JP5527915B2 - 水溶性ポリビニルアルコール（コ）ポリマーを有する電着塗料浴 - Google Patents

水溶性ポリビニルアルコール（コ）ポリマーを有する電着塗料浴 Download PDF

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Publication number
JP5527915B2
JP5527915B2 JP2001508277A JP2001508277A JP5527915B2 JP 5527915 B2 JP5527915 B2 JP 5527915B2 JP 2001508277 A JP2001508277 A JP 2001508277A JP 2001508277 A JP2001508277 A JP 2001508277A JP 5527915 B2 JP5527915 B2 JP 5527915B2
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JP
Japan
Prior art keywords
ethylenically unsaturated
vinyl alcohol
unsaturated monomer
copolymer
aqueous
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
JP2001508277A
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English (en)
Japanese (ja)
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JP2003504448A (ja
JP2003504448A5 (de
Inventor
ロイター ハーディ
シェムシャト ダグマール
グローセ−ブリンクハウス カール−ハインツ
ハイマン ウルリッヒ
ヨウク ヴァルター
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BASF Coatings GmbH
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BASF Coatings GmbH
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Filing date
Publication date
Application filed by BASF Coatings GmbH filed Critical BASF Coatings GmbH
Publication of JP2003504448A publication Critical patent/JP2003504448A/ja
Publication of JP2003504448A5 publication Critical patent/JP2003504448A5/ja
Application granted granted Critical
Publication of JP5527915B2 publication Critical patent/JP5527915B2/ja
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D13/00—Electrophoretic coating characterised by the process
    • C25D13/22—Servicing or operating apparatus or multistep processes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S524/00—Synthetic resins or natural rubbers -- part of the class 520 series
    • Y10S524/901—Electrodepositable compositions

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Paints Or Removers (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
  • Chemically Coating (AREA)
JP2001508277A 1999-06-30 2000-06-29 水溶性ポリビニルアルコール（コ）ポリマーを有する電着塗料浴 Expired - Lifetime JP5527915B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE19930060A DE19930060A1 (de) 1999-06-30 1999-06-30 Elektrotauchlackbad mit wasserlöslichem Polyvinylalkohol(co)polymeren
DE19930060.7 1999-06-30
PCT/EP2000/006035 WO2001002498A1 (de) 1999-06-30 2000-06-29 Elektrotauchlackbad mit wasserlöslichen polyvinylalkohol(co)polymeren

Publications (3)

Publication Number Publication Date
JP2003504448A JP2003504448A (ja) 2003-02-04
JP2003504448A5 JP2003504448A5 (de) 2013-10-24
JP5527915B2 true JP5527915B2 (ja) 2014-06-25

Family

ID=7913117

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2001508277A Expired - Lifetime JP5527915B2 (ja) 1999-06-30 2000-06-29 水溶性ポリビニルアルコール（コ）ポリマーを有する電着塗料浴

Country Status (9)

Country Link
US (1) US6951602B1 (de)
EP (1) EP1192226B1 (de)
JP (1) JP5527915B2 (de)
AT (1) ATE297967T1 (de)
AU (1) AU5979800A (de)
BR (1) BR0012095B1 (de)
DE (2) DE19930060A1 (de)
ES (1) ES2243279T3 (de)
WO (1) WO2001002498A1 (de)

Families Citing this family (36)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10009913B4 (de) * 2000-03-01 2004-12-23 Basf Coatings Ag Verfahren zur Herstellung von Mehrschichtlackierungen auf elektrisch leitfähigen Substraten und deren Verwendung
DE10209396A1 (de) * 2002-03-02 2003-09-18 Basf Coatings Ag Von unlöslichen Festkörpern freie Elekrotauchlacke (ETL)
JP2004197073A (ja) * 2002-12-02 2004-07-15 Sankyo Seiki Mfg Co Ltd 電着材料、およびモータ、並びにレンズ駆動装置
US7930815B2 (en) 2003-04-11 2011-04-26 Avery Dennison Corporation Conductive pattern and method of making
US20040200061A1 (en) * 2003-04-11 2004-10-14 Coleman James P. Conductive pattern and method of making
TWI328622B (en) * 2005-09-30 2010-08-11 Rohm & Haas Elect Mat Leveler compounds
US7381331B2 (en) * 2005-09-30 2008-06-03 General Electric Company Hydrophilic membrane and associated method
US8389653B2 (en) * 2006-03-30 2013-03-05 Basf Corporation Method of catalyzing a reaction to form a urethane coating and a complex for use in the method
US7374686B2 (en) * 2006-04-11 2008-05-20 Basf Corporation Electrocoat manufacturing process
US20080289968A1 (en) * 2007-05-25 2008-11-27 Basf Corporation Method of coating a substrate including a simultaneous cure
US8062760B2 (en) * 2008-06-19 2011-11-22 Basf Coatings Gmbh Electrocoat composition and process
MX2015003384A (es) 2012-11-09 2015-06-05 Basf Coatings Gmbh Metodo para mejorar el curado del revestimiento para articulo revestido en composicion de revestimiento para electrorrevestimiento, contaminada con fosfato, y composicion de revestimiento para electrorrevestimiento.
WO2015070929A1 (de) 2013-11-18 2015-05-21 Basf Coatings Gmbh Zweistufiges verfahren zur tauchlack-beschichtung elektrisch leitfähiger substrate unter verwendung einer bi(iii)-haltigen zusammensetzung
KR102359012B1 (ko) 2013-12-18 2022-02-08 바스프 코팅스 게엠베하 멀티코트 페인트 시스템을 금속 기판 상에 제조하는 방법 및 이에 의해 제조되는 멀티코트 페인트 시스템
MX2016007692A (es) 2013-12-18 2016-09-07 Basf Coatings Gmbh Metodo para producir un sistema de pintura multicapa.
EP2886207A1 (de) 2013-12-18 2015-06-24 BASF Coatings GmbH Verfahren zur Herstellung einer Mehrschichtlackierung
US10287452B2 (en) 2013-12-18 2019-05-14 Basf Coatings Gmbh Method for producing a multicoat paint system
EP3292164B1 (de) 2015-05-06 2021-12-08 BASF Coatings GmbH Verfahren zur herstellung einer mehrschichtlackierung
CA3004781C (en) 2015-11-26 2020-08-25 Basf Coatings Gmbh Method for producing a multicoat paint system
US10718059B2 (en) * 2017-07-10 2020-07-21 Rohm And Haas Electronic Materials Llc Nickel electroplating compositions with cationic polymers and methods of electroplating nickel
US11111372B2 (en) 2017-10-09 2021-09-07 Owens Corning Intellectual Capital, Llc Aqueous binder compositions
US11692105B2 (en) 2017-10-09 2023-07-04 Basf Coatings Gmbh Electrocoats containing at least one triazine compound
KR102594229B1 (ko) * 2017-10-09 2023-10-25 오웬스 코닝 인텔렉츄얼 캐피탈 엘엘씨 수성 결합제 조성물
MX2021004131A (es) 2018-10-12 2021-06-15 Basf Coatings Gmbh Metodo para producir un sistema de pintura multicapa por pos-adicion de al menos una capa base con una dispersion acuosa que comprende poliamidas y/o ceras de amida.
CN114025888B (zh) 2019-07-29 2023-07-25 巴斯夫涂料有限公司 制备包含闪光涂层的多层涂层的方法以及由所述方法获得的多层涂层
US20240141180A1 (en) 2019-10-23 2024-05-02 Basf Coatings Gmbh Pigmented Aqueous Coating Composition with Improved Stability Towards Pinholes
US11813833B2 (en) 2019-12-09 2023-11-14 Owens Corning Intellectual Capital, Llc Fiberglass insulation product
US20210238439A1 (en) 2019-12-30 2021-08-05 Axalta Coating Systems Ip Co., Llc Low density electrocoat composition with improved throwing power
US20210371678A1 (en) 2020-05-28 2021-12-02 Axalta Coating Systems Ip Co., Llc Electrocoating composition
WO2021261372A1 (ja) * 2020-06-23 2021-12-30 関西ペイント株式会社 カチオン電着塗料組成物
MX2023010568A (es) * 2021-03-10 2023-09-21 Basf Coatings Gmbh Dispersiones acuosas que contienen particulas polimericas modificadas con alcohol polivinilico cationico y material acuoso de electrorrecubrimiento que contienen dichas dispersiones.
EP4363509A1 (de) * 2021-07-01 2024-05-08 PPG Industries Ohio Inc. Elektroabscheidbare beschichtungszusammensetzungen
CA3222684A1 (en) * 2021-07-01 2023-01-05 Brian Carl OKERBERG Electrodepositable coating compositions
CN117751168A (zh) * 2021-07-01 2024-03-22 Ppg工业俄亥俄公司 可电沉积的涂层组合物
EP4186951A1 (de) 2021-11-30 2023-05-31 BASF Coatings GmbH Verfahren zur herstellung einer mehrschichtlackierung
WO2023117897A1 (en) 2021-12-21 2023-06-29 Basf Se Outbound - chemical prodcut with environmental attributes

Family Cites Families (51)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3882008A (en) 1966-09-20 1975-05-06 Nippon Soda Co Water-soluble and/or water-dispersible coating material and composition
US3922253A (en) 1971-10-28 1975-11-25 Ppg Industries Inc Self-crosslinking cationic electrodepositable compositions
JPS5073560A (de) * 1973-10-30 1975-06-17
AU509166B2 (en) 1975-11-04 1980-04-24 Toyo Kohan Co. Ltd. Composite coated steel sheet
JPS5394346A (en) 1977-01-27 1978-08-18 Shinto Paint Co Ltd Novel powder coating composition for electrodeposition
US4134866A (en) * 1977-06-03 1979-01-16 Kansai Paint Company, Limited Aqueous cationic coating from amine-epoxy adduct, polyamide, and semi-blocked polyisocyanate, acid salt
AT352842B (de) 1977-06-06 1979-10-10 Herberts & Co Gmbh Waesseriges ueberzugsmittel, insbesondere fuer die elektro-tauchlackierung, sowie verfahren zu seiner herstellung
ES486439A1 (es) 1978-12-11 1980-06-16 Shell Int Research Un procedimiento para la preparacion de un revestimiento in-soluble e infusible sobre una superficie
ATE6942T1 (de) * 1979-02-27 1984-04-15 Imperial Chemical Industries Plc Verfahren zur beschichtung von gegenstaenden durch elektro-tauchlackierung, in diesem verfahren verwendete zusammensetzungen und beschichtete gegenstaende.
JPS5644799A (en) 1979-09-14 1981-04-24 Mitsubishi Rayon Co Ltd Grinding method for electrodeposition coated article
WO1981003292A1 (en) 1980-05-12 1981-11-26 Minnesota Mining & Mfg Composition for mechanically depositing heavy metallic coatings
DE3044447C2 (de) 1980-11-26 1982-12-09 Basf Farben + Fasern Ag, 2000 Hamburg Verfahren zum Beschichten eines als Kathode geschalteten elektrisch leitfähigen Substrates und wässrige Dispersion dafür
AT372099B (de) 1981-11-26 1983-08-25 Vianova Kunstharz Ag Verfahren zur herstellung von waermehaertbaren, kationischen, wasserverduennbaren ueberzugsmitteln
US4711397A (en) 1982-01-11 1987-12-08 Essex Group, Inc. Electromagnetic fuel injector having continuous flow path
US4444954A (en) 1982-09-30 1984-04-24 The Sherwin-Williams Company Water reducible quaternary ammonium salt containing polymers
DE3324211A1 (de) 1983-07-05 1985-01-17 Basf Farben + Fasern Ag, 2000 Hamburg Hitzehaertbare bindemittelmischung
US4870524A (en) 1984-07-06 1989-09-26 Furukawa Aluminum Co., Ltd. Substrate for rigid disk storage media
DE3436345A1 (de) 1984-10-04 1986-04-17 Herberts Gmbh, 5600 Wuppertal Kathodisch abscheidbares waessriges elektrotauchlack-ueberzugsmittel und dessen verwendung zum beschichten von gegenstaenden
DE3518732A1 (de) 1985-05-24 1986-11-27 BASF Lacke + Farben AG, 4400 Münster Wasserverduennbare bindemittel fuer kationische elektrotauchlacke und verfahren zu ihrer herstellung
DE3624454A1 (de) 1986-02-13 1987-08-20 Hoechst Ag Aminourethane, verfahren zu ihrer herstellung und ihre verwendung
DE3615810A1 (de) 1986-05-10 1987-11-12 Herberts Gmbh Kathodisch abscheidbares waessriges elektrotauchlackueberzugsmittel und seine verwendung
US4710542A (en) 1986-05-16 1987-12-01 American Cyanamid Company Alkylcarbamylmethylated amino-triazine crosslinking agents and curable compositions containing the same
DE3628121A1 (de) 1986-08-19 1988-03-03 Herberts Gmbh Fremdvernetzende bindemittelkombination fuer mit wasser verduennbare lacke, kathodisch abscheidbares elektrotauchlackueberzugsmittel und dessen verwendung
AU590960B2 (en) 1986-09-04 1989-11-23 Nippon Paint Co., Ltd. Electrodeposition coating composition
ZA873916B (en) 1986-09-26 1988-02-24 Inmont Basf Cationic electrodepositable resin compositions containing polyurethane resin dispersions
DE3733552A1 (de) 1987-10-03 1989-04-13 Herberts Gmbh Kathodisch abscheidbares waessriges elektrotauchlack-ueberzugsmittel und dessen verwendung
US4931157A (en) 1988-02-18 1990-06-05 Ppg Industries, Inc. Epoxy resin advancement using urethane polyols and method for use thereof
DE3809695A1 (de) * 1988-03-23 1989-10-12 Hoechst Ag Haerter fuer kunstharze, diesen enthaltende haertbare mischungen sowie deren verwendung
US5084541A (en) 1988-12-19 1992-01-28 American Cyanamid Company Triazine crosslinking agents and curable compositions
US4939213A (en) 1988-12-19 1990-07-03 American Cyanamid Company Triazine crosslinking agents and curable compositions containing the same
JPH0339370A (ja) * 1989-07-05 1991-02-20 Honny Chem Ind Co Ltd 艶消電着塗料組成物
AT394197B (de) 1989-08-23 1992-02-10 Vianova Kunstharz Ag Verfahren zur herstellung von bindemitteln fuer kathodisch abscheidbare lacke
DE3940782A1 (de) 1989-12-09 1991-06-13 Herberts Gmbh Waessriges ueberzugsmittel fuer die elektrotauchlackierung und seine verwendung bei der herstellung von mehrschichtlackierungen
DE3942766A1 (de) 1989-12-23 1991-06-27 Basf Lacke & Farben Verfahren zum beschichten elektrisch leitfaehiger substrate, waessriger lack, epoxid-aminaddukt und verwendung des epoxid-aminadduktes als reibharz zur herstellung von pigmentpasten
JPH0418460A (ja) 1990-05-11 1992-01-22 Kansai Paint Co Ltd カチオン電着塗料用樹脂組成物
JPH0423873A (ja) * 1990-05-18 1992-01-28 Japan Synthetic Rubber Co Ltd コーティング用組成物
AT394729B (de) 1990-09-17 1992-06-10 Vianova Kunstharz Ag Verfahren zur herstellung von vernetzungskomponenten fuer kathodisch abscheidbarelackbindemittel
US5158849A (en) 1990-10-25 1992-10-27 Custom Papers Group Inc. Composition useful in transparent conductive coatings
JPH04366123A (ja) * 1991-06-12 1992-12-18 Asahi Chem Ind Co Ltd 水性化ブロックイソシアナート及びそれを用いた塗料組成物
JP3130959B2 (ja) * 1991-06-12 2001-01-31 旭化成工業株式会社 水系塗料組成物
DE4204581A1 (de) 1992-02-15 1993-08-19 Basf Lacke & Farben Verfahren zum lackieren elektrisch leitfaehiger substrate, waessrige elektrotauchlacke, verfahren zur herstellung einer waessrigen dispersion vernetzter polymermikroteilchen und nach diesem verfahren hergestellte dispersionen
DE4237490A1 (de) 1992-11-06 1994-05-11 Herberts Gmbh Überzugsmittel und dessen Verwendung zur Herstellung von säurebeständigen Lackierungen
DE4303787C1 (de) 1993-02-10 1994-03-24 Herberts Gmbh Verfahren zur Herstellung von Elektrotauchlacküberzügen, die frei von Oberflächenstörungen sind und Verwendung von wäßrigen Polyvinylalkohollösungen zur Nachbehandlung von elektrophoretisch abgeschiedenen Überzügen
JPH06248204A (ja) 1993-02-26 1994-09-06 Pentel Kk 艶消し電着塗料
JPH06248200A (ja) 1993-02-26 1994-09-06 Kansai Paint Co Ltd 加熱硬化型振動吸収用塗料組成物
TW328955B (en) 1993-05-14 1998-04-01 Cytec Tech Corp Process for preparing bis- or tris-carbamate functional 1,3,5-triazines, substantially halogen contamination free crosslinker compositions and new bis-or tris-carbamate functional 1,3,5-triazines
US5430078A (en) 1993-08-31 1995-07-04 Basf Corporation Electrodeposition coating composition comprising cellulose additive
CA2213824A1 (en) 1995-02-28 1996-09-06 Henkel Corporation Reducing or avoiding surface irregularities in electrophoretic painting of phosphated metal surfaces
DE19618379A1 (de) 1996-05-08 1997-11-13 Basf Lacke & Farben Mit Copolymeren des Vinylacetats modifizierte in Wasser dispergierbare Epoxidharze
DE19622221A1 (de) * 1996-06-03 1997-12-04 Henkel Kgaa Verfahren zur Beschichtung elektrisch leitfähiger Substrate
JP2001011201A (ja) 1999-07-01 2001-01-16 Denki Kagaku Kogyo Kk クロロプレン共重合体と金属との加硫接着体

Also Published As

Publication number Publication date
EP1192226B1 (de) 2005-06-15
JP2003504448A (ja) 2003-02-04
ES2243279T3 (es) 2005-12-01
AU5979800A (en) 2001-01-22
DE19930060A1 (de) 2001-01-11
EP1192226A1 (de) 2002-04-03
BR0012095B1 (pt) 2010-11-03
DE50010568D1 (de) 2005-07-21
ATE297967T1 (de) 2005-07-15
BR0012095A (pt) 2002-04-02
WO2001002498A1 (de) 2001-01-11
US6951602B1 (en) 2005-10-04

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