엘지화학 | 이중 금속 아연 착화합물과 이를 촉매로 사용한폴리카보네이트의 제조 방법 |
| WO2006099162A2 (en) | 2005-03-14 | 2006-09-21 | Georgia Tech Research Corporation | Polymeric salen compounds and methods thereof |
| US8232267B2 (en) | 2006-10-06 | 2012-07-31 | The Trustees Of Princeton University | Porphyrin catalysts and methods of use thereof |
| GB0708016D0 (en) | 2007-04-25 | 2007-06-06 | Univ Newcastle | Synthesis of cyclic carbonates |
| EP2573126B1 (en) | 2007-05-04 | 2014-09-24 | SK Innovation Co. Ltd. | A process for producing polycarbonates and a coordination complex used therefor |
| WO2008150033A1 (ja) | 2007-06-08 | 2008-12-11 | The University Of Tokyo | エポキシドと二酸化炭素との立体選択的交互共重合 |
| EP2096132A1 (en) | 2008-02-26 | 2009-09-02 | Total Petrochemicals Research Feluy | Monomers issued from renewable resources and process for polymerising them |
| BRPI0908982B8 (pt) | 2008-03-07 | 2018-08-07 | Univ Newcastle | síntese de carbonatos cíclicos |
| US8334380B2 (en) | 2008-05-09 | 2012-12-18 | Ppg Industries Ohio, Inc. | Method for producing bicyclic guanidines by use of a cyclic urea and a dehydrating agent |
| US8039618B2 (en) | 2008-05-09 | 2011-10-18 | Ppg Industries Ohio, Inc. | Method for producing bicyclic guanidines by use of a cyclic urea |
| CA2727959A1 (en) | 2008-07-30 | 2010-02-04 | Sk Energy, Co., Ltd. | Novel coordination complexes and process of producing polycarbonate by copolymerization of carbon dioxide and epoxide using the same as catalyst |
| CA2639870A1 (en) | 2008-09-29 | 2010-03-29 | Nova Chemicals Corporation | Trimerization |
| CN102665406B (zh) | 2009-12-24 | 2016-03-09 | 诺沃梅尔公司 | 合成多环胍化合物的方法 |
| KR101503745B1 (ko) | 2010-02-25 | 2015-03-19 | 에스케이이노베이션 주식회사 | 나이트레이트 음이온의 이산화탄소/에폭사이드 공중합 촉매 시스템 |
| US8288504B2 (en) | 2010-03-10 | 2012-10-16 | Ppg Industries Ohio, Inc. | Method of making a cyclic guanidine from dicyandiamide and coating compositions containing same |
| US8148490B2 (en) | 2010-03-10 | 2012-04-03 | Ppg Industries Ohio, Inc. | Method of making a cyclic guanidine from a guanidinium salt and a weak acid and coating compositions containing the same |
| US8563560B2 (en) | 2011-02-25 | 2013-10-22 | Ppg Industries Ohio, Inc. | Preparation of bicyclic guanidine salts in an aqueous media |
| GB201115565D0 (en) | 2011-09-08 | 2011-10-26 | Imp Innovations Ltd | Method of synthesising polycarbonates in the presence of a bimetallic catalyst and a chain transfer agent |
-
2010
- 2010-12-17 CN CN201080058473.7A patent/CN102665406B/zh active Active
- 2010-12-17 WO PCT/US2010/060985 patent/WO2011079041A1/en not_active Ceased
- 2010-12-17 US US13/515,634 patent/US8642771B2/en active Active
- 2010-12-17 EP EP10840015.1A patent/EP2515648B1/en active Active
- 2010-12-17 JP JP2012546076A patent/JP5766716B2/ja active Active
- 2010-12-17 KR KR1020127019400A patent/KR101885503B1/ko active Active
- 2010-12-17 NO NO10840015A patent/NO2515648T3/no unknown
-
2014
- 2014-01-06 US US14/148,455 patent/US9738647B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| EP2515648A1 (en) | 2012-10-31 |
| JP2013515728A (ja) | 2013-05-09 |
| NO2515648T3 (https=) | 2018-01-13 |
| US9738647B2 (en) | 2017-08-22 |
| CN102665406B (zh) | 2016-03-09 |
| WO2011079041A1 (en) | 2011-06-30 |
| CN102665406A (zh) | 2012-09-12 |
| EP2515648B1 (en) | 2017-08-16 |
| JP5766716B2 (ja) | 2015-08-19 |
| US20140194622A1 (en) | 2014-07-10 |
| EP2515648A4 (en) | 2014-08-27 |
| US8642771B2 (en) | 2014-02-04 |
| KR20120124419A (ko) | 2012-11-13 |
| US20120259112A1 (en) | 2012-10-11 |
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