JP5467863B2 - 電極活性材料の作製方法 - Google Patents

電極活性材料の作製方法 Download PDF

Info

Publication number
JP5467863B2
JP5467863B2 JP2009506784A JP2009506784A JP5467863B2 JP 5467863 B2 JP5467863 B2 JP 5467863B2 JP 2009506784 A JP2009506784 A JP 2009506784A JP 2009506784 A JP2009506784 A JP 2009506784A JP 5467863 B2 JP5467863 B2 JP 5467863B2
Authority
JP
Japan
Prior art keywords
precursor compounds
alkali metal
mixtures
vanadyl
group
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2009506784A
Other languages
English (en)
Japanese (ja)
Other versions
JP2009534288A (ja
Inventor
フォークナー タイタス
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Valence Technology Inc
Original Assignee
Valence Technology Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Valence Technology Inc filed Critical Valence Technology Inc
Publication of JP2009534288A publication Critical patent/JP2009534288A/ja
Application granted granted Critical
Publication of JP5467863B2 publication Critical patent/JP5467863B2/ja
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00Phosphorus; Compounds thereof
    • C01B25/16Oxyacids of phosphorus; Salts thereof
    • C01B25/26Phosphates
    • C01B25/45Phosphates containing plural metal, or metal and ammonium
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/14Phosphorus; Compounds thereof
    • B01J27/186Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J27/195Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium with vanadium, niobium or tantalum
    • B01J27/198Vanadium
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B15/00Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
    • C01B15/055Peroxyhydrates; Peroxyacids or salts thereof
    • C01B15/16Peroxyhydrates; Peroxyacids or salts thereof containing phosphorus
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G31/00Compounds of vanadium
    • C01G31/006Compounds containing, besides vanadium, two or more other elements, with the exception of oxygen or hydrogen
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/58Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/5825Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/70Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/40Electric properties
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/052Li-accumulators
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/13Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/136Electrodes based on inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Secondary Cells (AREA)
  • Electrodes For Compound Or Non-Metal Manufacture (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
JP2009506784A 2006-04-21 2007-04-20 電極活性材料の作製方法 Expired - Fee Related JP5467863B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US11/379,754 US7790319B2 (en) 2006-04-21 2006-04-21 Method for making electrode active material
US11/379,754 2006-04-21
PCT/US2007/067051 WO2007124401A2 (en) 2006-04-21 2007-04-20 Method for making electrode active material

Publications (2)

Publication Number Publication Date
JP2009534288A JP2009534288A (ja) 2009-09-24
JP5467863B2 true JP5467863B2 (ja) 2014-04-09

Family

ID=38619655

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2009506784A Expired - Fee Related JP5467863B2 (ja) 2006-04-21 2007-04-20 電極活性材料の作製方法

Country Status (7)

Country Link
US (2) US7790319B2 (ko)
EP (1) EP2010454A4 (ko)
JP (1) JP5467863B2 (ko)
KR (1) KR101392012B1 (ko)
CN (1) CN101426721B (ko)
CA (1) CA2649747C (ko)
WO (1) WO2007124401A2 (ko)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5396798B2 (ja) * 2008-09-30 2014-01-22 Tdk株式会社 活物質材料、それを用いた正極及びリチウムイオン二次電池
JP5347604B2 (ja) * 2009-03-16 2013-11-20 Tdk株式会社 α型結晶構造のLiVOPO4を主成分とする活物質粒子、これを含む電極、当該電極を備えるリチウム二次電池、及びこの活物質粒子の製造方法
JP5515343B2 (ja) * 2009-03-16 2014-06-11 Tdk株式会社 活物質の製造方法、活物質、電極及びリチウムイオン二次電池
CN102473905A (zh) * 2009-07-14 2012-05-23 川崎重工业株式会社 具备纤维电极的蓄电设备及其制造方法
US20110052473A1 (en) * 2009-08-25 2011-03-03 Tdk Corporation Method of manufacturing active material
JP5444942B2 (ja) * 2009-08-25 2014-03-19 Tdk株式会社 活物質の製造方法
JP5444943B2 (ja) * 2009-08-25 2014-03-19 Tdk株式会社 活物質の製造方法
JP5444944B2 (ja) * 2009-08-25 2014-03-19 Tdk株式会社 活物質及び活物質の製造方法
US20110052995A1 (en) * 2009-08-28 2011-03-03 Tdk Corporation Active material, electrode containing the same, lithium secondary battery provided therewith and method for manufacture of the active material
WO2012023439A1 (ja) * 2010-08-18 2012-02-23 株式会社 村田製作所 リン酸鉄の製造方法、リン酸鉄リチウム、電極活物質、及び二次電池
TW201311548A (zh) * 2011-08-03 2013-03-16 Murata Manufacturing Co 磷酸鋰鐵之製造方法、電極活性物質及二次電池
TW201311547A (zh) * 2011-08-03 2013-03-16 Murata Manufacturing Co 磷酸鋰鐵之製造方法、電極活性物質及二次電池
JP5610014B2 (ja) * 2012-03-27 2014-10-22 Tdk株式会社 リチウムイオン二次電池
JP2013206554A (ja) * 2012-03-27 2013-10-07 Tdk Corp 活物質、電極及びリチウムイオン二次電池
WO2013146864A1 (ja) * 2012-03-27 2013-10-03 Tdk株式会社 活物質、およびそれを用いた電極、ならびにリチウムイオン二次電池
JP6065746B2 (ja) * 2013-05-22 2017-01-25 株式会社豊田自動織機 層状岩塩構造の活物質の製造方法、層状岩塩構造の活物質
US9722247B2 (en) * 2015-06-10 2017-08-01 Toyota Motor Engineering & Manufacturing North America, Inc. Vanadyl phosphates as high energy density cathode materials for rechargeable sodium battery
US11289700B2 (en) 2016-06-28 2022-03-29 The Research Foundation For The State University Of New York KVOPO4 cathode for sodium ion batteries
US11251430B2 (en) 2018-03-05 2022-02-15 The Research Foundation For The State University Of New York ϵ-VOPO4 cathode for lithium ion batteries
CN110085925B (zh) * 2019-04-29 2020-08-04 中南大学 一种水系锌离子电池电解质膜及其制备和应用方法
CN111082018A (zh) * 2019-12-24 2020-04-28 湖南科技大学 一种LiVOPO4/C复合正极材料的制备方法

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6261988B1 (en) * 1996-03-08 2001-07-17 Nippon Shokubai Co., Ltd. Metal ion-exchanged phosphorus-vanadium compound and solid acid catalyst using the compound
US7189475B2 (en) * 2000-07-27 2007-03-13 Kabushiki Kaisha Toyota Chuo Kenkyusho Lithium secondary battery
JP4314859B2 (ja) * 2003-03-31 2009-08-19 祐作 滝田 非水電解質二次電池用電極活物質、非水電解質二次電池用電極及び非水電解質二次電池
US6858561B2 (en) * 2003-05-15 2005-02-22 Scientific Design Company, Inc. Phosphorus/vanadium catalyst preparation
JP4407211B2 (ja) * 2003-09-02 2010-02-03 日産自動車株式会社 非水電解質二次電池

Also Published As

Publication number Publication date
CN101426721B (zh) 2014-03-12
EP2010454A4 (en) 2015-04-29
WO2007124401A2 (en) 2007-11-01
US7790319B2 (en) 2010-09-07
CA2649747A1 (en) 2007-11-01
KR20080111077A (ko) 2008-12-22
EP2010454A2 (en) 2009-01-07
WO2007124401A3 (en) 2008-08-21
CA2649747C (en) 2014-09-09
CN101426721A (zh) 2009-05-06
KR101392012B1 (ko) 2014-05-07
JP2009534288A (ja) 2009-09-24
US20100303701A1 (en) 2010-12-02
US20070248520A1 (en) 2007-10-25
US8318353B2 (en) 2012-11-27

Similar Documents

Publication Publication Date Title
JP5467863B2 (ja) 電極活性材料の作製方法
US11251428B2 (en) Positive electrode active material manufacturing method with control of washing slurry liquid electrical conductivity
KR102202822B1 (ko) 비수계 전해질 이차전지용 정극 활물질, 이러한 비수계 전해질 이차전지용 정극 활물질의 제조 방법 및 이러한 비수계 전해질 이차전지용 정극 활물질을 이용한 비수계 전해질 이차전지
JP5544163B2 (ja) リチウム電池用高性能カソード材料
JP6116800B2 (ja) 正極活物質、これを採用した正極及びリチウム電池、並びにその製造方法
US7524584B2 (en) Electrode active material for a secondary electrochemical cell
JP5384935B2 (ja) 二次電気化学電池
US20070072034A1 (en) Secondary electrochemical cell
KR102420738B1 (ko) 비수계 전해질 이차 전지용 정극 활물질과 그의 제조 방법, 및 이 정극 활물질을 이용한 비수계 전해질 이차 전지
US10164250B2 (en) Lithium-iron-manganese-based composite oxide and lithium-ion secondary battery using same
KR20150090751A (ko) 양극 활물질 및 그 제조방법, 상기 양극 활물질을 채용한 양극과 리튬 전지
JP2017117700A (ja) 非水系電解質二次電池用正極活物質の製造方法
US20180069236A1 (en) Lithium-iron-manganese-based composite oxide and lithium-ion secondary battery using same
JP5284950B2 (ja) 新規な電極活性材料を有する2次電気化学セル
WO2019004148A1 (ja) 非水電解質二次電池用正極活物質、およびその製造方法、並びに、非水電解質二次電池
KR102420737B1 (ko) 비수계 전해질 이차 전지용 정극 활물질과 그의 제조 방법, 및 이 정극 활물질을 이용한 비수계 전해질 이차 전지
CN111587501A (zh) 用于可再充电锂电池的正极活性材料、包括其的正极和可再充电锂电池
WO2024122440A1 (ja) リチウム二次電池用正極活物質、その製造方法及びリチウム二次電池
JP2002246021A (ja) 非水電解質二次電池の負極用リチウム含有複合窒化物の製造法

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20100416

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20130326

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20130624

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20140114

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20140128

R150 Certificate of patent or registration of utility model

Free format text: JAPANESE INTERMEDIATE CODE: R150

LAPS Cancellation because of no payment of annual fees