JP5918358B2 - 塩素化プロペンの製造方法 - Google Patents
塩素化プロペンの製造方法 Download PDFInfo
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- JP5918358B2 JP5918358B2 JP2014513552A JP2014513552A JP5918358B2 JP 5918358 B2 JP5918358 B2 JP 5918358B2 JP 2014513552 A JP2014513552 A JP 2014513552A JP 2014513552 A JP2014513552 A JP 2014513552A JP 5918358 B2 JP5918358 B2 JP 5918358B2
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- reactor
- pentachloropropane
- stream
- chlorination
- dehydrochlorination
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/25—Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/10—Preparation of halogenated hydrocarbons by replacement by halogens of hydrogen atoms
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Description
Claims (5)
- 1,2−ジクロロプロパンを含む1種又は複数種の塩素化アルカンから塩素化プロペンを製造するための方法であって、フリーラジカル開始剤の存在下で行われる少なくとも1つの液相塩素化工程と、少なくとも1つの脱塩化水素工程とを含み、前記少なくとも1つの塩素化工程は、トリクロロプロパン異性体、テトラクロロプロパン異性体、ペンタクロロプロパン異性体及び未反応の1,2−ジクロロプロパンを含む下部流を生成し、前記トリクロロプロパン異性体、テトラクロロプロパン異性体及び未反応の1,2−ジクロロプロパンは、前記下部流から分離されて、前記塩素化工程に再循環される、前記方法。
- 前記塩素化工程は、トリクロロプロパン、テトラクロロプロパン及びペンタクロロプロパンの混合物を生成し、前記フリーラジカル開始剤は、1種又は複数種のアゾ化合物及び/又は過酸化化合物、UV光、又はこれらの組み合わせを含む、請求項1に記載の方法。
- 少なくとも1つの塩素化工程は、未反応の塩素、モノ塩素化プロペン及びHClを含む流れを生成し、前記HClは、無水HClとして前記流れから分離され、前記未反応の塩素は、前記流れから分離されて、前記塩素化工程に再循環される、請求項1に記載の方法。
- 前記ペンタクロロプロパン異性体は、前記下部流から分離され、さらに、1,1,2,2,3−ペンタクロロプロパン及び1,1,1,2,2−ペンタクロロプロパンを含む第一の流れと、1,1,2,3,3−ペンタクロロプロパンを含む第二の流れに分離され、そして、1,1,2,3−テトラクロロプロペン及び2,3,3,3−テトラクロロプロペンを提供するために、1,1,2,2,3−ペンタクロロプロパン及び1,1,1,2,2−ペンタクロロプロパンが苛性クラックされる、請求項1に記載の方法。
- 塩素化剤が、塩素、塩化スルフリル、又はこれらの組合せを含む、請求項1に記載の方法。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201161491816P | 2011-05-31 | 2011-05-31 | |
US61/491,816 | 2011-05-31 | ||
PCT/US2012/038613 WO2012166394A1 (en) | 2011-05-31 | 2012-05-18 | Process for the production of chlorinated propenes |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2014520100A JP2014520100A (ja) | 2014-08-21 |
JP5918358B2 true JP5918358B2 (ja) | 2016-05-18 |
Family
ID=46149752
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2014513552A Active JP5918358B2 (ja) | 2011-05-31 | 2012-05-18 | 塩素化プロペンの製造方法 |
Country Status (6)
Country | Link |
---|---|
US (1) | US9056808B2 (ja) |
EP (1) | EP2714631B1 (ja) |
JP (1) | JP5918358B2 (ja) |
CN (1) | CN103562163B (ja) |
CA (1) | CA2837292C (ja) |
WO (1) | WO2012166394A1 (ja) |
Families Citing this family (29)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102686544B (zh) | 2009-10-09 | 2017-02-15 | 蓝立方知识产权公司 | 用于生产氯化和/或氟化丙烯和高级烯烃的方法 |
EP2485832B1 (en) | 2009-10-09 | 2016-11-23 | Blue Cube IP LLC | Process for producing a chlorinated and/or fluorinated propene in an isothermal multitube reactors and |
CA2836493A1 (en) | 2011-05-31 | 2012-12-06 | Max Markus Tirtowidjojo | Process for the production of chlorinated propenes |
US9056808B2 (en) | 2011-05-31 | 2015-06-16 | Dow Global Technologies, Llc | Process for the production of chlorinated propenes |
MX336250B (es) | 2011-06-08 | 2016-01-13 | Dow Agrosciences Llc | Proceso para la produccion de propenos clorados y/o fluorados. |
CN109438173A (zh) | 2011-08-07 | 2019-03-08 | 蓝立方知识产权有限责任公司 | 生产氯化的丙烯的方法 |
EP2739596B1 (en) | 2011-08-07 | 2019-05-01 | Blue Cube IP LLC | Process for the production of chlorinated propenes |
CA2856271A1 (en) | 2011-11-21 | 2013-05-30 | Dow Global Technologies Llc | Process for the production of chlorinated alkanes |
US9284239B2 (en) | 2011-12-02 | 2016-03-15 | Blue Cube Ip Llc | Process for the production of chlorinated alkanes |
CA2856545A1 (en) | 2011-12-02 | 2013-06-06 | Dow Global Technologies Llc | Process for the production of chlorinated alkanes |
JP6170068B2 (ja) | 2011-12-13 | 2017-07-26 | ブルー キューブ アイピー エルエルシー | 塩素化プロパン及びプロペンの製造方法 |
CN110128239A (zh) | 2011-12-22 | 2019-08-16 | 蓝立方知识产权有限责任公司 | 生产四氯甲烷的方法 |
WO2013096706A1 (en) | 2011-12-23 | 2013-06-27 | Dow Global Technologies, Llc | Process for the production of alkenes and/or aromatic compounds |
JP2015529247A (ja) | 2012-09-20 | 2015-10-05 | ダウ グローバル テクノロジーズ エルエルシー | 塩素化プロペンの生成のためのプロセス |
US9321707B2 (en) | 2012-09-20 | 2016-04-26 | Blue Cube Ip Llc | Process for the production of chlorinated propenes |
JP6272878B2 (ja) | 2012-09-30 | 2018-01-31 | ブルー キューブ アイピー エルエルシー | せきクエンチおよびそれを組み込んだ方法 |
JP6363610B2 (ja) | 2012-10-26 | 2018-07-25 | ブルー キューブ アイピー エルエルシー | 混合器およびそれを組み込んだプロセス |
CA2893841C (en) | 2012-12-18 | 2018-07-24 | Dow Global Technologies Llc | Process for the production of chlorinated propenes |
JP6251286B2 (ja) * | 2012-12-19 | 2017-12-20 | ブルー キューブ アイピー エルエルシー | 塩素化プロペン生成のための方法 |
US8889930B2 (en) | 2013-01-22 | 2014-11-18 | Axiall Ohio, Inc. | Process for producing chlorinated hydrocarbons |
US9289758B2 (en) | 2013-01-22 | 2016-03-22 | Axiall Ohio, Inc. | Processes for producing chlorinated hydrocarbons and methods for recovering polyvalent antimony catalysts therefrom |
US9382176B2 (en) | 2013-02-27 | 2016-07-05 | Blue Cube Ip Llc | Process for the production of chlorinated propenes |
CA2903760C (en) | 2013-03-09 | 2018-02-20 | Blue Cube Ip Llc | Process for the production of chlorinated alkanes |
US9090531B2 (en) * | 2013-03-14 | 2015-07-28 | Honeywell International Inc. | Method for mitigating HCL generation during 1,1,2,3-tetrachloropropene purification |
US9139497B2 (en) | 2013-10-23 | 2015-09-22 | Axiall Ohio, Inc. | Process for producing chlorinated hydrocarbons in the presence of a polyvalent bismuth compound |
CN104987278B (zh) * | 2015-07-20 | 2016-09-28 | 山东联创互联网传媒股份有限公司 | 2,3,3,3-四氟丙烯的合成方法 |
BR112018005473B1 (pt) | 2015-09-21 | 2021-05-25 | Arkema Inc. | processo para produzir tetracloropropeno por desidrocloração catalisada em fase gasosa de pentacloropropano |
JP6843866B2 (ja) * | 2016-01-04 | 2021-03-17 | ブルー キューブ アイピー エルエルシー | ハロゲン化アルカンを調製するための改善されたプロセス |
JP2021520370A (ja) * | 2018-04-03 | 2021-08-19 | ブルー キューブ アイピー エルエルシー | ジェットループ反応器中の塩素化アルカンの苛性脱塩化水素により塩素化アルケンを調製するための改善されたプロセス |
Family Cites Families (197)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2630461A (en) | 1953-03-03 | Production of acetylene by incom | ||
US2119484A (en) | 1935-05-06 | 1938-05-31 | Du Pont | Chlorination of propylene dichloride |
GB471186A (en) | 1936-02-28 | 1937-08-30 | Du Pont | Improvements in or relating to the manufacture of chlorine derivatives of unsaturated hydrocarbons |
GB471187A (en) | 1936-02-28 | 1937-08-30 | Du Pont | Improvements in or relating to the manufacture of chlorinated hydrocarbons |
GB471188A (en) | 1936-02-28 | 1937-08-30 | Du Pont | Improvements in or relating to the manufacture of chlorinated hydrocarbons |
US2179378A (en) | 1936-07-18 | 1939-11-07 | Air Reduction | Production of acetylene |
US2207193A (en) | 1937-09-14 | 1940-07-09 | Shell Dev | Production of allyl type halides |
US2299441A (en) | 1939-09-02 | 1942-10-20 | Shell Dev | Catalytic halo-substitution of saturated organic compounds |
US2302228A (en) * | 1940-04-02 | 1942-11-17 | Du Pont | Method of chlorination with sulphuryl chloride and production of monochloro-trimethyl acetic acid |
US2370342A (en) | 1940-04-30 | 1945-02-27 | Tide Water Associated Oil Comp | Halogenation |
US2378859A (en) | 1941-08-08 | 1945-06-19 | Distillers Co Yeast Ltd | Splitting-off of hydrogen halide from halogenated hydrocarbons |
US2449286A (en) | 1945-07-16 | 1948-09-14 | Shell Dev | Production of 1, 3-dihalopropylenes |
US2435983A (en) | 1945-12-01 | 1948-02-17 | Universal Oil Prod Co | Production of liquid hydrocarbons |
US2588867A (en) | 1948-10-25 | 1952-03-11 | Dow Chemical Co | Pyrolytic production of chlorohydrocarbons |
US2688592A (en) | 1950-10-21 | 1954-09-07 | Diamond Alkali Co | Photochemical process for preparing carbon tetrachloride |
DE857955C (de) | 1951-03-23 | 1952-12-04 | Basf Ag | Verfahren zur Herstellung von Tetrachloraethylen neben Tetrachlorkohlenstoff |
US2762611A (en) | 1952-02-28 | 1956-09-11 | Pfaudler Co Inc | Tubular heat exchangers |
US2765359A (en) | 1953-02-10 | 1956-10-02 | Hydrocarbon Research Inc | Production of acetylene |
GB857086A (en) | 1956-08-30 | 1960-12-29 | Hoechst Ag | Process for the manufacture of carbon tetrachloride |
US3000980A (en) | 1958-04-07 | 1961-09-19 | Dow Chemical Co | Preparation of alkyl bromides |
US2973393A (en) | 1958-10-02 | 1961-02-28 | Dow Chemical Co | Chlorination of acetylenes |
US2964579A (en) | 1958-10-09 | 1960-12-13 | Houdry Process Corp | Selective hydrogenation of diolefins with copper chromite catalyst |
US3094567A (en) | 1960-02-25 | 1963-06-18 | Monsanto Chemicals | Chlorination of propynes |
US3112988A (en) | 1960-02-26 | 1963-12-03 | Sheil Oil Company | Mixing gases at supersonic velocity |
US3819731A (en) | 1960-03-23 | 1974-06-25 | Stauffer Chemical Co | Production of chlorinated unsaturated hydrocarbons |
BE622938A (ja) | 1961-09-28 | |||
US3446859A (en) | 1962-06-11 | 1969-05-27 | Hooker Chemical Corp | Vapor phase condensation process |
DE1570555A1 (de) | 1965-03-26 | 1970-01-29 | Bayer Ag | Verfahren zur Herstellung von Polyamidschaeumen |
US3502734A (en) | 1966-05-11 | 1970-03-24 | Du Pont | Process for partially chlorinating methyl chloride and/or methylene chloride |
ES332724A1 (es) | 1966-06-07 | 1967-12-01 | El Paso Products Co | Un procedimiento para la produccion de diolefinas. |
DE1568921A1 (de) | 1966-07-22 | 1970-03-26 | Knapsack Ag | Verfahren zur gemeinsamen Herstellung von 2,2,3- und 1,2,3-Trichlorbutan |
US3444263A (en) | 1966-11-09 | 1969-05-13 | Gulf Research Development Co | Method for converting ethylene to alpha olefins in the presence of an organic sulfide |
CH526333A (de) | 1967-05-19 | 1972-08-15 | Bayer Ag | Verfahren und Vorrichtung zur Durchführung von Reaktionen zwischen Gasen |
FR1546709A (fr) | 1967-10-10 | 1968-11-22 | Mini Ind Chimice | Procédé et appareil pour la fabrication en système continu de nitrosodérivés d'hydrocarbures |
DE1904426C3 (de) | 1969-01-30 | 1974-02-28 | Farbwerke Hoechst Ag, Vormals Meister Lucius & Bruening, 6000 Frankfurt | Verfahren zur Herstellung von Tetrachlorkohlenstoff aus Benzol und Chlor |
US3558438A (en) | 1968-10-30 | 1971-01-26 | Du Pont | Distillation process and apparatus |
US3551512A (en) | 1968-11-01 | 1970-12-29 | Diamond Shamrock Corp | Pressure process for preparing acetylene |
CA990738A (en) | 1971-07-30 | 1976-06-08 | Bruce E. Kurtz | Isothermal chlorination of methane, ethane and other compounds in a porous tube reactor |
US4513154A (en) | 1971-07-30 | 1985-04-23 | Allied Corporation | Process for consecutive competitive gas phase reaction |
US3823195A (en) * | 1971-12-27 | 1974-07-09 | Monsanto Co | Preparation of 1,1,2,3-tetrachloropropene from 1,2,3-trichloropropane |
NL160542C (nl) | 1971-12-17 | 1979-11-15 | Monsanto Co | Werkwijze voor het bereiden van 1,1,2,3,-tetrachloorpro- peen. |
US3926758A (en) | 1971-12-27 | 1975-12-16 | Monsanto Co | Preparation of 1,1,2,3-tetrachloropropene from 2,3-trichloropropane |
DE2257005A1 (de) | 1972-11-21 | 1974-05-22 | Merck Patent Gmbh | Loesungsmittel fuer die kernresonanzspektroskopie |
CH609022A5 (en) | 1973-06-12 | 1979-02-15 | Monsanto Co | Process for the preparation of 1,2,3-trichloropropene from 1,2,3-trichloropropane |
NL7313098A (ja) | 1973-09-22 | 1974-03-25 | ||
US3872664A (en) | 1973-10-15 | 1975-03-25 | United Aircraft Corp | Swirl combustor with vortex burning and mixing |
US3914167A (en) | 1974-08-26 | 1975-10-21 | Dow Chemical Co | Process for making cis-1,3-dichloropropene |
US4051182A (en) * | 1976-04-12 | 1977-09-27 | Stauffer Chemical Company | Process for the manufacture of α-chloropropionyl chloride |
US4038372A (en) | 1976-05-05 | 1977-07-26 | The United States Of America As Represented By The Secretary Of The Navy | Process for manufacturing chloramine |
US4319062A (en) | 1976-08-02 | 1982-03-09 | The Dow Chemical Company | Allyl chloride process |
JPS5479207A (en) | 1977-12-05 | 1979-06-25 | Showa Denko Kk | Preparation of 1,3-dichloropropene |
JPS54135712A (en) | 1978-04-13 | 1979-10-22 | Osaka Soda Co Ltd | Prepartion of 3-chloropropene |
SU899523A1 (ru) | 1979-07-03 | 1982-01-23 | Уфимский Нефтяной Институт | Способ получени 1,1,2,3-тетрахлорпропена |
AU563307B2 (en) | 1981-09-01 | 1987-07-02 | G.A. Olah | Methyl halides and methyl alcohol from methane |
US4535194A (en) | 1983-07-06 | 1985-08-13 | Monsanto Co. | Process for producing 1,1,2,3-tetrachloropropene |
US4650914A (en) | 1983-07-06 | 1987-03-17 | Monsanto Company | Process for producing 1,1,2,3-tetrachloropropene |
DE3415334A1 (de) | 1983-08-25 | 1985-03-14 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur herstellung von 1,1,2-trichlor-2-methyl-propan |
DE3415337A1 (de) | 1983-08-25 | 1985-03-14 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur herstellung von 3,3-dichlor-2-methyl-propen |
DE3415336A1 (de) | 1984-04-25 | 1985-10-31 | Chemische Werke Hüls AG, 4370 Marl | Verfahren zur herstellung von 1,2,3-trichlor-2-methyl-propan |
FR2569182B1 (fr) | 1984-08-20 | 1986-12-05 | Solvay | Procede pour effectuer des reactions de chloration substitutive de composes organiques au moyen de chlore moleculaire en presence d'un produit chlore servant d'initiateur radicalaire et initiateurs radicalaires utilises dans un tel procede |
DE3432720A1 (de) | 1984-09-06 | 1986-03-06 | Hüls AG, 4370 Marl | Verfahren zur herstellung von 1,2,3-trichlorpropan |
US4614572A (en) | 1985-07-08 | 1986-09-30 | The Dow Chemical Company | Liquid phase chlorination of chlorinated methanes |
DE3681768D1 (de) | 1985-07-30 | 1991-11-07 | Hartmut Wolf | Zerstaeubungsvorrichtung. |
US4644907A (en) | 1985-11-29 | 1987-02-24 | Hunter Edward H | Boiler tubes of enhanced efficiency and method of producing same |
US4727181A (en) | 1986-04-21 | 1988-02-23 | The Dow Chemical Company | Process for the preparation of α-halocinnamate esters |
GB8708618D0 (en) | 1987-04-10 | 1987-05-13 | Ici Plc | Production process |
GB8721964D0 (en) | 1987-09-18 | 1987-10-28 | Shell Int Research | Multitube reactor |
JPH01290639A (ja) | 1988-05-17 | 1989-11-22 | Daikin Ind Ltd | 1,1,1−トリフルオロ−2,2−ジクロロエタンの製造法 |
US5171899A (en) | 1988-05-17 | 1992-12-15 | Daikin Industries Ltd. | Process for production of 1,1,1-trifluoro-2,2-dichloroethane |
US4999102A (en) | 1988-12-16 | 1991-03-12 | The Amalgamated Sugar Company | Liquid transfer manifold system for maintaining plug flow |
US5254771A (en) | 1989-07-14 | 1993-10-19 | Hoechst Aktiengesellschaft | Process for the preparation of 1,1,1-trifluoro-2-2-dichloroethane under elevated pressure |
US5614323A (en) | 1989-11-20 | 1997-03-25 | Eastman Chemical Company | Powder coating compositions |
US5057634A (en) | 1989-12-19 | 1991-10-15 | E. I. Du Pont De Nemours And Company | Multistep synthesis of hexafluoropropylene |
US5178844A (en) | 1990-04-03 | 1993-01-12 | Phillips Petroleum Company | Method and apparatus for producing nitride products |
DE4012007A1 (de) | 1990-04-13 | 1991-10-17 | Erdoelchemie Gmbh | Verfahren zur reduktiven dehydrohalogenierung von halogenkohlenwasserstoffen und halogenethern |
GB9105167D0 (en) | 1991-03-12 | 1991-04-24 | Ici Plc | Chemical process |
US5254788A (en) | 1991-09-10 | 1993-10-19 | Stone And Webster Engineering Corporation | Process for the production of olefins from light paraffins |
US5262575A (en) | 1992-08-04 | 1993-11-16 | The Dow Chemical Company | Production of allylic chlorides |
JP2813100B2 (ja) | 1992-10-23 | 1998-10-22 | 株式会社トクヤマ | アリルクロライドの製造方法および製造装置 |
GB9315450D0 (en) | 1993-07-26 | 1993-09-08 | Zeneca Ltd | Chlorination process |
US5414166A (en) | 1993-11-29 | 1995-05-09 | Korea Institute Of Science And Technology | Process for the preparation of 1,1,1-trifluoro-2,2-dichloroethane |
JPH08119885A (ja) | 1994-10-25 | 1996-05-14 | Central Glass Co Ltd | フッ素化炭化水素の製造方法 |
US5504266A (en) | 1995-05-24 | 1996-04-02 | The Dow Chemical Company | Process to make allyl chloride and reactor useful in that process |
US5616819A (en) | 1995-08-28 | 1997-04-01 | Laroche Industries Inc. | Process for preparing fluorinated aliphatic compounds |
US6235951B1 (en) | 1996-01-17 | 2001-05-22 | Central Glass Company, Limited | Method for producing 1,1,1,3,3-pentafluoropropane |
US5689020A (en) | 1996-03-11 | 1997-11-18 | Laroche Industries Inc. | High temperature chlorination process for the preparation of polychloroolefins |
US6111150A (en) | 1996-06-20 | 2000-08-29 | Central Glass Company, Limited | Method for producing 1,1,1,3,3,-pentafluoropropane |
US6538167B1 (en) | 1996-10-02 | 2003-03-25 | Exxonmobil Chemical Patents Inc. | Process for producing light olefins |
US5986151A (en) | 1997-02-05 | 1999-11-16 | Alliedsignal Inc. | Fluorinated propenes from pentafluoropropane |
US5811605A (en) | 1997-02-19 | 1998-09-22 | Ppg Industries, Inc. | Preparation of 1,2,3,3-tetrachloropropene |
US5895825A (en) | 1997-12-01 | 1999-04-20 | Elf Atochem North America, Inc. | Preparation of 1,1,1,3,3-pentafluoropropane |
KR100624998B1 (ko) | 1997-12-18 | 2006-09-20 | 다우 글로벌 테크놀로지스 인크. | 단열 반응기 시스템에서 글리콜을 제조하는 방법 |
JP3518321B2 (ja) | 1998-03-23 | 2004-04-12 | ダイキン工業株式会社 | 1,1,1,3,3−ペンタフルオロプロパンの製造方法 |
US6187976B1 (en) | 1998-04-09 | 2001-02-13 | Alliedsignal Inc. | Process for the preparation of fluorine containing hydrohalocarbons |
EP0999200B1 (en) | 1998-11-04 | 2002-07-17 | Rohm And Haas Company | Process for the high yield production of methyl methacrylate or methacrylic acid |
JP4341087B2 (ja) * | 1998-11-24 | 2009-10-07 | 住友化学株式会社 | 1,1,3−トリクロロ−1−プロペンの製造方法 |
US6273180B1 (en) | 1998-12-23 | 2001-08-14 | L'air Liquide, Societe Anonyme Pour L'etude Et L'eploitation Des Procedes Georges Claude | Heat exchanger for preheating an oxidizing gas |
TW527218B (en) | 1999-03-16 | 2003-04-11 | Basf Ag | Multitube reactor, especially for catalytic gas-phase reactions |
EP1060788A1 (en) | 1999-06-15 | 2000-12-20 | Methanol Casale S.A. | Isothermal catalytic reactor for exothermic or endothermic heterogeneous reactions |
DE50011826D1 (de) | 1999-06-16 | 2006-01-12 | Solvay Fluor Gmbh | Uv-aktivierte chlorierung |
DE19952754A1 (de) | 1999-11-02 | 2001-05-10 | Krc Umwelttechnik Gmbh | Verfahren und Vorrichtung zur Kühlung und Reinigung von Vergasungsgasen |
JP3869170B2 (ja) | 1999-11-22 | 2007-01-17 | セントラル硝子株式会社 | 1,1,1,3,3−ペンタクロロプロパンの製造方法 |
JP5053493B2 (ja) | 1999-11-22 | 2012-10-17 | ダウ グローバル テクノロジーズ エルエルシー | エチレンを塩化ビニルに転化する方法および該方法のために有用な新規触媒組成物 |
US6118018A (en) | 1999-12-06 | 2000-09-12 | Occidental Chemical Corporation | Chlorination and bromination of aromatic compounds at atmospheric pressure |
JP2001213820A (ja) | 2000-01-31 | 2001-08-07 | Central Glass Co Ltd | 1,1,1,3,3−ペンタクロロプロパンの製造方法 |
US6613127B1 (en) | 2000-05-05 | 2003-09-02 | Dow Global Technologies Inc. | Quench apparatus and method for the reformation of organic materials |
DE10054840A1 (de) | 2000-11-04 | 2002-08-08 | Xcellsis Gmbh | Verfahren und Vorrichtung zum Starten eines Reaktors in einem Gaserzeugungssystem |
US6518467B2 (en) | 2000-12-29 | 2003-02-11 | Honeywell International Inc. | Method of making hydrofluorocarbons and hydrochlorofluorocarbons |
US6551469B1 (en) | 2001-11-27 | 2003-04-22 | Honeywell International | Photochlorination of 1,1,1,3,3-pentafluoropropane |
CN1277790C (zh) | 2002-01-11 | 2006-10-04 | 三菱化学株式会社 | 多管反应器,使用多管反应器的气相催化氧化法,和应用于多管反应器的启动方法 |
US7117934B2 (en) | 2002-03-15 | 2006-10-10 | H2Gen Innovations, Inc. | Method and apparatus for minimizing adverse effects of thermal expansion in a heat exchange reactor |
US6924403B2 (en) | 2002-06-26 | 2005-08-02 | E. I. Du Pont De Nemours And Company | Synthesis of hexafluoropropylene |
US6683216B1 (en) | 2002-11-06 | 2004-01-27 | Eastman Chemical Company | Continuous process for the preparation of amines |
GB0301660D0 (en) | 2003-01-24 | 2003-02-26 | Redding John | Dredging scouring & excavation |
SI1587612T1 (sl) | 2003-01-31 | 2019-01-31 | Man Energy Solutions Se | Oplaščen cevni reaktor za izvedbo katalitičnih reakcij v plinski fazi in postopek za obratovanje le-tega |
JP2007524719A (ja) | 2003-03-07 | 2007-08-30 | ダウ グローバル テクノロジーズ インコーポレイティド | ポリエーテルポリオール製造連続方法及びシステム |
WO2005005037A1 (ja) | 2003-07-14 | 2005-01-20 | Mitsubishi Rayon Co., Ltd. | 固定床多管式反応器 |
US7345209B2 (en) | 2004-04-29 | 2008-03-18 | Honeywell International Inc. | Processes for synthesis of 1,3,3,3-tetrafluoropropene |
US7880040B2 (en) | 2004-04-29 | 2011-02-01 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
MXPA06001255A (es) | 2003-07-31 | 2006-05-15 | Dow Global Technologies Inc | Proceso de oxidacion, y reactor con sistema de alimentacion modificado. |
US20060292046A1 (en) | 2003-07-31 | 2006-12-28 | Dow Global Technologies Inc. | Oxidation process and reactor with modified feed system |
US6825383B1 (en) | 2003-09-22 | 2004-11-30 | Council Of Scientific And Industrial Research | Catalytic process for regiospecific chlorination of alkanes, alkenes and arenes |
US7951982B2 (en) | 2004-04-29 | 2011-05-31 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
US8084653B2 (en) * | 2004-04-29 | 2011-12-27 | Honeywell International, Inc. | Method for producing fluorinated organic compounds |
CA2564991C (en) | 2004-04-29 | 2013-03-19 | Honeywell International Inc. | Processes for synthesis of 1,3,3,3-tetrafluoropropene and 2,3,3,3-tetrafluoropropene |
MXPA06012467A (es) | 2004-04-29 | 2007-01-29 | Honeywell Int Inc | Procesos para la sintesis de 1,3,3,3-tetrafluoropropeno. |
US9102579B2 (en) | 2004-04-29 | 2015-08-11 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
US7659434B2 (en) | 2004-04-29 | 2010-02-09 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
US7674939B2 (en) | 2004-04-29 | 2010-03-09 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
US8383867B2 (en) | 2004-04-29 | 2013-02-26 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
US8058486B2 (en) | 2004-04-29 | 2011-11-15 | Honeywell International Inc. | Integrated process to produce 2,3,3,3-tetrafluoropropene |
US20080021229A1 (en) | 2004-05-21 | 2008-01-24 | Maughon Bob R | Process for Preparing Epichlorhydrin from Ethane |
MY142153A (en) | 2004-12-10 | 2010-09-30 | Shell Int Research | Reactor tube apparatus |
JP5027670B2 (ja) | 2004-12-22 | 2012-09-19 | イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー | 光化学反応用の末端官能化パーフルオロ(アルキルビニルエーテル)反応器壁の官能化共重合体、炭化水素およびハロ炭化水素中のフッ素含有率の増加方法およびオレフィン製造方法 |
JP4501158B2 (ja) | 2005-03-30 | 2010-07-14 | 富士フイルム株式会社 | マイクロ化学装置の運転方法 |
US7396965B2 (en) | 2005-05-12 | 2008-07-08 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
US7511101B2 (en) | 2005-05-13 | 2009-03-31 | Fina Technology, Inc. | Plug flow reactor and polymers prepared therewith |
JP2007021396A (ja) | 2005-07-19 | 2007-02-01 | Japan Science & Technology Agency | 重金属の除去方法 |
WO2007018298A1 (en) | 2005-08-09 | 2007-02-15 | Canon Kabushiki Kaisha | Fluid-processing device and fluid-processing method |
DE102005044501A1 (de) | 2005-09-16 | 2007-03-22 | Roquette, Eberhard, Dipl.-Ing. | Veresterungsdüse |
EP2546225B1 (en) | 2006-01-03 | 2017-12-20 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
US8071825B2 (en) | 2006-01-03 | 2011-12-06 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
CN103193584B (zh) | 2006-01-03 | 2015-07-01 | 霍尼韦尔国际公司 | 制备氟化有机化合物的方法 |
US7695695B2 (en) | 2006-01-18 | 2010-04-13 | Lg Chem, Ltd. | Reactor or heat exchanger with improved heat transfer performance |
DE102007008876A1 (de) | 2006-02-21 | 2007-12-27 | Sachtleben Chemie Gmbh | Verfahren zur Durchführung chemischer und physikalischer Prozesse und Reaktionszelle |
CN101415664B (zh) | 2006-03-31 | 2012-05-30 | 纳幕尔杜邦公司 | 氢氟烯烃的同时制备 |
US7836941B2 (en) | 2006-05-19 | 2010-11-23 | Exxonmobil Research And Engineering Company | Mitigation of in-tube fouling in heat exchangers using controlled mechanical vibration |
US20080073063A1 (en) | 2006-06-23 | 2008-03-27 | Exxonmobil Research And Engineering Company | Reduction of fouling in heat exchangers |
FR2902785B1 (fr) | 2006-06-26 | 2008-08-08 | Solvay | Procede de fabrication de 1,2-dichloroethane |
JP2008063314A (ja) | 2006-09-04 | 2008-03-21 | Tokyo Kasei Kogyo Kk | 環境調和型超原子価ヨウ素試剤 |
WO2008030441A1 (en) | 2006-09-05 | 2008-03-13 | E. I. Du Pont De Nemours And Company | 1,2,3,3,3-pentafluoropropene production processes |
US8398882B2 (en) | 2006-10-31 | 2013-03-19 | E I Du Pont De Nemours And Company | Processes for the production of fluoropropanes and halopropenes and azeotropic compositions of 2-chloro-3,3,3-trifluoro-1-propene with HF and of 1,1,1,2,2-pentafluoropropane with HF |
US20080207962A1 (en) | 2007-02-23 | 2008-08-28 | Velliyur Nott Mallikarjuna Rao | Compositions containing chromium, oxygen, and at least two modifier metals selected the group consisting of gold, silver, and palladium, their preparation, and their use as catalysts and catalyst precursors |
EP2135888A4 (en) | 2007-04-10 | 2014-10-01 | Asahi Glass Co Ltd | COMPOUND CATALYST OF METAL CYANIDE COMPLEX WITH ORGANIC LIGAND, METHOD OF MANUFACTURING THEREOF, AND METHOD FOR PRODUCING POLYETHEREPOLYOLE |
JP2009000592A (ja) | 2007-06-19 | 2009-01-08 | Hitachi Ltd | 反応器および反応システム |
JP2010531897A (ja) | 2007-06-27 | 2010-09-30 | アーケマ・インコーポレイテッド | ヒドロフルオロオレフィンを製造する2段階法 |
KR101550250B1 (ko) | 2007-06-27 | 2015-09-04 | 알케마 인코포레이티드 | 하이드로플루오로올레핀의 제조 방법 |
US20090018377A1 (en) | 2007-07-09 | 2009-01-15 | Boyce C Bradford | Catalytic process for the preparation of fluorinated halocarbons |
JP5339229B2 (ja) | 2007-07-24 | 2013-11-13 | ナガセケムテックス株式会社 | 超原子価ヨウ素反応剤を用いる芳香族化合物および複素環式芳香族化合物のポリマーの製造方法 |
US8258355B2 (en) | 2007-07-25 | 2012-09-04 | Honeywell International Inc. | Processes for preparing 1,1,2,3-tetrachloropropene |
US9035111B2 (en) | 2007-08-22 | 2015-05-19 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
EP2190954A1 (de) | 2007-09-18 | 2010-06-02 | Uhde GmbH | Vergasungsreaktor und verfahren zur flugstromvergasung |
PL2197837T3 (pl) | 2007-10-04 | 2014-07-31 | Urea Casale Sa | Proces i instalacja do wytwarzania mocznika |
US9079818B2 (en) | 2007-10-15 | 2015-07-14 | Honeywell International Inc. | Process for synthesis of fluorinated olefins |
WO2009061954A1 (en) | 2007-11-06 | 2009-05-14 | Quantumsphere, Inc. | System and method for ammonia synthesis |
KR20100099182A (ko) | 2007-11-20 | 2010-09-10 | 이 아이 듀폰 디 네모아 앤드 캄파니 | 하이드로플루오로알칸올 및 하이드로플루오로알켄의 합성 |
JP5508281B2 (ja) | 2007-12-19 | 2014-05-28 | オクシデンタル ケミカル コーポレイション | 塩素化された炭化水素を作る方法 |
GB0800470D0 (en) | 2008-01-11 | 2008-02-20 | Redding John | Improvements in or relating to jet nozzles |
CN101597209A (zh) | 2008-03-20 | 2009-12-09 | 霍尼韦尔国际公司 | 用于制备2,3,3,3-四氟丙烯的一体式方法 |
US8071826B2 (en) | 2008-04-04 | 2011-12-06 | Honeywell International Inc. | Process for the preparation of 2,3,3,3-tetrafluoropropene (HFO-1234yf) |
KR101639087B1 (ko) | 2008-08-07 | 2016-07-13 | 바스프 에스이 | 방향족 이소시아네이트의 제조 방법 |
MX2011003147A (es) | 2008-09-25 | 2011-05-25 | Central Glass Co Ltd | Proceso para producir 1,3,3,3-tetrafluoropropeno. |
CN105646136A (zh) | 2008-10-13 | 2016-06-08 | 蓝立方知识产权公司 | 用于生产氯化和/或氟化丙烯的方法 |
JP5571681B2 (ja) | 2008-11-19 | 2014-08-13 | アーケマ・インコーポレイテッド | ヒドロフルオロオレフィンを製造するための方法 |
JP5582036B2 (ja) | 2008-12-25 | 2014-09-03 | 旭硝子株式会社 | 1,1−ジクロロ−2,3,3,3−テトラフルオロプロペンおよび2,3,3,3−テトラフルオロプロペンの製造方法 |
CN101492341B (zh) | 2009-03-05 | 2012-03-28 | 杨海珍 | 饱和多氯代烷烃的制备方法 |
KR101374000B1 (ko) | 2009-04-23 | 2014-03-12 | 다이킨 고교 가부시키가이샤 | 2,3,3,3-테트라플루오로프로펜의 제조 방법 |
CN101544535B (zh) | 2009-05-01 | 2012-07-18 | 浙江三美化工股份有限公司 | 一种合成1,1,1,3,3-五氯丙烷的制备方法 |
EP2429977B1 (en) | 2009-05-13 | 2014-11-05 | Daikin Industries, Ltd. | Process for preparing chlorine-containing fluorocarbon compound |
US8581011B2 (en) | 2009-10-09 | 2013-11-12 | Dow Global Technologies, Llc | Process for the production of chlorinated and/or fluorinated propenes |
CN102686544B (zh) | 2009-10-09 | 2017-02-15 | 蓝立方知识产权公司 | 用于生产氯化和/或氟化丙烯和高级烯烃的方法 |
CN102639475A (zh) | 2009-11-16 | 2012-08-15 | 阿科玛股份有限公司 | 纯化和稳定化氯烯烃的方法 |
CN102630221B (zh) | 2009-11-27 | 2015-03-25 | 大金工业株式会社 | 制备1,1,2,3-四氯丙烯的方法 |
WO2011077191A1 (en) | 2009-12-23 | 2011-06-30 | Arkema France | Catalytic gas phase fluorination of 1230xa to 1234yf |
JP2011144148A (ja) | 2010-01-18 | 2011-07-28 | Nippon Zeon Co Ltd | 含水素ハロゲン化シクロペンタン、及びヘプタフルオロシクロペンテンの製造方法 |
CN101955414A (zh) | 2010-04-20 | 2011-01-26 | 南通泰禾化工有限公司 | 1,1,2,3-四氯丙烯生产工艺 |
DE102010022414A1 (de) | 2010-06-01 | 2011-12-01 | Günther Kramb jun. | Emulgiervorrichtung |
WO2012011844A1 (ru) | 2010-07-21 | 2012-01-26 | Открытое Акционерное Общество "Научно-Исследовательский И Проектный Институт Карбамида И Продуктов Органического Синтеза" (Оао Ниик) | Газожидкостный реактор (варианты) |
CN101913980A (zh) | 2010-09-07 | 2010-12-15 | 西安近代化学研究所 | 1,1,1,3,3-五氯丙烷的生产方法 |
CN101913979A (zh) | 2010-09-07 | 2010-12-15 | 西安近代化学研究所 | 1,1,1,3,3-五氯丁烷的生产方法 |
CN101982227B (zh) | 2010-09-15 | 2013-03-20 | 山东东岳高分子材料有限公司 | 一种用于高温裂解的气体快速混合反应装置及应用 |
CN102001911B (zh) | 2010-09-20 | 2013-09-25 | 西安近代化学研究所 | 2,3,3,3-四氟丙烯的制备方法 |
WO2012081482A1 (ja) | 2010-12-16 | 2012-06-21 | 株式会社トクヤマ | 炭素数3の塩素化炭化水素の製造方法 |
CA2836493A1 (en) | 2011-05-31 | 2012-12-06 | Max Markus Tirtowidjojo | Process for the production of chlorinated propenes |
CN102249846B (zh) | 2011-05-31 | 2013-05-08 | 浙江师范大学 | 一种2-氯-3, 3, 3-三氟丙烯和2, 3-二氯-1, 1-二氟丙烯的联产制备方法 |
US9056808B2 (en) | 2011-05-31 | 2015-06-16 | Dow Global Technologies, Llc | Process for the production of chlorinated propenes |
CN102351637B (zh) | 2011-08-31 | 2013-10-23 | 浙江师范大学 | 一种2, 3, 3, 3-四氟丙烯的制备方法 |
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