JP5486300B2 - セラミック多孔質膜の製造方法及びセラミックフィルタの製造方法 - Google Patents
セラミック多孔質膜の製造方法及びセラミックフィルタの製造方法 Download PDFInfo
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- JP5486300B2 JP5486300B2 JP2009511295A JP2009511295A JP5486300B2 JP 5486300 B2 JP5486300 B2 JP 5486300B2 JP 2009511295 A JP2009511295 A JP 2009511295A JP 2009511295 A JP2009511295 A JP 2009511295A JP 5486300 B2 JP5486300 B2 JP 5486300B2
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- ceramic
- sol
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- substrate
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- 239000000919 ceramic Substances 0.000 title claims description 159
- 239000012528 membrane Substances 0.000 title claims description 68
- 238000004519 manufacturing process Methods 0.000 title claims description 43
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 58
- 239000000758 substrate Substances 0.000 claims description 57
- 239000000463 material Substances 0.000 claims description 36
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 30
- 239000000377 silicon dioxide Substances 0.000 claims description 29
- 239000011148 porous material Substances 0.000 claims description 26
- 238000001035 drying Methods 0.000 claims description 24
- 239000002904 solvent Substances 0.000 claims description 11
- 238000007664 blowing Methods 0.000 claims description 9
- 239000002344 surface layer Substances 0.000 claims description 7
- 239000010408 film Substances 0.000 description 79
- 210000004027 cell Anatomy 0.000 description 19
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 18
- 239000007788 liquid Substances 0.000 description 18
- 238000000034 method Methods 0.000 description 15
- 238000000576 coating method Methods 0.000 description 14
- 238000000926 separation method Methods 0.000 description 14
- 239000000243 solution Substances 0.000 description 14
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 12
- 230000015572 biosynthetic process Effects 0.000 description 11
- 239000011248 coating agent Substances 0.000 description 11
- 238000005755 formation reaction Methods 0.000 description 11
- 230000007547 defect Effects 0.000 description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 6
- 230000002093 peripheral effect Effects 0.000 description 6
- 230000000873 masking effect Effects 0.000 description 5
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 4
- 238000010790 dilution Methods 0.000 description 4
- 239000012895 dilution Substances 0.000 description 4
- 238000010304 firing Methods 0.000 description 4
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 3
- 238000001914 filtration Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 229910017604 nitric acid Inorganic materials 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 238000007605 air drying Methods 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- 230000018044 dehydration Effects 0.000 description 2
- 238000006297 dehydration reaction Methods 0.000 description 2
- 238000007865 diluting Methods 0.000 description 2
- 239000010410 layer Substances 0.000 description 2
- 238000001471 micro-filtration Methods 0.000 description 2
- 238000005192 partition Methods 0.000 description 2
- 239000012466 permeate Substances 0.000 description 2
- 239000010409 thin film Substances 0.000 description 2
- 238000009423 ventilation Methods 0.000 description 2
- 240000002853 Nelumbo nucifera Species 0.000 description 1
- 235000006508 Nelumbo nucifera Nutrition 0.000 description 1
- 235000006510 Nelumbo pentapetala Nutrition 0.000 description 1
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 description 1
- 239000003929 acidic solution Substances 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 150000004703 alkoxides Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 238000000861 blow drying Methods 0.000 description 1
- 229910010293 ceramic material Inorganic materials 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 229910052878 cordierite Inorganic materials 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- JSKIRARMQDRGJZ-UHFFFAOYSA-N dimagnesium dioxido-bis[(1-oxido-3-oxo-2,4,6,8,9-pentaoxa-1,3-disila-5,7-dialuminabicyclo[3.3.1]nonan-7-yl)oxy]silane Chemical compound [Mg++].[Mg++].[O-][Si]([O-])(O[Al]1O[Al]2O[Si](=O)O[Si]([O-])(O1)O2)O[Al]1O[Al]2O[Si](=O)O[Si]([O-])(O1)O2 JSKIRARMQDRGJZ-UHFFFAOYSA-N 0.000 description 1
- KZHJGOXRZJKJNY-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Si]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O KZHJGOXRZJKJNY-UHFFFAOYSA-N 0.000 description 1
- 238000003618 dip coating Methods 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 230000001747 exhibiting effect Effects 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 229910052863 mullite Inorganic materials 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 238000001612 separation test Methods 0.000 description 1
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 1
- 229910010271 silicon carbide Inorganic materials 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 239000011550 stock solution Substances 0.000 description 1
- 238000000108 ultra-filtration Methods 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
- B01D67/0039—Inorganic membrane manufacture
- B01D67/0048—Inorganic membrane manufacture by sol-gel transition
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D63/00—Apparatus in general for separation processes using semi-permeable membranes
- B01D63/06—Tubular membrane modules
- B01D63/066—Tubular membrane modules with a porous block having membrane coated passages
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2323/00—Details relating to membrane preparation
- B01D2323/42—Details of membrane preparation apparatus
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dispersion Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2009511295A JP5486300B2 (ja) | 2006-10-18 | 2007-10-18 | セラミック多孔質膜の製造方法及びセラミックフィルタの製造方法 |
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2006284400 | 2006-10-18 | ||
| JP2006284400 | 2006-10-18 | ||
| JP2009511295A JP5486300B2 (ja) | 2006-10-18 | 2007-10-18 | セラミック多孔質膜の製造方法及びセラミックフィルタの製造方法 |
| PCT/JP2007/070763 WO2008050814A1 (en) | 2006-10-18 | 2007-10-18 | Method of manufacturing ceramic porous membrane and method of manufacturing ceramic filter |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2010506699A JP2010506699A (ja) | 2010-03-04 |
| JP2010506699A5 JP2010506699A5 (enExample) | 2012-04-05 |
| JP5486300B2 true JP5486300B2 (ja) | 2014-05-07 |
Family
ID=39099680
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2009511295A Active JP5486300B2 (ja) | 2006-10-18 | 2007-10-18 | セラミック多孔質膜の製造方法及びセラミックフィルタの製造方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US20080096751A1 (enExample) |
| EP (1) | EP2083942A1 (enExample) |
| JP (1) | JP5486300B2 (enExample) |
| CN (1) | CN101528329B (enExample) |
| AU (1) | AU2007310057B2 (enExample) |
| BR (1) | BRPI0717636A2 (enExample) |
| CA (1) | CA2666279C (enExample) |
| WO (1) | WO2008050814A1 (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20180081194A (ko) * | 2017-01-05 | 2018-07-16 | 한국기계연구원 | 세라믹 분리막의 표면 개질 방법 |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7923060B2 (en) * | 2006-10-18 | 2011-04-12 | Ngk Insulators, Ltd. | Method of manufacturing ceramic filter |
| JP2010089000A (ja) * | 2008-10-07 | 2010-04-22 | Ngk Insulators Ltd | 分離膜の製造方法 |
| CN101664646B (zh) * | 2009-09-27 | 2012-09-19 | 南京工业大学 | 一种陶瓷超滤膜的制备方法及自动涂膜装置 |
| JP5662937B2 (ja) * | 2009-09-29 | 2015-02-04 | 日本碍子株式会社 | ゼオライト膜の製造方法、およびその製造方法により得られたゼオライト膜 |
| JP5075186B2 (ja) * | 2009-10-30 | 2012-11-14 | 日本碍子株式会社 | ナノ濾過膜の製造方法 |
| US8926926B2 (en) * | 2009-11-25 | 2015-01-06 | GM Global Technology Operations LLC | Exhaust particulate management for gasoline-fueled engines |
| WO2011118252A1 (ja) | 2010-03-24 | 2011-09-29 | 日本碍子株式会社 | シリカ膜の製造方法 |
| JP2012040549A (ja) | 2010-07-22 | 2012-03-01 | Ngk Insulators Ltd | シリカ膜、及びその製造方法 |
| CN102989326B (zh) * | 2011-09-09 | 2014-10-29 | 佛山高品环保技术有限公司 | 一种用于循环水处理的陶瓷膜及其制备方法 |
| WO2013145318A1 (ja) * | 2012-03-30 | 2013-10-03 | イビデン株式会社 | ハニカムフィルタ及びハニカムフィルタの製造方法 |
| WO2014081218A1 (ko) * | 2012-11-21 | 2014-05-30 | 한국생산기술연구원 | 세라믹 필터의 제조방법 |
| US9796632B2 (en) | 2012-11-21 | 2017-10-24 | Korea Institute Of Industrial Technology | Method for manufacturing ceramic filter |
| CN103230746B (zh) * | 2013-04-17 | 2015-02-18 | 滨州学院 | 一种无机微滤膜的涂膜设备及方法 |
| KR101725256B1 (ko) * | 2016-09-05 | 2017-04-11 | 주식회사 이앤이켐 | 고열전도성 세라믹 코팅제 및 이의 시공방법 |
| CN110272298B (zh) * | 2018-03-16 | 2022-05-06 | 翁志龙 | 一种氧化钛陶瓷超滤膜的制备方法 |
| JP7505750B2 (ja) | 2019-08-05 | 2024-06-25 | 国立大学法人広島大学 | 分離膜の製造方法及び分離膜 |
Family Cites Families (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5523021A (en) * | 1978-08-04 | 1980-02-19 | Nissan Motor | Method of coating oneebody carrier |
| NL8303079A (nl) * | 1983-09-05 | 1985-04-01 | Stichting Energie | Werkwijze voor de bereiding van scheurvrije semi-permeabele anorganische membranen. |
| JPS61238315A (ja) * | 1985-04-12 | 1986-10-23 | Ngk Insulators Ltd | 複層フイルタの製造方法 |
| US4980062A (en) * | 1988-09-16 | 1990-12-25 | W. R. Grace & Co.-Conn. | Inorganic membrane |
| JPH0398626A (ja) * | 1989-09-13 | 1991-04-24 | Ngk Insulators Ltd | 無機多孔質膜およびその製造法 |
| US5342431A (en) * | 1989-10-23 | 1994-08-30 | Wisconsin Alumni Research Foundation | Metal oxide membranes for gas separation |
| US5269926A (en) * | 1991-09-09 | 1993-12-14 | Wisconsin Alumni Research Foundation | Supported microporous ceramic membranes |
| JPH0745010B2 (ja) | 1990-03-16 | 1995-05-17 | 日本碍子株式会社 | セラミック膜フイルタ |
| JPH0899027A (ja) * | 1994-09-30 | 1996-04-16 | Kyocera Corp | ガス分離用セラミック構造体及びその製造方法 |
| JP3769739B2 (ja) * | 1994-11-17 | 2006-04-26 | 住友電気工業株式会社 | 多孔質セラミックス膜及びその製造方法 |
| US5772735A (en) * | 1995-11-02 | 1998-06-30 | University Of New Mexico | Supported inorganic membranes |
| IN195165B (enExample) * | 1996-06-21 | 2005-01-28 | Engelhard Corp | |
| US20010026838A1 (en) * | 1996-06-21 | 2001-10-04 | Engelhard Corporation | Monolithic catalysts and related process for manufacture |
| US5953832A (en) * | 1998-04-28 | 1999-09-21 | Engelhard Corporation | Method for drying a coated substrate |
| FR2754737B1 (fr) * | 1996-10-21 | 1999-01-15 | Tech Sep | Membrane inorganique de nanofiltration et son application dans l'industrie sucriere |
| US6341701B1 (en) * | 1996-12-27 | 2002-01-29 | Ngk Insulators, Ltd. | Ceramic porous membrane including ceramic of ceramic and ceramic sol particles, ceramic porous body including the membrane, and method of manufacturing the membrane |
| JP3589559B2 (ja) * | 1996-12-27 | 2004-11-17 | 日本碍子株式会社 | セラミックス多孔質膜、これを用いたセラミックス多孔質体及びこれらの製造方法 |
| JP3774037B2 (ja) * | 1996-12-27 | 2006-05-10 | 日本碍子株式会社 | チタニアを結合材とするセラミックス多孔質膜、これを用いたセラミックスフィルター及びこれらの製造方法 |
| JPH10249175A (ja) * | 1997-03-12 | 1998-09-22 | Kyocera Corp | 多孔質分離膜及びその製造方法 |
| EP1089806B1 (en) * | 1998-05-28 | 2004-06-16 | Stichting Energieonderzoek Centrum Nederland | Process of producing a microporous hydrophobic inorganic membrane |
| JP2001261465A (ja) * | 2000-03-16 | 2001-09-26 | Ngk Insulators Ltd | セラミックス多孔質フィルターの製造方法 |
| JP2001259324A (ja) * | 2000-03-23 | 2001-09-25 | Ngk Insulators Ltd | セラミックスフィルターの製造方法 |
| US7100707B2 (en) * | 2004-01-16 | 2006-09-05 | Harold Howard | Stabilized soil core samples and method for preparing same |
| JP2005247605A (ja) * | 2004-03-02 | 2005-09-15 | Ngk Insulators Ltd | セラミック多孔質体及びその製造方法 |
| DE102004040548A1 (de) * | 2004-08-21 | 2006-02-23 | Umicore Ag & Co. Kg | Verfahren zum Beschichten eines Wandflußfilters mit feinteiligen Feststoffen und damit erhaltenes Partikelfilter und seine Verwendung |
| JP2006189027A (ja) * | 2004-12-06 | 2006-07-20 | Denso Corp | 排ガス浄化フィルタ |
| US7923060B2 (en) * | 2006-10-18 | 2011-04-12 | Ngk Insulators, Ltd. | Method of manufacturing ceramic filter |
-
2007
- 2007-09-06 US US11/850,696 patent/US20080096751A1/en not_active Abandoned
- 2007-10-18 CA CA2666279A patent/CA2666279C/en not_active Expired - Fee Related
- 2007-10-18 EP EP07830497A patent/EP2083942A1/en not_active Withdrawn
- 2007-10-18 JP JP2009511295A patent/JP5486300B2/ja active Active
- 2007-10-18 BR BRPI0717636-8A2A patent/BRPI0717636A2/pt not_active Application Discontinuation
- 2007-10-18 AU AU2007310057A patent/AU2007310057B2/en not_active Ceased
- 2007-10-18 CN CN200780038792XA patent/CN101528329B/zh not_active Expired - Fee Related
- 2007-10-18 WO PCT/JP2007/070763 patent/WO2008050814A1/en not_active Ceased
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20180081194A (ko) * | 2017-01-05 | 2018-07-16 | 한국기계연구원 | 세라믹 분리막의 표면 개질 방법 |
Also Published As
| Publication number | Publication date |
|---|---|
| EP2083942A1 (en) | 2009-08-05 |
| AU2007310057A1 (en) | 2008-05-02 |
| CN101528329B (zh) | 2013-07-10 |
| WO2008050814A1 (en) | 2008-05-02 |
| CA2666279C (en) | 2013-04-02 |
| CN101528329A (zh) | 2009-09-09 |
| US20080096751A1 (en) | 2008-04-24 |
| BRPI0717636A2 (pt) | 2013-10-15 |
| JP2010506699A (ja) | 2010-03-04 |
| CA2666279A1 (en) | 2008-05-02 |
| AU2007310057B2 (en) | 2011-09-22 |
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