KR101037592B1 - 전기전도성 탄소 원섬유계 잉크 및 코팅 - Google Patents
전기전도성 탄소 원섬유계 잉크 및 코팅 Download PDFInfo
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- KR101037592B1 KR101037592B1 KR1020047020166A KR20047020166A KR101037592B1 KR 101037592 B1 KR101037592 B1 KR 101037592B1 KR 1020047020166 A KR1020047020166 A KR 1020047020166A KR 20047020166 A KR20047020166 A KR 20047020166A KR 101037592 B1 KR101037592 B1 KR 101037592B1
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Abstract
Description
잉크 용도 | 점도 범위 |
제트 잉크 | |
수성 잉크 제트 | 20℃에서 1 내지 3cps |
연속 잉크 제트 | 20℃에서 1 내지 5cps |
UV 경화성 잉크 | 50℃에서 10 내지 15cps 또는 상온에서 50 내지 100cps |
고연 용융 잉크 제트 | 125℃에서 10 내지 25cps 또는 상온에서 고체 |
25℃에서의 인쇄용 잉크 | |
그라비아 | 30-200cps |
곡면인쇄용 | 50-500 cps |
신문잉크 | 200-1,000cps |
공판인쇄 | 1,000-50,000cps |
활판인쇄용 | 1,000-50,000cps |
평판인쇄용 | 10,000-80,000cps |
탄소 원섬유 종류 | 고체 함량 |
일반 CC | ∼5% 내지 ∼6% |
산화된 CC | ∼6% 내지 ∼7.5% |
BN | ∼7% 내지 ∼9% |
시료 | 코팅 횟수 | 두께(㎛) | 저항(Ω-cm) |
18-4 | 2 | 12 | 0.08 |
185-1 | 1 | 6 | 0.03 |
품목번호 | CC/BN(gm) | 아크릴(xp-9901) | 설피놀 CT324 |
64-01 | 산화된 BN(1.3) | 0.1gm | 0 |
66-02 | 산화된 CC(1.0) | 0.1gm | 0 |
55-03 | 일반 CC(1.0) | 0 | 1.5gm |
79-04 | 일반 CC(0.75) | 1.0gm | 0 |
79-06 | 일반 BN(1.0) | 0.75gm | 0 |
Claims (57)
- 원통형 탄소 원섬유로서, 이 원통의 축과 동심원성인 1 이상의 흑연층을 보유하고, 열분해 침착된 탄소 오버코트가 없으며, 0.4nm 내지 100nm 사이의 균일한 직경을 가지고, 길이:직경비가 5보다 큰 탄소 원섬유; 및액체 매개제를 함유하는 전기전도성 잉크로서,점도가 25 ℃에서 측정했을 때 1 내지 50,000 cps 범위이며 고분자 결합제를 포함하지 않는 전기전도성 잉크.
- 원통형 탄소 원섬유로서, 이 원통의 축과 동심원성인 1 이상의 흑연층을 보유하고, 열분해 침착된 탄소 오버코트가 없으며, 0.4nm 내지 100nm 사이의 균일한 직경을 가지고, 길이:직경비가 5보다 큰 탄소 원섬유; 및액체 매개제를 함유하는 전기전도성 잉크로서,점도가 25 ℃에서 측정했을 때 1 내지 50,000 cps 범위이며 고분자 결합제를 포함하며, 잉크 내 탄소 원섬유의 중량%가 고분자 결합제의 중량%보다 큰 전기전도성 잉크.
- 원통형 탄소 원섬유로서, 이 원통의 축과 동심원성인 1 이상의 흑연층을 보유하고, 열분해 침착된 탄소 오버코트가 없으며, 0.4nm 내지 100nm 사이의 균일한 직경을 가지고, 길이:직경비가 5보다 큰 탄소 원섬유; 및액체 매개제를 함유하는 전기전도성 잉크로서,점도가 25 ℃에서 측정했을 때 1 내지 50,000 cps 범위이며 고분자 결합제를 포함하며, 고분자 결합제의 양이 잉크의 0.1-10 중량% 범위인 전기전도성 잉크.
- 원통형 탄소 원섬유로서, 이 원통의 축과 동심원성인 1 이상의 흑연층을 보유하고, 열분해 침착된 탄소 오버코트가 없으며, 0.4nm 내지 100nm 사이의 균일한 직경을 가지고, 길이:직경비가 5보다 큰 탄소 원섬유; 및액체 매개제를 함유하는 전기전도성 잉크로서,점도가 25 ℃에서 측정했을 때 1 내지 50,000 cps 범위이며 요변성(thixotropic)인 전기전도성 잉크.
- 청구항 5은(는) 설정등록료 납부시 포기되었습니다.제4항에 있어서, 추가로 고분자 결합제를 포함하는 것이 특징인 전기전도성 잉크.
- 청구항 6은(는) 설정등록료 납부시 포기되었습니다.제1항 내지 제5항 중 어느 한 항에 있어서, 원섬유가 산화된 것인 전기전도성 잉크.
- 청구항 7은(는) 설정등록료 납부시 포기되었습니다.제2항 내지 제5항 중 어느 한 항에 있어서, 고분자 결합제가 하이드록시-관능화 비닐 에스테르, 아크릴계 공중합체, 셀룰로스 아세테이트 부티레이트, 하이드록실에틸 셀룰로스, 카르복실메틸 셀룰로스 및 아크릴계 고분자로 이루어진 그룹 중에서 선택되는 것이 특징인 전기전도성 잉크.
- 청구항 8은(는) 설정등록료 납부시 포기되었습니다.제1항 내지 제5항 중 어느 한 항에 있어서, 액체 매개제가 비탄화수소 극성 유기 용매인 것이 특징인 전기전도성 잉크.
- 청구항 9은(는) 설정등록료 납부시 포기되었습니다.제1항 내지 제5항 중 어느 한 항에 있어서, 액체 매개제가 카르비톨, 카르비톨 아세테이트, 부틸 카르비톨, 부틸 카르비톨 아세테이트, 부티로락톤, 아세톤, 메틸에틸케톤, 사이클로헥사논, 이염기성 에스테르 용매, 디글림, 고비등 알코올 및 알코올 에스테르로 이루어진 그룹 중에서 선택되는 것이 특징인 전기전도성 잉크.
- 청구항 10은(는) 설정등록료 납부시 포기되었습니다.제8항에 있어서, 유기 용매가 비등점이 150℃ 내지 200℃ 범위인 것이 특징인 전기전도성 잉크.
- 청구항 11은(는) 설정등록료 납부시 포기되었습니다.제1항 내지 제5항 중 어느 한 항에 있어서, 액체 매개제가 물인 것이 특징인 전기전도성 잉크.
- 청구항 12은(는) 설정등록료 납부시 포기되었습니다.제1항 내지 제5항 중 어느 한 항에 있어서, 탄소 원섬유가 전기전도성 잉크의 1 내지 5중량% 범위로 존재하는 것이 특징인 전기전도성 잉크.
- 청구항 13은(는) 설정등록료 납부시 포기되었습니다.제1항 내지 제5항 중 어느 한 항에 있어서, 탄소 원섬유가 전기전도성 잉크의 1.5 내지 2.5중량% 범위로 존재하는 것이 특징인 전기전도성 잉크.
- 청구항 14은(는) 설정등록료 납부시 포기되었습니다.제2항, 제3항 또는 제5항에 있어서, 고분자 결합제가 전기전도성 잉크의 0.5 내지 10중량% 범위로 존재하는 것이 특징인 전기전도성 잉크.
- 청구항 15은(는) 설정등록료 납부시 포기되었습니다.제2항, 제3항 또는 제5항에 있어서, 고분자 결합제가 전기전도성 잉크의 3 내지 6중량% 범위로 존재하는 것이 특징인 전기전도성 잉크.
- 청구항 16은(는) 설정등록료 납부시 포기되었습니다.제1항 내지 제4항 중 어느 한 항에 있어서, 탄소 원섬유가 직경이 3.5 내지 70nm 범위인 것이 특징인 전기전도성 잉크.
- 청구항 17은(는) 설정등록료 납부시 포기되었습니다.제1항 내지 제4항 중 어느 한 항에 있어서, 탄소 원섬유가 어골(fishbone) 형태인 것이 특징인 전기전도성 잉크.
- 청구항 18은(는) 설정등록료 납부시 포기되었습니다.제1항 내지 제4항 중 어느 한 항에 있어서, 추가로 계면활성제를 함유하는 것이 특징인 전기전도성 잉크.
- 청구항 19은(는) 설정등록료 납부시 포기되었습니다.제1항 내지 제4항 중 어느 한 항에 있어서, 탄소 원섬유가 응집물 형태인 것이 특징인 전기전도성 잉크.
- 청구항 20은(는) 설정등록료 납부시 포기되었습니다.제19항에 있어서, 응집물이 코움사(combed yarn)형 응집물, 솜사탕형 응집물, 새둥지형 응집물, 개방망형 응집물, 단벽 로프 및 이의 혼합물로 이루어진 그룹 중에서 선택되는 것이 특징인 전기전도성 잉크.
- 청구항 21은(는) 설정등록료 납부시 포기되었습니다.제1항 내지 제4항 중 어느 한 항에 있어서, 탄소 원섬유가 산화된 다중벽 탄소 원섬유인 것이 특징인 전기전도성 잉크.
- 청구항 22은(는) 설정등록료 납부시 포기되었습니다.제1항 내지 제4항 중 어느 한 항에 있어서, 카본 블랙, 흑연 또는 이의 혼합물로 이루어진 그룹 중에서 선택되는 탄소 물질을 추가로 포함하는 것이 특징인 전기전도성 잉크.
- 청구항 23은(는) 설정등록료 납부시 포기되었습니다.제1항 내지 제4항 중 어느 한 항에 있어서, 전기전도성 잉크가 1.0 내지 1.5 범위의 요변성도를 보유하는 것이 특징인 전기전도성 잉크.
- 청구항 24은(는) 설정등록료 납부시 포기되었습니다.원통형이고, 이 원통의 축과 동심원성인 1 이상의 흑연층을 보유하며, 열분해 침착된 탄소가 없고, 0.4nm 내지 100nm 사이의 균일한 직경을 가지며, 길이:직경비가 5보다 큰 탄소 원섬유를 액체 매개제에 첨가하여 용액을 제조하는 단계;상기 용액 중의 탄소 원섬유를 분산시켜 분산된 용액을 형성하는 단계;상기 분산된 용액 중의 탄소 원섬유를 분쇄시켜 분쇄된 용액을 형성하는 단계;상기 분쇄된 용액을 여과하여 전기전도성 잉크를 형성시키는 단계를 포함하는, 제1항 내지 제4항 중 어느 한 항에 따른 전기전도성 잉크의 제조방법.
- 청구항 25은(는) 설정등록료 납부시 포기되었습니다.제24항에 있어서, 탄소 원섬유를 액체 매개제에 첨가하여 용액을 제조하기 전에 액체 매개제와 고분자 결합제를 혼합하는 단계를 추가로 포함하는 것이 특징인, 전기전도성 잉크의 제조방법.
- 청구항 26은(는) 설정등록료 납부시 포기되었습니다.제24항에 있어서, 분산 단계가 초음파처리를 통해 수행되는 것이 특징인, 전기전도성 잉크의 제조방법.
- 청구항 27은(는) 설정등록료 납부시 포기되었습니다.제24항에 있어서, 분쇄 단계가 3중 로울 분쇄기를 이용하여 수행되는 것이 특징인, 전기전도성 잉크의 제조방법.
- 청구항 28은(는) 설정등록료 납부시 포기되었습니다.제24항에 있어서, 여과 단계가 스크린(screen)를 이용하여 수행되는 것이 특징인, 전기전도성 잉크의 제조방법.
- 청구항 29은(는) 설정등록료 납부시 포기되었습니다.제24항에 있어서, 고분자 결합제가 하이드록시-관능화 비닐 에스테르, 셀룰로스 아세테이트 부티레이트 및 아크릴계 고분자로 이루어진 그룹 중에서 선택되는 것이 특징인 전기전도성 잉크의 제조방법.
- 청구항 30은(는) 설정등록료 납부시 포기되었습니다.제24항에 있어서, 액체 매개제가 비탄화수소 극성 유기 용매인 것이 특징인 전기전도성 잉크의 제조방법.
- 청구항 31은(는) 설정등록료 납부시 포기되었습니다.제24항에 있어서, 액체 매개제가 카르비톨, 카르비톨 아세테이트, 부틸 카르비톨, 부틸 카르비톨 아세테이트, 부티로락톤, 아세톤, 메틸에틸케톤, 사이클로헥사논, 이염기성 에스테르 용매, 디글림, 고비등 알코올, 알코올 에스테르 및 물로 이루어진 그룹 중에서 선택되는 것이 특징인 전기전도성 잉크의 제조방법.
- 청구항 32은(는) 설정등록료 납부시 포기되었습니다.제24항에 있어서, 액체 매개제가 물인 것이 특징인 전기전도성 잉크의 제조방법.
- 청구항 33은(는) 설정등록료 납부시 포기되었습니다.제24항에 있어서, 액체 매개제가 비등점이 150℃ 내지 200℃ 범위인 것이 특징인 전기전도성 잉크의 제조방법.
- 청구항 34은(는) 설정등록료 납부시 포기되었습니다.제24항에 있어서, 탄소 원섬유가 이 원섬유 축과 직각인 c-축을 보유하고 직경이 3.5 내지 70nm 범위인 것이 특징인 전기전도성 잉크의 제조방법.
- 청구항 35은(는) 설정등록료 납부시 포기되었습니다.제24항에 있어서, 탄소 원섬유가 어골 형태인 것이 특징인 전기전도성 잉크의 제조방법.
- 청구항 36은(는) 설정등록료 납부시 포기되었습니다.제24항에 있어서, 탄소 원섬유가 응집물 형태인 것이 특징인 전기전도성 잉크의 제조방법.
- 청구항 37은(는) 설정등록료 납부시 포기되었습니다.제36항에 있어서, 응집물이 코움사(combed yarn)형 응집물, 솜사탕형 응집물, 새둥지형 응집물, 개방망형 응집물, 단벽 로프 및 이의 혼합물로 이루어진 그룹 중에서 선택되는 것이 특징인 전기전도성 잉크의 제조방법.
- 청구항 38은(는) 설정등록료 납부시 포기되었습니다.제24항에 있어서, 탄소 원섬유가 산화된 다중벽 탄소 원섬유인 것이 특징인 전기전도성 잉크의 제조방법.
- 청구항 39은(는) 설정등록료 납부시 포기되었습니다.제1항 내지 제5항 중 어느 한 항에 기재한 전도성 잉크를 사용하여 제조한 전기전도성 코팅.
- 청구항 40은(는) 설정등록료 납부시 포기되었습니다.제24항에 기재한 제조방법에 따라 제조한 전도성 잉크를 이용하여 제조한 전기전도성 코팅.
- 청구항 41은(는) 설정등록료 납부시 포기되었습니다.제1항에 기재한 잉크를 공판인쇄하여 전기전도성 코팅을 형성시키는 것을 포함하여, 상기 잉크를 사용하여 전기전도성 코팅을 제조하는 방법.
- 청구항 42은(는) 설정등록료 납부시 포기되었습니다.제41항에 있어서, 잉크의 점도가 1000 내지 50,000 cps 사이인 것이 특징인 방법.
- 청구항 43은(는) 설정등록료 납부시 포기되었습니다.제1항에 기재한 잉크를 잉크젯 인쇄하여 전기전도성 코팅을 형성시키는 단계를 포함하여, 상기 잉크를 이용하여 전기전도성 코팅을 제조하는 방법.
- 청구항 44은(는) 설정등록료 납부시 포기되었습니다.제43항에 있어서, 원섬유가 산화된 원섬유인 것이 특징인 방법.
- 청구항 45은(는) 설정등록료 납부시 포기되었습니다.제43항에 있어서, 잉크의 점도가 1 내지 3cps 사이인 것이 특징인 방법.
- 청구항 46은(는) 설정등록료 납부시 포기되었습니다.제1항에 기재한 잉크를 마스크를 통해 분무하여 전기전도성 코팅을 형성시키는 것을 포함하여, 상기 잉크를 이용하여 전기전도성 코팅을 제조하는 방법.
- 청구항 47은(는) 설정등록료 납부시 포기되었습니다.제46항에 있어서, 잉크의 점도가 1 내지 5cps 사이인 것이 특징인 방법.
- 청구항 48은(는) 설정등록료 납부시 포기되었습니다.제41항 내지 제47항 중 어느 한 항에 기재한 방법에 따라 제조한 코팅을 함유하는 전계 방출 캐쏘드.
- 청구항 49은(는) 설정등록료 납부시 포기되었습니다.제1항 내지 제5항 중 어느 한 항에 기재한 잉크를 사용하여 제조된 패턴화된 캐쏘드를 함유하고, 0.1 내지 2.0v/㎛ 사이에서 작동하는 전계 방출 캐쏘드.
- 청구항 50은(는) 설정등록료 납부시 포기되었습니다.제49항에 있어서, 탄소 원섬유가 이 원섬유 축에 직각인 c-축을 보유하고 직경이 3.5 내지 70nm 사이인 것이 특징인 전계 방출 캐쏘드.
- 청구항 51은(는) 설정등록료 납부시 포기되었습니다.제48항에 기재한 캐쏘드를 함유하는 디스플레이 장치.
- 청구항 52은(는) 설정등록료 납부시 포기되었습니다.제49항에 기재한 캐쏘드를 함유하는 디스플레이 장치.
- 청구항 53은(는) 설정등록료 납부시 포기되었습니다.제41항 내지 제47항 중 어느 한 항에 기재한 방법에 따라 제조한 전기전도성 코팅을 사용하여 만들어진 1개 이상의 인쇄된 전극을 함유하는 슈퍼축전기(supercapacitor).
- 청구항 54은(는) 설정등록료 납부시 포기되었습니다.제41항 내지 제47항 중 어느 한 항에 기재한 방법에 따라 제조한 코팅을 함유하는 인쇄 저항기.
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EP1514280B1 (en) | 2007-05-30 |
US8545730B2 (en) | 2013-10-01 |
EP1514280A4 (en) | 2005-11-23 |
US7852613B2 (en) | 2010-12-14 |
US20120153235A1 (en) | 2012-06-21 |
ATE363716T1 (de) | 2007-06-15 |
DE60314138T2 (de) | 2008-01-24 |
MXPA04012373A (es) | 2005-02-25 |
WO2003107359A1 (en) | 2003-12-24 |
CN100375201C (zh) | 2008-03-12 |
US8083970B2 (en) | 2011-12-27 |
DE60314138D1 (de) | 2007-07-12 |
JP2005530313A (ja) | 2005-10-06 |
KR20050014856A (ko) | 2005-02-07 |
US20050224764A1 (en) | 2005-10-13 |
US20080111110A1 (en) | 2008-05-15 |
AU2003238250B2 (en) | 2009-06-11 |
AU2003238250A1 (en) | 2003-12-31 |
CA2489423A1 (en) | 2003-12-24 |
EP1514280A1 (en) | 2005-03-16 |
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