JPWO2008015852A1 - 接着剤組成物及び回路部材の接続構造 - Google Patents
接着剤組成物及び回路部材の接続構造 Download PDFInfo
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- JPWO2008015852A1 JPWO2008015852A1 JP2008527684A JP2008527684A JPWO2008015852A1 JP WO2008015852 A1 JPWO2008015852 A1 JP WO2008015852A1 JP 2008527684 A JP2008527684 A JP 2008527684A JP 2008527684 A JP2008527684 A JP 2008527684A JP WO2008015852 A1 JPWO2008015852 A1 JP WO2008015852A1
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Abstract
Description
フェノキシ樹脂(商品名:PKHM−30、InChem社製)40質量部を、メチルエチルケトン60質量部に溶解して、固形分40質量%のフェノキシ樹脂溶液を調製した。
ブチラール樹脂(商品名:デンカブチラール3000−1、電気化学工業社製)40質量部を、メチルエチルケトン60質量部に溶解して、固形分40質量%のブチラール樹脂溶液とした。
ポリエステルウレタン樹脂として、UR−3210(商品名、東洋紡社製、樹脂分30質量%のメチルエチルケトン及びトルエン溶解品)を準備した。
重量平均分子量2000のポリブチレンアジペートジオール(アルドリッチ社製)450質量部、重量平均分子量2000のポリオキシテトラメチレングリコール(アルドリッチ社製)450質量部、及び1,4−ブチレングリコール(アルドリッチ社製)100質量部を、メチルエチルケトン4000質量部中で均一に混合した。そこに、ジフェニルメタンジイソシアネート(アルドリッチ社製)390質量部を加え、50℃で反応させてウレタン樹脂を得た。得られたウレタン樹脂の重量平均分子量は10万であった。
9,9−ビス(4−ヒドロキシフェニル)フルオレンエチレンオキサイド変性ジアクリレート(商品名:EA−0200、大阪ガス株式会社製、EO鎖の繰り返し数(式(A)におけるk+lの値):2、重量平均分子量:546.61)、9,9−ビス(4−ヒドロキシフェニル)フルオレンエチレンオキサイド変性ジアクリレート(商品名:EA−0500、大阪ガス株式会社製、EO鎖の繰り返し数(式(A)におけるk+lの値):5、重量平均分子量:678.77)、EO変性ビスフェノールAジアクリレート(商品名:FA−324A、日立化成工業株式会社製)、及び、2−(メタ)アクリロイロキシエチルホスフェート(商品名:ライトエステルP−2M、共栄社株式会社製)を準備した。
攪拌機、温度計、冷却管及び空気ガス導入管を備えた反応容器に空気ガスを導入した後、2−ヒドロキシエチルアクリレート238質量部(2.05モル)、数平均分子量860のポリ(ヘキサメチレンカーボネート)ジオール(アルドリッチ社製)860質量部(1モル)、ハイドロキノンモノメチルエーテル0.53質量部、ジブチルスズジラウレート5.53質量部を仕込み、70〜75℃に加熱し、イソフォロンジイソシアネート666質量部(3モル)を3時間かけて均一に滴下して反応させた。IR測定によりイソシアネートが消失したことを確認して反応を終了し、ウレタンアクリレート(UA)を得た。得られたウレタンアクリレートの数平均分子量は3700であった。
t−ヘキシルパーオキシ−2−エチルヘキサノエート(商品名:パーヘキシルO、日本油脂株式会社製)を準備した。
ポリスチレンを核とする粒子の表面に、厚み0.2μmのニッケル層を設け、このニッケル層の外側に、厚み0.02μmの金層を設けた。これにより、平均粒径4μm、比重2.5の導電性粒子を作製した。
上述した各材料を固形質量比で下記表1に示す割合で配合し、そこへ更に上記導電性粒子を1.5体積%(接着剤組成物の全体積基準)配合分散させて接着剤組成物を得た。得られた接着剤組成物を、厚み80μmのフッ素樹脂フィルムに塗工装置を用いて塗布し、70℃で10分間の熱風乾燥を行なうことにより、接着剤層の厚みが20μmのフィルム状接着剤を得た。
上記製法によって得たフィルム状接着剤を用いて、ライン幅25μm、ピッチ50μm、厚み18μmの銅回路を500本有するフレキシブル回路板(FPC基板)と、0.2μmの酸化インジウム(ITO)の薄層を形成したガラス(ITO基板、厚み1.1mm、表面抵抗20Ω/□)とを、熱圧着装置(加熱方式:コンスタントヒート型、東レエンジニアリング株式会社製)を用いて、160℃の温度にて3MPaで10秒間の加熱加圧を行った。これにより、幅2mmにわたりFPC基板とITO基板とをフィルム状接着剤の硬化物により接続した接続体(回路部材の接続構造)を作製した。
実施例1で得られたフィルム状接着剤を、真空包装を施した状態で、40℃にて3日間放置した。その後、この放置後のフィルム状接着剤を用いて、実施例1と同様にFPC基板とITO基板とを160℃、3MPa、10秒間の加熱圧着により幅2mmにわたって接続し、接続体(回路部材の接続構造)を作製した。得られた接続体の接着直後の接着強度及び接続抵抗を上記実施例1等と同様の方法で測定したところ、接着強度は710N/m、接続抵抗は1.2Ωであり、貯蔵安定性に優れることが確認された。
Claims (5)
- (a)熱可塑性樹脂と、
(b)分子内に1つ以上のフルオレン構造を有するラジカル重合性化合物と、
(c)ラジカル重合開始剤と、
を含有する、接着剤組成物。 - 更に、(d)分子内に1つ以上のリン酸基を有するビニル化合物を含有する、請求項1に記載の接着剤組成物。
- 前記(a)熱可塑性樹脂が、フェノキシ樹脂、ポリエステル樹脂、ポリウレタン樹脂、ポリエステルウレタン樹脂、ブチラール樹脂、アクリル樹脂、及び、ポリイミド樹脂からなる群より選択される少なくとも一種を含むものである、請求項1又は2に記載の接着剤組成物。
- 更に、(e)導電性粒子を含有する、請求項1〜3のうちのいずれか一項に記載の接着剤組成物。
- 第一の回路基板の主面上に第一の回路電極が形成された第一の回路部材と、
第二の回路基板の主面上に第二の回路電極が形成された第二の回路部材と、
前記第一の回路基板の主面と前記第二の回路基板の主面との間に設けられ、前記第一の回路電極と前記第二の回路電極とを対向配置させた状態で前記第一及び第二の回路部材同士を接続する回路接続部材と、
を備える回路部材の接続構造であって、
前記回路接続部材は、請求項1〜4のうちのいずれか一項に記載の接着剤組成物の硬化物からなり、
対向する前記第一の回路電極と前記第二の回路電極とが電気的に接続されている、回路部材の接続構造。
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