JP7436997B2 - フィラー及びその生成方法、高周波信号伝送用電解銅箔の製造方法 - Google Patents
フィラー及びその生成方法、高周波信号伝送用電解銅箔の製造方法 Download PDFInfo
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- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 title claims description 66
- 239000000945 filler Substances 0.000 title claims description 65
- 238000004519 manufacturing process Methods 0.000 title claims description 41
- 239000011889 copper foil Substances 0.000 title claims description 38
- 230000008054 signal transmission Effects 0.000 title claims description 15
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims description 111
- 239000000654 additive Substances 0.000 claims description 96
- 239000000047 product Substances 0.000 claims description 94
- 238000000354 decomposition reaction Methods 0.000 claims description 73
- 230000000996 additive effect Effects 0.000 claims description 63
- 239000000243 solution Substances 0.000 claims description 49
- 239000000919 ceramic Substances 0.000 claims description 40
- 238000006243 chemical reaction Methods 0.000 claims description 39
- GPNNOCMCNFXRAO-UHFFFAOYSA-N 2-aminoterephthalic acid Chemical compound NC1=CC(C(O)=O)=CC=C1C(O)=O GPNNOCMCNFXRAO-UHFFFAOYSA-N 0.000 claims description 33
- 238000001179 sorption measurement Methods 0.000 claims description 29
- 239000010949 copper Substances 0.000 claims description 28
- 229910052802 copper Inorganic materials 0.000 claims description 28
- 239000003792 electrolyte Substances 0.000 claims description 28
- 238000000034 method Methods 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 12
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 12
- 239000011521 glass Substances 0.000 claims description 11
- 239000011259 mixed solution Substances 0.000 claims description 11
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 8
- 238000003756 stirring Methods 0.000 claims description 8
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 8
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 6
- NQXWGWZJXJUMQB-UHFFFAOYSA-K iron trichloride hexahydrate Chemical compound O.O.O.O.O.O.[Cl-].Cl[Fe+]Cl NQXWGWZJXJUMQB-UHFFFAOYSA-K 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 6
- 239000002245 particle Substances 0.000 claims description 5
- 238000000861 blow drying Methods 0.000 claims description 4
- 238000005119 centrifugation Methods 0.000 claims description 4
- 239000003960 organic solvent Substances 0.000 claims description 4
- -1 polytetrafluoroethylene Polymers 0.000 claims description 4
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims description 4
- 239000004810 polytetrafluoroethylene Substances 0.000 claims description 4
- 239000002243 precursor Substances 0.000 claims description 4
- 239000006228 supernatant Substances 0.000 claims description 4
- 239000004677 Nylon Substances 0.000 claims description 3
- PMHQVHHXPFUNSP-UHFFFAOYSA-M copper(1+);methylsulfanylmethane;bromide Chemical compound Br[Cu].CSC PMHQVHHXPFUNSP-UHFFFAOYSA-M 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims description 3
- 238000001027 hydrothermal synthesis Methods 0.000 claims description 3
- 230000003472 neutralizing effect Effects 0.000 claims description 3
- 229920001778 nylon Polymers 0.000 claims description 3
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims description 3
- 238000001291 vacuum drying Methods 0.000 claims description 3
- 238000005406 washing Methods 0.000 claims description 3
- 239000013082 iron-based metal-organic framework Substances 0.000 description 61
- 238000011017 operating method Methods 0.000 description 10
- 230000000052 comparative effect Effects 0.000 description 8
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 description 8
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 7
- 238000004070 electrodeposition Methods 0.000 description 7
- 238000005868 electrolysis reaction Methods 0.000 description 6
- 230000007423 decrease Effects 0.000 description 5
- 238000004891 communication Methods 0.000 description 4
- 230000005540 biological transmission Effects 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 238000004811 liquid chromatography Methods 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 230000003746 surface roughness Effects 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 229910000365 copper sulfate Inorganic materials 0.000 description 2
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 description 2
- 230000008878 coupling Effects 0.000 description 2
- 238000010168 coupling process Methods 0.000 description 2
- 238000005859 coupling reaction Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000002848 electrochemical method Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000010408 film Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 150000003071 polychlorinated biphenyls Chemical class 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- 239000010409 thin film Substances 0.000 description 2
- 229910052719 titanium Inorganic materials 0.000 description 2
- 239000010936 titanium Substances 0.000 description 2
- 238000009827 uniform distribution Methods 0.000 description 2
- JPVYNHNXODAKFH-UHFFFAOYSA-N Cu2+ Chemical compound [Cu+2] JPVYNHNXODAKFH-UHFFFAOYSA-N 0.000 description 1
- 229920003188 Nylon 3 Polymers 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 229910010293 ceramic material Inorganic materials 0.000 description 1
- 238000002144 chemical decomposition reaction Methods 0.000 description 1
- 239000007810 chemical reaction solvent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 229910001431 copper ion Inorganic materials 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000002500 effect on skin Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000011888 foil Substances 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 150000004687 hexahydrates Chemical class 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000006259 organic additive Substances 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 230000002572 peristaltic effect Effects 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 238000004445 quantitative analysis Methods 0.000 description 1
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
- B01J20/223—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material containing metals, e.g. organo-metallic compounds, coordination complexes
- B01J20/226—Coordination polymers, e.g. metal-organic frameworks [MOF], zeolitic imidazolate frameworks [ZIF]
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/3071—Washing or leaching
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D1/00—Electroforming
- C25D1/04—Wires; Strips; Foils
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/3078—Thermal treatment, e.g. calcining or pyrolizing
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/3092—Packing of a container, e.g. packing a cartridge or column
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
- B01J20/3202—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the carrier, support or substrate used for impregnation or coating
- B01J20/3204—Inorganic carriers, supports or substrates
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C1/00—Electrolytic production, recovery or refining of metals by electrolysis of solutions
- C25C1/12—Electrolytic production, recovery or refining of metals by electrolysis of solutions of copper
-
- H—ELECTRICITY
- H04—ELECTRIC COMMUNICATION TECHNIQUE
- H04B—TRANSMISSION
- H04B3/00—Line transmission systems
- H04B3/02—Details
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05K—PRINTED CIRCUITS; CASINGS OR CONSTRUCTIONAL DETAILS OF ELECTRIC APPARATUS; MANUFACTURE OF ASSEMBLAGES OF ELECTRICAL COMPONENTS
- H05K1/00—Printed circuits
- H05K1/02—Details
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- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C7/00—Constructional parts, or assemblies thereof, of cells; Servicing or operating of cells
- C25C7/02—Electrodes; Connections thereof
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- Chemical Kinetics & Catalysis (AREA)
- Analytical Chemistry (AREA)
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- Microelectronics & Electronic Packaging (AREA)
- Computer Networks & Wireless Communication (AREA)
- Signal Processing (AREA)
- Electrolytic Production Of Metals (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
- Compounds Of Iron (AREA)
Description
フィラー(MI-Fe-MOFs/PC)の生成方法は以下の通りとした。
フィラー(MI-Fe-MOFs/PC)の生成方法は以下の通りとした。
フィラー(MI-Fe-MOFs/PC)の生成方法は以下の通りとした。
フィラー(MI-Fe-MOFs/PC)の生成方法は以下の通りとした。
フィラー(MI-Fe-MOFs/PC)の生成方法は以下の通りとした。
フィラー(MI-Fe-MOFs/PC)の生成方法は以下の通りとした。
フィラー(MI-Fe-MOFs/PC)の生成方法は以下の通りとした。
フィラー(MI-Fe-MOFs/PC)の生成方法は以下の通りとした。
フィラー(MI-Fe-MOFs/PC)の生成方法は以下の通りとした。
フィラー(MI-Fe-MOFs/PC)の生成方法は以下の通りとした。
フィラー(MI-Fe-MOFs/PC)の生成方法は以下の通りとした。
2 フィラー
3 メッシュ状ナイロン
Claims (8)
- フィラーの生成方法であって、
前記フィラーは、
電解銅箔の添加剤分解生成物分子の鋳型構造がインプリンティングされた結晶状のフィラーであって、
原料として、
塩化鉄(III)六水和物:3g、
鋳型分子:0.15~3g、
N,N-ジメチルホルムアミド:60g、
2-アミノテレフタル酸:1g、
多孔質セラミックス:6~30g、を含み、
前記鋳型分子は、電解銅箔の添加剤分解生成物分子であることを特徴とするフィラーの生成方法。 - フィラーの生成方法であって、
ステップS01:塩化鉄(III)六水和物と鋳型分子を水中に溶解して反応溶液を形成し、
ステップS02:反応溶液にN,N-ジメチルホルムアミドを加え、攪拌して溶解させ、
ステップS03:反応溶液に2-アミノテレフタル酸を加え、攪拌して溶解させ、
ステップS04:多孔質セラミックスを反応溶液に浸漬して攪拌し、
ステップS05:水熱法で反応溶液を処理し、添加剤分解生成物分子を除去して、添加剤分解生成物分子の鋳型構造がインプリンティングされた結晶状のフィラーを生成する、との反応ステップを含むことを特徴とする請求項1に記載のフィラーの生成方法。 - 前記ステップS05は、
ステップS05.1:ステップS04で攪拌した反応溶液をポリテトラフルオロエチレンライニングボトルに投入したあと反応釜に移し、送風乾燥炉に配置して反応させ、
ステップS05.2:反応終了後に冷却し、反応溶液を取り出して遠心分離にかけてから、上清液を廃棄して生成物を収集し、
ステップS05.3:N,N-ジメチルホルムアミドで生成物を一次洗浄し、未配位の反応前駆体を洗い流し、
ステップS05.4:メタノールで生成物を二次洗浄し、生成物中の鋳型分子-添加剤分解生成物を洗い流し、
ステップS05.5:2回洗浄した生成物を遠心分離にかけて収集し、真空乾燥させて、添加剤分解生成物分子の鋳型構造がインプリンティングされたフィラーを取得する、とのステップを含むことを特徴とする請求項2に記載のフィラーの生成方法。 - 前記フィラーの生成過程において、2-アミノテレフタル酸、塩化鉄(III)六水和物、N,N-ジメチルホルムアミド及び水の質量パーセント濃度は、
2-アミノテレフタル酸:塩化鉄(III)六水和物:N,N-ジメチルホルムアミド:水=1:3:60:200であることを特徴とする請求項2に記載のフィラーの生成方法。 - 前記鋳型分子の生成方法では、
添加剤と濃硫酸を含む混合溶液を調製し、
電解反応に関与しない2つの材料を陽極及び陰極として混合溶液中に配置し、
混合溶液を電気分解し、
NaOH溶液で電解液を中和したあと、アセトン有機溶媒で抽出することで鋳型分子を取得することを特徴とする請求項2に記載のフィラーの生成方法。 - 前記多孔質セラミックスには、酸化アルミニウム多孔質セラミックス、ジルコニア多孔質セラミックス、又は窒化アルミニウム多孔質セラミックスのいずれかを採用することを特徴とする請求項2に記載のフィラーの生成方法。
- 前記多孔質セラミックスの粒径は、100μmよりも大きく、且つ1000μmよりも小さいことを特徴とする請求項2に記載のフィラーの生成方法。
- 高周波信号伝送用電解銅箔の製造方法であって、
添加剤分解生成物吸着カラムを電解槽に接続し、
添加剤分解生成物吸着カラムを用いて電解槽内の銅電解液を濾過することで、銅電解液中の添加剤分解生成物の除去を実現しつつ、添加剤は残留させて、高周波信号伝送用電解銅箔を製造する、とのステップを含み、
前記添加剤分解生成物吸着カラムは、
フィラーを収容するガラス管と、
ガラス管内に設置されてフィラーの両端を閉塞する2つのメッシュ状ナイロン、を含み、
前記フィラーは請求項2で記載した方法で生成されることを特徴とする製造方法。
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JP2001295090A (ja) | 2000-04-14 | 2001-10-26 | Mitsui Mining & Smelting Co Ltd | 電解銅箔の製造方法、電解銅箔、銅張り積層板およびプリント配線板 |
JP2001329390A (ja) | 2000-05-18 | 2001-11-27 | Mitsui Mining & Smelting Co Ltd | 電解銅箔の電解装置及びその電解装置で得られた電解銅箔 |
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